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Mixed results of seven methods for organic residue analysis applied to one vessel with the residue of a known foodstuff
Institution:1. Separation Science Group, Department of Organic and Macromolecular Chemistry, Ghent University, Krijgslaan 281 S4, B-9000 Gent, Belgium;2. Historical Archaeology Research Group, Department of Archaeology, Ghent University, Sint-Pietersnieuwstraat 35, The UFO, B-9000 Gent, Belgium;3. Monument Vandekerckhove nv, Afdeling Archeologie, Oostrozebekestraat 54, B-8770 Ingelmunster, Belgium;4. Archaeometry and Natural Sciences, Department of Archaeology, Ghent University, Sint-Pietersnieuwstraat 35, The UFO, B-9000 Gent, Belgium;5. Raman Spectroscopy Research Group, Department of Analytical Chemistry, Ghent University, Krijgslaan 281 S12, B-9000 Gent, Belgium;1. University Research Institute for Iberian Archaeology, University of Jaén, Campus Las Lagunillas, 23071 Jaén, Spain;2. Analytical Chemistry Research Group, Department of Physical and Analytical Chemistry, University of Jaén, Campus Las Lagunillas, 23071 Jaén, Spain
Abstract:Several methods of archaeological organic residue analysis were applied to a single unglazed and unseasoned ceramic vessel that had absorbed residues of heated camel milk. Sections of the wall of this vessel were sent to eleven archaeological laboratories. Seven reported their results before the identity of the residue was revealed, during the 70th Annual Meeting of the Society for American Archaeology. Methods included stable carbon and nitrogen isotope ratio analysis, protein analysis and lipid analysis. These laboratory techniques provide a biochemical analysis of the residue in a ceramic matrix, the archaeological interpretation of which can be rather difficult. The exact source of the residue was not identified by any laboratory, but it is evident that residue analysis can provide valuable information, especially when combined with additional archaeological and historical data. We therefore support a close cooperation of those working in this field to develop it to its full potential.
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