Justification for reassessing elemental analysis data of ceramics,sediments and lithics using rare earth element concentrations and ratios

The mensuration of multi‐elemental concentrations from assorted archaeological materials has always required great care and attention to detail to ensure good‐quality data and their ensuing interpretations. Although most suspect data were generated before the wide use of computers, error‐free data are not still a certainty. This paper presents the geochemical rationale for a proposed chemical data‐assessment process, using a globally dispersed collection of ceramic, sediment and lithic data. It is argued that this process can allow archaeologists and archaeometrists to investigate systematically older and current data sets and, if need be, alter them to the reliable values they were originally intended to include.     

The Hellenistic and Roman Syracuse (Sicily) Fine Pottery Production Explored by Chemical and Petrographic Analysis

The chemical composition and petrographic features of 51 samples of fine pottery selected from the archaeological site of Syracuse have been established by means of optical microscopy and X‐ray fluorescence spectrometry, with the aim of creating a reference group for the ceramics produced in this important Greek colony during the Hellenistic–Roman period. This reference group is constrained by the analysis of six kiln wasters and of raw materials outcropping in the studied area. Among the studied findings, the main part is assignable imputably to local production, while some specimens probably come from Greece and other colonies (Messina and Gela). The Syracuse fine pottery is characterized by inclusions formed mainly by quartz and micaceous and fossiliferous groundmass. The used pastes were more or less purified through the removal of the sandy‐to‐coarse silty granulometric fraction. The multivariate statistical analysis of chemical data permits the identification of production at Syracuse on the basis of comparison with the kiln wasters and the Plio‐Pleistocene clays.     

The potential of chironomid (Insecta: Diptera) larvae in archaeological investigations of floodplain and lake settlements

The head capsules of chironomids (Insecta: Diptera) are well preserved in sediments and can be recognised to a high taxonomic level, usually genus and sometimes species. Work on lake sediments has shown that they can be accurate indicators of water temperature, oxygen regimes, and nutrient status (particularly total phosphorus and chlorophyll-a), as well as heavy metal pollution. No systematic chironomid analyses, however, have previously been undertaken on archaeological deposits. In order to address this we assessed the use of chironomids in three types of archaeological deposit; firstly, a lake core at the edge of a lake settlement (crannog), secondly, a palaeochannel infill adjacent to a multi-period settlement site and lastly, a Roman well deposit from a floodplain environment. The chironomid assemblages are shown to vary significantly both between and within the sites and reflect the immediate environment and the adjacent area. The lake sediment assemblage reflects the construction of the crannog through elevated levels of organic detritus, wood and woody debris. The palaeochannel assemblage reveals changing natural conditions and nutrient enrichment probably associated with settlement during the Saxon period. The well assemblage is taxonomically restricted and indicative of organic debris, dead plant material, animal dung and possibly human effluent deposited after abandonment of the well. Dry storage of the palaeochannel and well sediments for several years did not appear to affect the concentration or state of preservation of the head capsules. The chironomid reconstructions are shown to provide an additional indicator of human activity which has the potential to provide quantitative data on the character of aquatic environments associated with archaeological sites.     

The application of luminescence dating in American archaeology

Luminescence dating is underutilized in American archaeology given the theoretical advantages of direct dating that it confers. Recent advances in understanding the physical processes underlying the method have also made it more reliable as a dating tool. This research as well as potential applications is reviewed.     

Archaeopedological analyses around a Neolithic hearth and the beginning of Sabaean irrigation in the oasis of Ma'rib (Ramlat as-Sab'atayn,Yemen)

Archaeopedological analyses in the oasis of Ma'rib (Yemen) yield new information of Neolithic land use, Bronze Age soil formation, and Sabaean irrigation. The AMS radiocarbon age of a Neolithic fireplace buried under Sabaean irrigation sediments in the Southern oasis indicates Pre-Sabaean human activities in Wadi Dhana about 5600 years ago. The associated Mid-Holocene palaeosol, developed in fluvial sediments of Wadi Dhana and also in the filling of the hearth, marks the Bronze Age-land surface before it was covered with irrigation sediments. Based on AMS radiocarbon data from charcoal in reservoir sediments of the “Great Dam” and an estimated time span of pedogenesis of the Mid-Holocene palaeosol in this region, we propose the beginning of the irrigation in Ma'rib in the period of 2500–1000 cal yr BC.     

On the Possible Origins of an Unusual (Mid to Late Holocene) Coastal Deposit,Old Punt Bay,South‐East Australia

An unusual coarse, shelly sedimentary unit is found elevated above present mean sea level in a sheltered pocket embayment at Old Punt Bay in south‐eastern Australia. The coarse sediments, diverse microfauna, and large shelly macrofauna of mixed affinity suggest that the deposit is the result of high‐energy deposition. The deposit was previously thought to have been deposited 1000–1300 cal bp based on one shell dated using ¹⁴C and amino acid racemisation. However, additional ¹⁴C dating indicates a likely age of ～2500 cal bp . Regardless of age constraints, the presence of rock‐encrusting oyster shells and large articulated bivalves, suggests that the depositional event must have been capable of removing and transporting coarse sediments (rock clasts), bivalves, and oysters shells from a variety of seaward environments and depositing them with little abrasion, something storm waves are unlikely to do. The deposit may be tsunamigenic. If a tsunami origin is accepted, the new dating results indicate that it is possibly coeval with a tsunami event previously reported to have affected several other sites along the coast of New South Wales at c. 2900 cal bp . Consequently, this deposit provides evidence for the event at a new site and importantly, a tighter constraint on the likely date of the events occurrence. It further adds weight to the developing catalogue of palaeotsunamis that may have affected the south‐eastern coast of Australia. Regardless of the deposit's origins, if viewed from a coastal planning perspective, this deposit indicates that this part of the coast has experienced large‐scale overwash events in the past that if repeated, would be catastrophic. There are serious implications for risk management.     

Provenance study of early and middle bronze age pottery from Kaman-Kalehöyük,Turkey, by heavy mineral analysis and geochemical analysis of individual hornblende grains

The provenance of Early Bronze Age and early Middle Bronze Age pottery produced between 2100 and 1970 B.C. and excavated from Kaman-Kalehöyük, Turkey was studied using mineralogical methods, including heavy mineral analysis and geochemical study of individual hornblende grains. The relative abundances of heavy minerals in the fabrics of 20 Early Bronze Age (EBA) and early Middle Bronze Age (MBA) pottery sherds, together with 27 local sediments collected within a radius of 25 km of the site were studied. The heavy mineral distributions in the Kaman region were statistically analyzed for consistencies in their occurrence. Amphibole was found to be the most abundant heavy mineral in most of the analyzed samples, followed by titanite and epidote. The amounts of other minerals such as garnet, clinopyroxene, and zircon are subordinate. Different proportions of heavy minerals in the fabrics allow categorization of the EBA and early MBA potteries into 5 groups. Comparative study of heavy mineral assemblages of local sediments and pottery suggests that half of the EBA and most of the MBA potteries were produced from sediment near the excavation site, whereas the other half of the EBA potteries were produced from sediment occurring at 25 km east or more east of the site. The geochemistry of individual amphibole grains was studied by electron-microprobe analysis. Most of the studied amphibole grains are calcic and aluminous, corresponding to hornblende. They can be further characterized into four types based on their chemical composition. The combination of heavy mineral identity and hornblende geochemistry provides diagnostic evidence for the origins of Kaman-Kalehöyük pottery. These and analogous heavy mineral techniques are effective archaeometric tools for determining pottery provenance.     

A modified sampler for uncontaminated DNA cores from soft sediments

A piston-type mud sampler is described. It is a development of the Livingstone corer and was designed to extract cores for DNA analysis of sediments. Prevention of contamination was paramount. As the entire system is self-contained and the sample is retained in the corer, it was found ideal for extracting very soft sediments which could not be captured by existing corers.     

Sediments exposed to high temperatures: reconstructing pyrotechnological processes in Late Bronze and Iron Age Strata at Tel Dor (Israel)

Many of the sediments analysed from Tel Dor (Israel) show structural alterations indicating that they were exposed to high temperatures. This observation is consistent with the abundant evidence for use of pyrotechnology from the earliest exposed Middle Bronze Age strata through the Roman period. Such structurally altered sediments may well represent one of the more widespread and durable records of pyrotechnology, and as such could be invaluable for reconstructing past human activities. The specific aims of this research are therefore to develop the means for identifying local sediments that were altered by different pyrotechnological activities and to elucidate the varying circumstances whereby sediments were exposed to high temperatures in a Late Bronze and Iron Age 1 section.