The 9th‐Century‐AD Belitung Wreck,Indonesia: analysis of a resin lump

The 9th‐century‐AD Belitung wreck was discovered in 1998 in the Java Sea. Construction techniques rapidly confirmed that it was unlike any known Chinese or Southeast Asian vessel. The uncertainty about its origins was resolved in 2008 by timber identifications: it was constructed in the Middle East (probably Oman or Yemen). This paper, on the characterization of a dammar resin lump collected in the vicinity of the wreck, supplies additional evidence confirming the probable re‐stitching of the vessel somewhere in Asia. © 2010 The Authors     

Species identification of archaeological dung remains: A critical review of potential methods

Abstract

Dung, macroscopically recognisable as such or not, can more commonly be found in archaeological contexts than is perhaps realised. Up to now, identification of dung to the species which produced it is usually either tenuous, or is not possible. However, species identification can be very informative and is necessary before any further studies can be conducted on the dung, for example on health and hygiene in the past and palaeoecology. This study presents a review of potential methods by which species identifications of archaeological dung can be undertaken. Criteria for identification can be divided into three broad categories: morphometric features of the dung; the content of dung and contextual evidence. Overall, the chances of a precise identification are high; however, a combination of different criteria and techniques will often be necessary to establish a secure identification. Moreover, preservation issues may exclude the application of some criteria while several criteria require more research and the expansion of reference collections of recent material. The overall aim is to move towards standardised methods for species identification of archaeological dung.     

Biomolecular archaeology of ancient tuberculosis: response to “Deficiencies and challenges in the study of ancient tuberculosis DNA” by Wilbur et al. (2009)

It is sixteen years since the first detection of Mycobacterium tuberculosis DNA in archaeological specimens, yet the validity of findings continues to be questioned. Rigorous scientific scrutiny and debate is valuable and has led to a coalescence of procedures and precautions amongst those actively engaged in this work. It is disappointing that these good practices are not recognised by certain scientists whose primary expertise is in the related fields of archaeology, palaeopathology, and eukaryote ancient DNA. There is a danger that by constant repetition, disputable and inadequately justified concerns will assume the status of self-perpetuating myths and misunderstandings. We discuss these issues with reference to a recent article in this journal, in which clear peer-reviewed scientific data were specifically targeted as part of a general critique of the field of the palaeomicrobiology of tuberculosis. We believe we have given sufficient evidence and cogent argument to persuade the unbiased reader that the views in the critique by Wilbur et al. are unjustified.     

Biostratigraphic Evidence Relating to the Age‐Old Question of Hannibal's Invasion of Italy,II: Chemical Biomarkers and Microbial Signatures

As discussed in Part I, a large accumulation of mammalian faeces at the mire site in the upper Guil Valley near Mt. Viso, dated to 2168 cal ¹⁴C yr., provides the first evidence of the passage of substantial but indeterminate numbers of mammals within the time frame of the Punic invasion of Italia. Specialized organic biomarkers bound up in a highly convoluted and bioturbated bed constitute an unusual anomaly in a histosol comprised of fibric and hemist horizons that are usually expected to display horizontal bedding. The presence of deoxycholic acid and ethylcoprostanol derived from faecal matter, coupled with high relative numbers of Clostridia 16S rRNA genes, suggests a substantial accumulation of mammalian faeces at the site over 2000 years ago. The results reported here constitute the first chemical and biological evidence of the passage of large numbers of mammals, possibly indicating the route of the Hannibalic army at this time. Combined with the geological analysis reported in Part I, these data provide a background supporting the need for further historical archaeological exploration in this area.     

A comparative geochemical study of bituminous boat remains from H3, As-Sabiyah (Kuwait), and RJ-2, Ra's al-Jinz (Oman)

This paper presents a geochemical analysis of fragments of bituminous amalgam from H3, As‐Sabiyah (Kuwait), and RJ‐2, Ra's al‐Jinz (Oman). The fragments bear barnacles on one side and reed impressions on the other, and are thought to have been part of the coating of reed‐bundle boats. The material from H3 dates to between 5300–4900 BC, while that of RJ‐2 dates to 2500–2100 BC. Samples from both sites were geochemically compared to archaeological and ethnographic material from Kosak Shamali (northern Syria, c.5000–4400 BC), RH‐5 (Oman, 4400–3500 BC) and Baghdad (central Iraq, 1900 AD). The composition of the bituminous amalgams was studied in detail. Rock‐Eval Pyrolysis gave a measure of Total Organic Carbon in the samples, and allowed an initial comparison of the data sets using various parameters. Examination of the proportions of soluble and insoluble organic matter allowed an assessment of the quantity of vegetal matter added to the bitumen to make the bituminous amalgam. The composition of the Ra's al‐Jinz material was studied using X‐Ray Diffraction analysis and thin‐section petrography, in order to assess the proportions of various minerals in the bituminous amalgams. It was concluded that the recipe for the bituminous mixture used to coat reed‐bundle and wooden boats did not differ significantly from that commonly used to make ‘mortar’ for architectural purposes in Mesopotamia. Traces of animal fats or fish oils were not found in the analysed Ra's al‐Jinz material, in contrast to previous hypotheses regarding the composition of the mixture. Comparison of the gross composition of extractable organic matter (the constituents of pure bitumen, soluble in chloroform or dichloromethane) showed the progressive effects of weathering on the samples. The isotopic composition of the bituminous material from H3 and the other sites was then compared to that of bitumen seeps and crude oils from Mesopotamia, Iran and Oman. The most significant result is that the material from As‐Sabiyah originated in Kuwait, at a surface seep at Burgan, while the material from Ra's al‐Jinz had a source in northern Mesopotamia.     

Faecal biomarker and archaeobotanical analyses of sediments from a public latrine shed new light on ruralisation in Sagalassos, Turkey

A public latrine in the ‘Imperial Baths’ of Sagalassos was transformed into a dump site in the early Byzantine period. Several layers of urban waste, including ceramics, bones, glass and perhaps excrements were deposited on the floor. Faecal biomarker analyses and archaeobotanical analyses were conducted to reconstruct the history of the room. 5β-stanols of human origin, such as coprostanol, were found in the sewage channels together with mineralised plant remains, indicating a human faecal context. The botanical remains are furthermore representative of the Roman diet of the Sagalassians. Soil layers, deposited on top of the latrine floor and dating to the early Byzantine period, contained herbivore derived 5β-stanols, such as 5β-stigmastanol and epi-5β-stigmastanol. Additionally, a clear predominance of epi-5β-stanols over 5β-stanols showed that the animal dung has been subject to composting. In this period, the former latrine was clearly used as a manure production site which is further confirmed by stratigraphic evidence of large amounts of urban waste artefacts, which were commonly collected together with manure before application on the fields. The results of the present study support the theory that off-site potsherd scattering can be used as a proxy for manuring events. Additionally, the data show key evidence for vertical migration of 5β-stanols and presumably also for the leaching of bile acids.     

A geochemical study of bituminous mixtures from Failaka and Umm an-Namel (Kuwait), from the Early Dilmun to the Early Islamic period

This paper is the last in a series presenting geochemical analyses of fragments of bituminous mixtures excavated from archaeological sites in Kuwait. The first was devoted to bituminous boat remains from the Ubaid‐related Neolithic site of H3, As‐Sabiyah, while the second dealt with bituminous amalgams from the Partho‐Sasanian site of ^cAkkaz, a former island now joined to the south side of Kuwait Bay. This, the third, refers to bitumen‐bearing samples from two other islands, Failaka and Umm an‐Namel, and covers a time span including the Early Dilmun period, the Kassite period and the Hellenistic to Early Islamic periods. The composition of the bituminous amalgams was studied in detail. The proportions of soluble and insoluble organic matter as well as vegetal organic matter were evaluated. Mineralogical composition by X‐Ray diffraction and thin‐section analysis was used to estimate the mineral input in the bituminous mixtures. It can be confirmed that the recipes used in the preparation of these bituminous amalgams comply with those traditionally used in antiquity, as seen at many sites in Mesopotamia and the Gulf. Analysis of the soluble organic matter, and especially its ‘‘saturates’’ fraction, provided sterane and terpane distributions and the measurement of diagnostic molecular ratios. These data, complemented by the isotopic composition of asphaltenes, allowed the identification of the sources of the bitumen, by calibration with numerous references from Iran and northern Iraq (oil seeps, bitumen from archaeological sites). It was established that the bitumen from Failaka and Umm an‐Namel was mainly imported from central Iraq (Hit‐Abu Jir) and northern Iraq (around Mosul). One sample of oil‐stained sand, dating to the Early Dilmun period, originated from Burgan and thus documents small‐scale imports from inland Kuwait. These results, and those of previous analyses, agree with the geopolitical context of the Early Dilmun, Kassite and Hellenistic periods, and the maritime trade routes that linked Mesopotamia to the settlements of the Gulf and beyond. The paper concludes with an overview of recent bitumen provenance analyses, and discerns chronological patterns in the distribution of Iraqi and Iranian bitumen in the Gulf and Indian Ocean, from the Neolithic to the Islamic periods.