Scanning electron microscope study of normal vertebrae and ribs from early medieval human skeletons

A method is described for the preparation of vertebral body and rib sections of archaeological context, for scanning electron microscopy (SEM). The specimens included in the present paper are macroscopically normal and are male and female in juvenile and adult age brackets. The changing directionality of trabeculae and the changing ratio of trabecular bone to cancellous space are noted in relation to the age at death.     

The Pyramids—Cement or Stone?

Several samples of pyramids from Giza were obtained. The samples were analysed by scanning electron microscopy, electron diffraction by X-rays, powder X-ray diffraction, inductively coupled plasmography, Fourier-transform infrared spectroscopy and other techniques. Some scientists who have recently studied the pyramids have suggested that the pyramids were poured into place, stone by stone. The prevailing theory among Egyptologists is, of course, that the pyramids were built from blocks of natural stone. All of the results obtained during this study directly support the concept that the pyramids are made of limestone and are not cementitious in nature.     

Avian egg-shell from archaeological sites

Avian egg-shell occurs fairly commonly on archaeological sites, particularly in alkaline deposits. It is rarely studied in detail. Egg-shell structure is described briefly below and features which may be of value for identification purposes are discussed. Egg-shells from 14 archaeological sites are tentatively identified as goose, domestic fowl, duck and guinea fowl. It seems likely that confident identification should ultimately be possible using a combination of features. This should yield information complementary to osteological evidence for the history of the utilization of birds and their eggs.     

The Evolution of the Vitruvian Recipes over 500 Years of Floor‐Making Techniques: The Case Studies of the Domus delle Bestie Ferite and the Domus di Tito Macro (Aquileia,Italy)

The paper reports the results of a research project aimed at the characterization of the floor bedding mortars of two Roman houses in Aquileia (north‐eastern Italy), the Domus delle Bestie Ferite and the Domus di Tito Macro. Seventy floor bedding mortars of the two domus were selected and almost half were fully minero‐petrographically characterized by means of optical microscopy operated in transmitted light (OM‐TL), X‐ray powder diffraction analyses coupled with quantitative phase analysis by means of the Rietveld method (XRPD‐QPA) and scanning electron microscopy with EDS microanalysis (SEM–EDS). The results indicate an evolution of the mortar preparation techniques over time in the mosaic of both houses. The materials are compared to the traditional Roman recipes for specific construction techniques.     

A technological study of ancient faience from Egypt

The chemical compositions and microstructures of some 35 faience objects from Egypt spanning the period from the Middle Kingdom through to the 22nd dynasty are determined using analytical scanning electron microscopy. Replicate faience beads glazed in the laboratory using the efflorescence and cementation methods are similarly investigated. In efflorescence glazing, there appears to be preferential efflorescence of soda over potash, and in cementation glazing, preferential take up of potash over soda into the glaze. These data are then used to try to infer the raw materials and methods of glazing employed in the production of the ancient faience. The glaze/glass phases present in the faience differ significantly in composition from that of New Kingdom glass. This could be due either to the use of different plant ashes or to changes in the composition of the plant ashes during the production of faience and/or glass. Although it is only rarely possible to determine with certainty whether ancient faience was glazed by efflorescence, cementation or application, the observed microstructures provide an indication of the approach adopted to achieve desired performance characteristics such as strength.     

Raspadita: a new lithic tool from the Isthmus of Rivas,Nicaragua

A new lithic tool type was discovered at the Pacific Nicaraguan archaeological site of Santa Isabel (AD 800–1350) and named raspadita (small scraper). Thousands of these small tools (1–2 cm in length) were found. They have a rounded proximal edge and a pointed distal end. In this study, the raspaditas are proved to be a coherent tool class with minimal variation in size, shape, material type and usewear. They were manufactured from white chert bladelet cores using soft hammer percussion and pressure flaking unifacial retouch. Usewear points to a composite tool form and a scraping function for the raspaditas. Scanning electron microscopy determined a ventral leading, dorsal following, unidirectional scraping motion for the raspadita proximal end. The material that was scraped has still to be definitely determined but phytoliths visible in the SEM images suggest that the composite tool was used for plant processing.     

The Carving Technology of the Handle‐Shaped Artefacts from Yinxu (c.1300–1046 bc) in China

The handle‐shaped artefact is a special jade object of the Three Dynasties (c.2000–200 bc ) period. The manufacturing technology and function of the handle‐shaped artefacts are widely questioned. In this paper, two handle‐shaped artefacts from Yinxu (c.1300–1046 bc ) are tested by digital microscope, Raman spectrometer and scanning electron microscope. The results indicate that the handle‐shaped artefacts might be made in four steps, namely rough shape cutting, edge reforming, handle making and single‐side polishing. It also suggests that the handle‐shaped artefacts might be used as sacrificial offerings, but not as hairpins or handles.     

Bone preservation in human remains from the Terme del Sarno at Pompeii using light microscopy and scanning electron microscopy

Archaeological bone can show marked and complex alterations depending on the environment in which it was buried. In this study, the state of preservation of 27 femurs recovered from the archaeological site of Pompeii was evaluated by light microscopy and scanning electron microscopy. Most of the bone samples, prepared by the grinding method, showed good histological preservation, although they were characterized by microfissures (microcracking). Nine bone samples showed different states of histological preservation, including worst preservation (two femurs), due to diagenetic processes. Cryostat bone sections stained with thionin or 4′,6′-diamidino-phenylindole (DAPI) revealed the persistence of DNA within some osteocyte lacunae. Scanning electron microscopy analysis showed that ultrastructural characters, such as lamellae and collagen fibres, are recognizable only in unaltered bone. Our results reveal that most Pompeian samples are well preserved since they have a bone microstructure virtually indistinguishable from that of fresh bone. In methodological terms, although each of the various morphological methods used contributes information, histological and histochemical analyses are the most informative for studying the preservation state of bone and allow for rapid essential screening of archaeological bone.     

Pigment analysis in Bronze Age Aegean and Eastern Mediterranean painted plaster by laser-induced breakdown spectroscopy (LIBS)

Laser-Induced Breakdown Spectroscopy (LIBS) was used in the examination of Bronze Age painted plaster samples from several sites in the Aegean and Eastern Mediterranean. The elemental content of paint materials was determined in most cases leading to the identification of the pigment used in agreement with data from analyses of the same samples with other established techniques. The analyses demonstrate that a virtually non-destructive technique such as LIBS provides sufficient data for the elemental characterisation of painting materials while in parallel has the capability for routine, rapid analysis of archaeological objects enabling the quick characterisation or screening of different types of artefacts. This certainly shows an important way forward in technological studies of fragile and scarce archaeological material.     

A new approach to recording and monitoring wet-preserved archaeological wood using three-dimensional laser scanning

The analysis and preservation of organic materials preserved within wetland environments represents one of the most costly parts of any post-excavation strategy. This paper outlines the application of high-resolution terrestrial laser scanning to one class of preserved material, worked archaeological wood. Scanning allowed the recording of the artefacts in three dimensions and the identification of features such as toolmarks. Features can be measured and volumetrically modelled within the digital environment, which may not always be possible for these often fragile materials using conventional techniques. Repeat scanning of the artefacts provided an opportunity to use comparative analysis software to investigate changes in the morphology of artefacts under contrasting conditions of short-term storage. The results suggest that immersion in water results in the least deterioration, whereas both freezing and air-drying caused distortion and degradation. This paper demonstrates that laser scanning provides a viable alternative post-excavation method for the recording, analysis and long-term ‘virtual archiving’ of organic archaeological materials, which may be more cost-effective in some instances than other methods of preservation.