U-series dating of soda straw stalactites from excavated deposits: method development and application to Blanche Cave, Naracoorte, South Australia

This study aimed to further test the method, reported by St Pierre et al. (2009), to develop robust chronologies of deposits in limestone caves through U/Th (Uranium/Thorium or U-Series) dating of soda straw stalactites. The chronology of fossil bearing deposits at Blanche Cave was further constrained with thermal ionisation mass spectrometry (TIMS) U/Th dating of 17 additional soda straw stalactite samples, and results were compared to recalibrated ¹⁴C ages of charcoal. The results support the assertion that soda straw stalactites can provide ages close to the time of sediment deposition and may be used as reliable chronological markers, particularly for periods reaching or beyond the radiocarbon dating limit. The application of an enhanced cleaning technique facilitated the reduction of detrital Th in samples, significantly increasing age accuracy and precision. Additionally U/Th age accuracy and precision was increased through the application of site-specific measured U/Th ratios to correct for the detrital ²³⁰Th component in samples.     

Expanding the utility of Uranium-series dating of speleothems for archaeological and palaeontological applications

Uranium-series (U-series) dating of speleothems is frequently used for palaeoclimate studies but its archaeological and palaeontological applications are limited to stratigraphically significant speleothem formations, such as flowstones, to provide maximum and minimum temporal points. This study targeted soda straw stalactites for U-series dating. In contrast to other speleothem formations, soda straw stalactites are fragile, have typically short life spans (usually only years but rarely up to a few hundred years) and are frequently incorporated into cave deposits. Results of thermal ionisation mass spectrometry (TIMS) U-series dating of soda straw stalactites from palaeontological excavations at Blanche Cave, South Australia, show that small, dense, clean straws tend to yield ages closest to the time of stratigraphic deposition. A correlation between soda straw U-series ages and radiocarbon ages of charcoal from the site is shown. Multiple soda straw age determinations for a single stratigraphic unit are required in order to verify age concordance. In conjunction with other dating methods, U-series dating of soda straw stalactites may help to significantly constrain the age of stratigraphic units and associated archaeological and palaeontological deposits in order to provide more robust chronologies. Here we advocate the collection of soda straw stalactites at future excavations of limestone cave sites.     

The influence of climatic change on the Late Bronze Age Collapse and the Greek Dark Ages

Between the 13th and 11th centuries BCE, most Greek Bronze Age Palatial centers were destroyed and/or abandoned. The following centuries were typified by low population levels. Data from oxygen-isotope speleothems, stable carbon isotopes, alkenone-derived sea surface temperatures, and changes in warm-species dinocysts and formanifera in the Mediterranean indicate that the Early Iron Age was more arid than the preceding Bronze Age. A sharp increase in Northern Hemisphere temperatures preceded the collapse of Palatial centers, a sharp decrease occurred during their abandonment. Mediterranean Sea surface temperatures cooled rapidly during the Late Bronze Age, limiting freshwater flux into the atmosphere and thus reducing precipitation over land. These climatic changes could have affected Palatial centers that were dependent upon high levels of agricultural productivity. Declines in agricultural production would have made higher-density populations in Palatial centers unsustainable. The ‘Greek Dark Ages’ that followed occurred during prolonged arid conditions that lasted until the Roman Warm Period.