NEW ARCHAEOMAGNETIC STUDIES NEAR XI'AN,CHINA*

Archaeomagnetic and mineral magnetic studies were made of known-age samples from fired structures and sediments from archaeological sites near Xi'an, China. The fired materials retained a stable record of the direction of the past geomagnetic field, which compared well with previous investigations and could contribute to an archaeomagnetic calibration curve. However, discrepancies with documented observations of the field were noted.     

The Application of Steroidal Biomarkers to Track the Abandonment of a Roman Wastewater Course at the Agora (Athens,Greece)*

A subterranean, stone‐built, sediment‐filled culvert discovered during excavations at the Agora (Athens, Greece) was dated to the Roman period on the basis of its characteristic construction and associated finds, including coins. The location of the culvert relative to other adjacent watercourses and an ancient river bed suggested that the structure was a sewer. This was confirmed through a multi‐molecular biomarker approach based on analysis of the bile acids associated with sediment filling the sewer, using gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS). The acid fraction contained predominantly deoxycholic and lithocholic acids, while the neutral steroid fraction comprised a complex mixture of Δ⁵ sterol and 5β‐ and 5α‐stanols, dominated by coprostanol, suggesting the presence of faecal matter of predominantly human origin. The concentrations of neutral and acidic faecal biomarkers were observed to vary in tandem, with the highest concentrations being found in the sediment at the base of the fill in the culvert. A reduction in concentration occurred with decreasing depth of the fill, with concentrations in the uppermost samples being little different from control samples of sediment taken beyond the confines of the culvert. The enhanced concentration of bile acids relative to 5β‐stanols compared with fresh human faeces must reflect the enhanced diagenetic stability of the former, thereby making bile acids the possibly preferred biomarker for this type of study. The quantitative data obtained suggest that the culvert fell rapidly out of use, possibly coinciding with the Slavic incursion in AD 582–3.     

Identifying Chemical Activity Residues on Prehistoric House Floors: A Methodology And Rationale For Multi‐Elemental Characterization of a Mild Acid Extract of Anthropogenic Sediments

Archaeologists have employed sediment chemistry in site prospection for nearly a century. For example, phosphorus is a good indicator of human occupation, because it is a generic indicator of human activity. Recently, multi‐element studies of sediments have successfully identified specific activity areas by analysing other elements in addition to phosphorus. To reach its full potential, however, sediment chemistry must be undertaken with an understanding of how these residues are formed and of the chemical indicators that can be used to identify specific activities. Methodologies that optimize the extraction of specific residues must be employed. Not to do so is a naïve application of the technique.     

CHARACTERIZING THE MICROMORPHOLOGY OF SEDIMENTS ASSOCIATED WITH CHINCHORRO MUMMIFICATION IN ARICA,CHILE USING SEM AND EDS

We use scanning electron microscopy (SEM) and energy‐dispersive spectroscopy (EDS) to analyse clay sediments used during the mummification process of Chinchorro mummies from northern Chile. The significance of this study is that no prior work has characterized the sediment used by the Chinchorro during mortuary preparation and this approach offers a necessary preliminary step towards identifying modern equivalents for the materials used by the Chinchorro. Understanding the unique characteristics of this material may also help understand why they are so well preserved and aid in the future curation of Chinchorro mummies.     

ARCHAEOLOGICAL AND CHEMICAL RESEARCH ON SEDIMENTS AND CERAMICS AT POLIDEPORTIVO (SPAIN): AN INTEGRATED APPROACH*

This paper proposes a preliminary approach to the integration of archaeological evidence and various chemical analyses (phosphorus and lipid) on sediments and ceramics. Phosphorus and organic matter analyses are, thus, used for the study of sediments, and lipid analyses for pottery from structure 19 of the Late Neolithic—Early Copper site known as ‘Polideportivo’, Martos, southern Spain. The results of both types of analysis point to a predominantly domestic function for this structure.     

Reconnaissance of the Hannibalic Route in the Upper Po Valley,Italy: Correlation with Biostratigraphic Historical Archaeological Evidence in the Upper Guil Valley,France

Controversy over the alpine route taken by the Hannibalic Army from the Rhône Basin into Italia in 218 bc (2168 cal bp ) has raged amongst classicists for over two millennia. Because Hannibal crossed the Alps, the significance for identifying the route taken by the Punic Army lies more in its potential for identifying sites of historical archaeological significance than a resolution of one of history's most enduring questions. While compelling stratigraphic, geochemical and microbiological evidence has been recovered from an alluvial floodplain mire in the upper Guil Valley, located below the Col de la Traversette (about 3000 masl) on the French–Italian border, it potentially identifies the invasion route as the one originally proposed by Sir Gavin de Beer in 1974. The dated layers in several sections, termed the MAD (mass animal deposition) beds based on disrupted/churned bedding and key/specialized biological components strongly supports de Beer's thesis that Hannibal chose the highest transit col into Italia. In addition to other physical evidence, we present here new physical, geomorphological and stratigraphic evidence, all calibrated by radiocarbon dating, that suggests Hannibal's imprint on the landscape exists in coalescing alluvial fans in the upper Po catchment of northern Italy.