NEUTRON ACTIVATION ANALYSIS OF AD 1660–1930 EUROPEAN COPPER-COLOURED BLUE GLASS TRADE BEADS FROM ONTARIO,CANADA

Blue glass trade beads from well-dated late seventeenth- to early twentieth-century sites and collections have been analysed non-destructively by instrumental neutron activation analysis. The beads display enough variations in their elemental contents to allow us to characterize the different chemistries. The implication of these results is that similar chemical analyses of blue beads from undated archaeological sites may be used to help date the sites, since each bead chemistry has a specific earliest period.     

PETROGRAPHIC AND STABLE ISOTOPE ANALYSES OF LATE CLASSIC ULÚA MARBLE VASES AND POTENTIAL SOURCES*

Ulúa marble vases from the Ulúa Valley of northwestern Honduras are a hallmark luxury good from Late Classic (ad 600–900) Mesoamerica. Archaeological and stylistic data point to centralized production at one site, Travesía. This paper analyses stable isotope and petrographic data from the vases and three potential procurement areas. The results indicate that the vases were produced from one primary source with one, potentially two, secondary sources. Procurement patterns most probably corresponded to contemporary communication routes. The results clearly indicate that a multi‐method approach is necessary for sourcing marble from Honduras.     

MULTIVARIATE ANALYSIS OF THE ENERGY DISPERSIVE X-RAY FLUORESCENCE RESULTS FROM BLUE AND WHITE CHINESE PORCELAINS*

The energy dispersive X-ray fluorescence technique was employed to study non-destructively the surface of 66 samples of Chinese porcelain, of different periods and origins, and determine the contents of 13 chemical elements, namely, Ti, Mn, Fe, Co, Ni, Cu, Zn, Ga, Pb, Rb, Sr, Y and Zr. Principal components analysis was performed on these 13 variables, and scatter plots, incorporating the first, second and third principal components, used to study the clustering behaviour of the data. Based on these results, discriminant analysis was then performed on the data, and discriminant functions established for attributing the period and origin of the porcelains.     

THE OCCURRENCE OF PALYGORSKITE IN THE YUCATÁN PENINSULA: ETHNO‐HISTORIC AND ARCHAEOLOGICAL CONTEXTS*

Palygorskite is a rare clay mineral used by the ancient Mayas for fabricating the Maya blue pigment and for other purposes. It seems to have been obtained from a restricted area in the Yucatán peninsula where important archaeological sites are found. Geological samples from different localities in this area show a high content in palygorskite, indicating that this clay is widespread in Yucatán. Combining structural, morphological, compositional and geochemical methods, we analysed the common characteristics of Yucatecan palygorskites, and compared them with palygorskites from other origins around the world. These results can be used for defining a fingerprint of Yucatecan palygorskite to be used in provenance studies of archaeological artefacts, in particular the Maya blue pigment.     

EVIDENCE FOR THE USE OF EGYPTIAN BLUE IN AN 11TH CENTURY MURAL ALTARPIECE BY SEM–EDS,FTIR AND SR XRD (CHURCH OF SANT PERE,TERRASSA, SPAIN)

The present study shows the analysis performed on pigment samples taken from Sant Pere (Terrassa, Catalonia, Spain), a remarkable church built in the Romanesque style. On the basis of the results obtained from the analysis, an interesting discussion arises after finding evidence of Egyptian blue in one of the samples, a discovery that was not expected due to the time period of the samples. The pigments were identified by the combined use of FTIR and SEM with an EDS facility. For the blue pigment, since the EDS and FTIR analyses suggested the possible presence of cuprorivaite, micro‐XRD experiments using synchrotron radiation were run.     

NEUTRON ACTIVATION ANALYSIS OF SIXTEENTH- AND SEVENTEENTH-CENTURY EUROPEAN BLUE GLASS TRADE BEADS FROM THE EASTERN GREAT LAKES AREA OF NORTH AMERICA*

Sixteenth- and seventeenth-century European blue glass trade beads from aboriginal sites in the eastern Great Lakes area of North America have been analysed non-destructively using low neutron dose instrumental neutron activation analysis, so that the beads could be returned to their keepers. Dark blue (cobalt-coloured) beads are readily separable from turquoise (copper-coloured) beads. Differences in the chemistries of the turquoise blue beads appear to be useful in separating glass beads from the two centuries. Low calcium, sixteenth-century turquoise beads tend to distintegrate by a leaching of the alkali metals.     

ISSUES RELATED TO DETERMINING BURIAL CHRONOLOGY BY FLUORIDE ANALYSIS OF BONE FROM THE MAYA ARCHAEOLOGICAL SITE OF CHAU HIIX,BELIZE*

Fluoride percentage of bone is often used to determine relative dates of burials in archaeological contexts. An analysis of prehistoric Maya burials at Chau Hiix, Belize, identifies taphonomic factors, including soil composition, grave depth, soil disturbance, age at death and cortical bone thickness, that cause variations in the rate of fluoride absorption by altering the access of water to bone. This example demonstrates that fluoride dating is unlikely to be useful at most prehistoric Maya sites because of the inconsistent taphonomy due to typically diverse mortuary practices, and it also serves as a cautionary tale for applications of this methodology in other contexts.     

A SPECTROSCOPIC INVESTIGATION OF PIGMENT AND CERAMIC SAMPLES FROM COPÁN,HONDURAS*

A combination of micro‐Raman spectroscopy, micro‐infrared spectroscopy and SEM–EDX was employed to characterize decorative pigments on Classic Maya ceramics from Copán, Honduras. Variation in red paint mixtures was correlated with changing ceramic types and improvements in process and firing techniques. We have confirmed the use of specular hematite on Coner ceramics by the difference in intensities of Raman bands. Different compositions of brown paint were correlated with imported and local wares. The carbon‐iron composition of the ceramic type, Surlo Brown, was confirmed. By combining micro‐Raman analysis with micro‐ATR infrared and SEM–EDX, we have achieved a more comprehensive characterization of the paint mixtures. These spectroscopic techniques can be used non‐destructively on raw samples as a rapid confirmation of ceramic type.     

A Taphonomic Approach to Late Classic Maya Mortuary Practices at Xuenkal,Yucatán,Mexico

Abstract

Following a brief introduction to mortuary practices in Prehispanic Maya society, we outline the analytical procedures followed during the excavation and laboratory investigation of five burial assemblages from the Late Classic period site of Xuenkal, Yucatán, Mexico. A detailed account of a sequence of primary and secondary interments is provided with a focus on taphonomic and biovital information, emphasizing the importance of an interdisciplinary approach, especially human taphonomy, for the reconstruction of complex Maya mortuary treatments. Our results show that bodies of the dead or their parts followed surprisingly long and complex funerary paths.     

Evidence for Maya Household Subsistence and Domestic Activities: Use-Wear Analysis of the Chipped Chert Assemblage from Pook’s Hill,Belize

Abstract

From 1999–2005, the Belize Valley Archaeological Reconnaissance Project excavated Pook’s Hill (PKH-1), a single plazuela group located in the Roaring Creek Valley, Cayo District, Belize. Artifacts recovered at Pook’s Hill date predominantly to the Late and Terminal Classic (A.D. 700–950) and can be stratigraphically segregated into two distinct occupation phases, namely a Late Classic (A.D. 700–830) and a Terminal Classic-Early Postclassic (A.D. 830–9507+) phase. The chipped chert and chalcedony tools from the two phases were included in a combined program of low- and high-power use-wear analysis to reconstruct aspects of the socioeconomy. The results of the analyses reveal that the site’s inhabitants produced and used both formal and informal tools for a wide variety of subsistence and domestic tasks, and for the production of some utilitarian items. Stone tool use-wear evidence and the recovery of small quantities of other artifacts suggest that the Maya from Pook’s Hill produced more valuable objects of bone, stone, and shell, although it is difficult to accurately identify craft-production activities at the site from the context of recovery. Despite some variation in the specific activities undertaken with the chipped stone tools over time, the organization of lithic technology at Pook’s Hill did not change significantly from the Late Classic into the Early Postclassic period.