Non‐Destructive Survey of Early Roman Copper‐Alloy Brooches using Portable X‐ray Fluorescence Spectrometry

This paper argues that portable X‐ray fluorescence spectrometry (pXRF) is a suitable elemental measurement technique to study the production of copper‐alloy artefacts. However, rather than try to imitate the accuracy and precision of laboratory techniques, it is more beneficial to deploy it in a survey role, one that attempts to model chronological and geographical changes within large quantities of artefacts. To achieve this, it was investigated to what extent corrosion and the issues surrounding surface measurements affect the potential of this type of research. Analyses on early Roman period brooches gathered in the Nijmegen region of the Netherlands were subsequently compared with published data.     

Degradation processes in colourless Roman glass: cases from the Bocholtz burial

A group of Roman glass objects from the Bocholtz burial in the SW of Limburg (The Netherlands) was found to have been subject to varying degrees of degradation. Many of the 25 colourless glass objects were fragmented to pieces <0.1 cm (“sugared”), whereas the three transparent blue-green glass objects were in near-pristine state. Analyses using SEM, XRF and EDS revealed that the fragmentation was the direct result of the intense leaching of Na₂O from the glass structure and its replacement with water. The resulting gel layers with low-Na₂O contents and large amounts of water are sensitive to cracking when they dry out. Thin-walled glass appears to be less sensitive to cracking from the resulting stress than thick-walled glass. Local differences in the moisture regime during burial also influence the severity of the glass degradation. Glass with low concentrations of CaO seems to be the most sensitive to this form of degradation. The typical blue-green Roman glass is less sensitive as it generally has considerably higher concentrations of CaO.     

Effects of site lithology on geochemical signatures of human occupation in archaeological house plans in the Netherlands

This study presents the application of multi-element soil analyses (X-ray fluorescence spectroscopy and inductively coupled plasma optical emission spectroscopy of 1 M HCl extracts) to grid samples from 3 archaeological house plans embedded in sandy clays, clays and sands to assess effects of site lithology on geochemical signatures of human occupation.     

Fuel, Fire and Heat: an experimental approach to highlight the potential of studying ash and char remains from archaeological contexts

As in traditional societies today ancient societies probably selected different fuels to meet specific heat requirements. Char and ash, the end products of fire, are often found in abundance in archaeological contexts. These end products can provide information regarding (i) the original fuel resource and type, (ii) the characteristics of the fire and (iii) combined with other archaeological evidence shed further light on possible socio-economic activity(-ies) associated with that fire. The three main fuel resources would have been (i) modern vegetation, (ii) fossil fuel and (iii) animal by-products. Local availability and abundance would have influenced the choice made.In this study an experimental approach was adopted to try and distinguish between the three different fuel resources that are known to have been used by ancient societies (and continue to be used by traditional societies today) from their char and ash remains to help determine original fuel-type and understand the relative heating properties. For this end one fuel-type from each fuel resource listed above, namely wood, peat and cow dung, was chosen.     

Tools for Predicting Damage to Archaeological Sites Caused by One-Dimensional Loading

Tools are developed to predict damage to archaeological remains caused by the construction of line infrastructure on soft soil. They are based on numerical modelling and laboratory testing supported by X-ray microcomputed tomographic observations, and micromorphological analyses of thin sections. They have been validated for one-dimensional (1D) loading at two sites in the Netherlands where soil has been placed on top of organic layers rich in ecofacts and overlaying Pleistocene sands.

Numerical prediction of the deformation of soft layers underneath an embankment remains a challenge for geo-technical engineers. Errors on surface settlement prediction reach ±15% of the measured total settlement.

Laboratory observations show that vulnerable artefacts can get crushed when packed loosely in pure assemblies under 1D loading equivalent to less than 5 m of sand. Fragmentation is assimilated to loss of archaeological value as it compromises recovery during sieving. Embedment in a sandy or a very compressible organic matrix has a beneficial effect on the resistance of ecofacts. Embedded ecofacts can resist a load of more than 12 m of sand. Flattening and re-orientation of soft plant remains occur during 1D loading without microscopic damage of tissues.     

Under Pressure: A Laboratory Investigation into the Effects of Mechanical Loading on Charred Organic Matter in Archaeological Sites

The present publication investigates what happens to archaeological sites when they are built over. Focus is put on the degradation of charred organic materials by static loading. It is assumed that materials lose archaeological value if their fragments become too small to be recovered, or too distorted to be classified at species level. Several charred ecofacts of a few millimetres in size (wood fragments, hazelnut shells, and seeds) have been selected and subjected to individual particle strength tests. Assemblages of these particles have also been compressed one-dimensionally and scanned at several stages of testing using laboratory based X-ray microtomography. Microscopic damage by splitting or crushing is found to be limited at the macroscopic yield stress. It initiated at stresses less than 80 kPa for the weakest assemblages, and in all cases at stresses below 320 kPa. (80 kPa represents the load of a 6 m high sand embankment on soft soil that has half-settled underneath the groundwater table, while 320 kPa corresponds to stresses applied beneath the pile foundation level of high-rise buildings.) Sand seeded with charred particles has also been tested to illustrate the beneficial effect of embedment of charred particles in sand during static one dimensional loading.     

Between the Piles. Studying Excavation Photographs to Determine the Area of Physical Disturbance Caused by Piling in the Netherlands

Excavation photographs that show piles can be used to determine and measure the area of disturbance around piles. Until now, this has only been done at a small scale and with ideal examples. The present study shows that less ideal photographs can also be used to determine the disturbance around piles, at a much larger scale. Using predefined methods of documentation and registration, data can be collected about the disturbance of different types of piles, with varied piling techniques, in various burial environments and archaeological contexts. This data will be used in the second phase of the research to determine the loss of archaeological information due to piling.     

Erosion and Errors: Testing the Use of Repeated LIDAR Analyses and Erosion Modelling for the Assessment and Prediction of Erosion of Archaeological Sites?

Slope soil erosion is one of the main threats to archaeological sites. Several methods were applied to establish the erosion rates at archaeological sites. Digital elevation models (DEMs) from three different dates were used. We compared the elevations from these three models to estimate erosion. We also applied the landscape evolution model LAPSUS with the available DEMs as basis. Spatial processing errors and effects of tillage and harvesting practices explain most of the DEM elevation differences between the recordings. Increased DEM resolution does not result in more precise or reliable erosion. The present technological level of landscape evolution modelling makes it possible to indicate areas most vulnerable to soil displacement by surface runoff erosion and tillage. Future research, using sediment and surface dating techniques such as deposit of radionuclides, heavy metals and OSL dating will provide a more accurate estimation of erosion rates and the subsequent impact on archaeological sites.     

Relax,Don’t Do It: A Future for Archaeological Monitoring

Preservation in situ and the monitoring of archaeological sites have become important themes since the acceptance and implementation of the Valletta Treaty. In the last few decades, our knowledge of degradation processes has increased manyfold, and a range of techniques have been tested and applied for use in both assessment and monitoring. Despite these successes, all is not well. First, we have little notion of the speed of the decay processes involved. This makes it difficult to distinguish between acute and protracted degradation. Apart from that, many assessments and subsequent monitoring projects rely (too?) heavily on complex and costly specialist technology. For any future preservation — in situ — projects low-tech observations together with best estimates of decay rates and archaeological site information should be combined to make an accurate assessment of the effects of decay on the archaeological record. Monitoring for preservation purposes is only appropriate if (1) decay processes occur within a relevant and measurable time scale, and (2) if mitigating actions can be taken or preservation ex situ can be performed (i.e. a rescue excavation) if significant degradation takes place.