木材中挥发性有机酸的SPMEGC/MS分析研究

采用木材制作的藏展空间,木材释放出的挥发性有机酸,在一定的温湿度条件下,会对文物造成不良的影响,因此需要建立一套对木材挥发性有机酸测定的方法.为此,采用固相微萃取(SPME)样品预处理技术,分离富集木材中的挥发性有机物,结合气相色谱-质谱(GC/MS)联用技术对木材中挥发性有机酸进行半定量分析,研究了9种木材中挥发性有机酸的挥发量和分布规律.结果表明,不同木材有机酸的挥发量差别较大.实验结果可为博物馆在装修和储藏中对材料的筛选提供科学依据.     

博物馆藏展材料评估筛选的薄膜试片测试法

为改善Oddy测试法实验周期长,依靠目测判断腐蚀程度的状况研究建立了一种薄膜试片测试法,研发薄膜试片、设计成套测试容器与夹具、改变测试条件并结合数码采集腐蚀图像和对腐蚀图像数字化分析等简化藏展材料评估筛选实验操作、缩短测试时间和提高结果分级判别能力.另外,固相微萃取和气质联用仪(SPME-GC/MS)被用于表征藏展材料在挥发和降解过程中所释放的污染物成分,佐证其对银、铜和铅金属文物的潜在危害.新建薄膜试片测试法表明,14d的测试周期不仅大大缩短了测试时间,简化了操作,而且薄膜试片的使用也有利于克服人为分级的主观判断性,为数字化分级打下坚实基础.     

无酸纸的发展及其在文物保护中的应用

无酸纸是很重要的一种馆藏文物保护载体.本文对无酸纸的发展现状及在文物保护中的应用进行了总结.同时指出,根据我国文物保护的需要,研制文物保护专用无酸纸并建立相关的评价标准是无酸纸的发展趋势.     

博物馆文物环境用甲醛净化材料评价方法研究

博物馆文物环境因装饰材料所致甲醛污染以及由此产生对文物危害问题已被普遍关注.为了评价净化材料实际使用中对污染物去除净化能力,搭建了静态试验舱,建立了该环境中甲醛的定量分析方法.研究了甲醛溶液法和人造板散发法两种产生甲醛气体的方法,以及吸附材料不同加入方法等对净化材料评价结果的影响,研究试验舱内甲醛浓度随时间的变化规律,建立了净化材料脱附量检测方法,分别测定了活性炭和三种壳聚糖基净化材料的净化效果.结果表明,用人造板散发法产生甲醛气体方法能用于甲醛净化材料的评价,得到净化率指标反映了净化材料在实际文物环境中的应用效果,脱附量指标能直观比对和反映净化材料对污染物的吸附稳定性.     

Construction of a quartz OSL standardised growth curve (SGC) for aeolian samples from the Horqin dunefield in northeastern China

It has been suggested that the standardised growth curve (SGC) method can be used to de-terminate D_e accurately and reduce the measurement time. However, different opinions regarding the applicability of the SGC method exist. In this paper, we report the construction of quartz OSL SGC for 35 aeolian samples from different parts of the Horqin dunefield in northeastern China, and then test their applicability for D_e determination. Our results suggest that: 1) up to a regeneration dose of 80 Gy, the SGC of the Horqin dunefield can be fitted using the exponential plus linear equation, with the r² value of 0.97, and all the regeneration dose points closely stick to the fitting line, implying that all samples share a very similar dose-response curve; 2) for samples with Des ranging from 1 to 50 Gy, the ratios of SAR D_e to SGC D_e fall within the range of 0.9–1.1, and the average ratio of SAR D_e to SGC D_e is 1.01±0.01, close to unity. Therefore, the construction of SGC is correct, and the SGC is an effective procedure for accurate D_e determination for samples from the study area.     

Testing the standardized growth curve (SGC) to OSL dating coastal sediments from the south Bohai Sea, China

It has been suggested that the standardized growth curve (SGC) method can be used to accurately determinate equivalent dose (D_e) and reduce measurement time. However, different opinions regarding the applicability of the SGC method exist. In this paper, we evaluated quartz OSL SGCs of marine and coastal sediments of different grain sizes and different cores in the south Bohai Sea in China, and tested their applicability to the determination of D_e values. Our results suggested as follows: (1) The SGC method is applicable to both multiple- and single-aliquot regenerative-dose (MAR and SAR) protocols of OSL dating and efficiently provides reliable estimates of D_e. (2) Finesand quartz of different palaeodoses showed highly similar dose-response curves and an SGC was developed, but old samples using the SGC method have large uncertainties. (3) For coarse-silt quartz, two different types of dose-response curves were recorded: low-dose (≤60Gy) and high-dose (≥100Gy). The growth curves of low-dose quartz were similar to each other, facilitating the use of SGC in D_e estimations, but errors tended to be larger than those obtained in the SAR method. For high-dose (100–300Gy) quartz, the SGC was also found to be reliable, but there was large uncertainty in D_e (>300Gy) estimation. We suggest that SGC could be employed for the dating of marine and coastal sediments dating using either MAR or SAR OSL protocol and either fine-silt, coarse-silt or fine-sand quartz.     

Technological Maturity and Development without Research: The Challenge for Malaysian Manufacturing

Propelled largely by direct investment via multinationals, Malaysia’s manufacturing sector has grown rapidly and is changing its output‐mix. In 1992, the share of high‐tech products in Malaysian manufacturing exceeded that of Japan, Korea or Taiwan. However, this ‘maturity’ was acquired without a strong research base. This article provides a framework which looks at the role of research and development (R&D) in conferring technological maturity and assesses the progress Malaysian manufacturing has made in this regard. The authors find that while multinationals have transferred many aspects of production, they have been slow in transferring R&D expertise. Neither has indigenous innovation filled this gap. Consequently, the long‐term sustainability of the industrial transformation process in Malaysia is in jeopardy. The article concludes with suggestions for corrective policies.     

Publications briefly noted

China

ANGELA ZITO. Of Body and Brush: grand Sacrifice as Text/Performance in Eighteenth‐Century China. Chicago: University of Chicago Press, 1998. xix, 311 pp. US$17.95, paper.

JAMES D. SEYMOUR and RICHARD ANDERSON. New Ghosts Old Ghosts: prisons and Labor Reform Camps in China. Armonk: M. E. Sharpe, 1998. xvii, 313 pp. Bibliography, tables, charts, maps, index. No price given, hardcover.

ANDREW NATHAN. China's Transition. New York: Columbia University Press, 1998. xiv, 313 pp. US$27.50, paper.

Y. M. YEUNG and DAVID K. Y. CHU (eds). Guangdong: survey of a Province Undergoing Rapid Change, 2nd ed. Hong Kong: Chinese University Press, 1998. xviii, 536 pp. HK$310.00, hardcover.

Japan and Korea

STEVEN D. CARTER (ed & trans). Unforgotten Dreams: poems by the Zen Monk Shotetsu. New York: Columbia University Press, 1997. xxx, 232 pp. US$19.00, paper.

LAURA HEIN and MARK SELDEN (eds). Living with the Bomb: American and Japanese Cultural Conflicts in the Nuclear Age. Armonk: M. E. Sharpe, 1997. 300 pp. US$19.95, paper.

ROY STARRS. An Artless Art: the Zen Aesthetic of Shiga Naoya. Surrey: Curzon Press, 1998. 261 pp. US$47.00, hardcover.

VICTOR ARGY and LESLIE STEIN. The Japanese Economy. London: Macmillan, 1997. 379 pp. £47.50, hardcover; £17.50, paper.

MARISAKO and HIROKI SATO (eds). Japanese Labour and Management in Transition: diversity, Flexibility and Participation. London: Routledge, 1997. 344 pp. £50.00, hardcover; £14.99, paper.

KEVIN WATKINS. Economic Growth with Equity: lessons from East Asia. Oxford: Oxfam, 1998. 160 pp. £6.95, paper.

South Asia

S. W. R. DE A. SAMARASINGHE and VIDYAMALI SAMARASINGHE. Historical Dictionary of Sri Lanka (Asian/Oceanian Historical Dictionaries, no. 26) Lanham, Md. and London: Scarecrow Press, 1998. xliii, 214 pp. Chronology, appendices, bibliography. US$38.50, hardcover.

Southeast Asia

HERMAN C. KEMP. Bibliographies on Southeast Asia. Leiden: KITLV Press, 1998. Bibliographical Series no 22. xix, 1128 pp. NLG 175, paper.

DAVID LEE (ed). Documents on Australian Foreign Policy 1937–49, volume XV: Indonesia 1949. Canberra: Department of Foreign Affairs and Trade, 1998. xxv, 675 pp. A$57.50, hardcover; $37.50, paper.

J. TH. LINDBLAD (ed). Historical Foundations of a National Economy in Indonesia, 1890s‐1990s. Amsterdam: Koninklijke Nederlandse Academie van Wetenschappen, 1996 (Verhandelingen, Afd. Letterkunde, Nieuwe Reeks, deel 167). viii, 427 pp. NLG 95, paper.

MANUEL F. MONTES. The Currency Crisis in Southeast Asia. Singapore: Institute of Southeast Asian Studies, third reprint (updated), 1998. xxxvii, 88 pp. US$24.00, hardcover; US$17.90, paper.

DANG PHONG and MELANIE BERESFORD. Authority Relations and Economic Decision‐making in Vietnam: an Historical Perspective. Copenhagen: Nordic Institute of Asian Studies, 1998. 117 pp. £30.00.

BOB REECE. Masa Jepun: Sarawak under the Japanese 1941–1945. N.p.: Sarawak Literary Society, n.d. xix, 254 pp. No price given, hardcover.

D. S. RANJIT SINGH and JATSWAN S. SIDHU. Historical Dictionary of Brunei Darussalam. Lanham, MD and London: Scarecrow Press, 1997. xliv, 179 pp. Asian/ Oceanian Historical Dictionaries no. 25. 9 maps. US$64.00, hardcover.

C. VAN DIJK and J. LEEMBURG‐DEN HOLLANDER. European Directory of South‐East Asian Studies, x, 618 pp. NLG 40.

JORGE MANUEL DOS SANTOS ALVES. O Dominio do Norte de Sumatra. A historia dos sultanatos de Samudera‐Pacem e de Achem e das suas relacoes com os Portugueses (1500–1580) . Lisbon: Sociedade Historica da Independencia de Portugal, 1999.

General Asia

TON OTTO and AD BORSBOOM (eds). Cultural Dynamics of Religious Change in Oceania. Verhandelingen 176. Leiden: KITLV Press, 1997. viii, 144 pp. NLG 40, paper.

RONG‐I WU and YUN‐PENG CHU (eds). Business, Markets and Government in the Asia Pacific: competition Policy, Convergence and Pluralism. London: Routledge, 1998. x, 348 pp. Bibliography, figures, tables, index. £19.99, paper.

DARRELL Y. HAMAMOTO and RODOLFO D. TORRES (ed). New American Destinies: a Reader in Contemporary Asian and Latino Immigration. London: Routledge, 1997. 350 pp. £16.99, paper.

RUTH HAYHOE and JULIA PAN (eds). East‐West Dialogue in Knowledge and Higher Education. Armonk: M. E. Sharpe, 1996. xvii, 316 pp. US$72.95, hardcover.

EVA‐MARIE KROLLER, ALLAN SMITH, JOSUA MOSTOW, ROBERT KRAMER (eds). Pacific Encounters: the Production of Self and Others. Vancouver: Institute of Asian Research, 1997. 217 pp. CAN$19.95, paper.

INSTITUTE OF ASIAN RESEARCH, UNIVERSITY OF BRITISH COLUMBIA. The Empowerment of Asia: reshaping Global Society. Vancouver: The Institute, University of British Columbia, c. 1998. 137 pp. CAN$10.00, paper.

ROBERT ALDRICH and JOHN CONNELL. The Last Colonies. Cambridge, UK: Cambridge University Press, 1998. xiv, 335 pp. A$59.95, hardcover.

R. F. WAITERS and T. G. McGEE, with GINNY SULLIVAN (eds). Asia‐Pacific: new Geographies of the Pacific Rim. Bathurst, NSW: Crawford House Publishing, 1997. xxi, 362 pp. No price given, paper.

HAIDER A. KHAN. Technology, Development and Democracy: limits of National Innovation Systems in the Age of Postmodernism. Cheltenham, UK: Edward Elgar, 1998. x, 198 pp. £49.95, hardcover.