Snail assemblages: interrogating an environmental controversy involving Powelliphanta augusta and the mining industry in Aotearoa New Zealand

In 2004, a controversy arose in Aotearoa New Zealand's coal mining sector that involved Powelliphanta augusta, a species of land snail. This paper considers that controversy in terms of emergent assemblages involving the snail, the mining industry, the Department of Conservation, political action by environmental non‐government organisations, and public expressions of environmental and other values. Three sets of relations embedded in those assemblages are examined—those related to positioning and organising nature; values, politics, and power relations; and human and non‐human materialities. Those relations illuminate how a protracted controversy and its objects form a “social test bed” for contested views in legislation and guidelines dealing with economy, conservation, and restoration. To assess the dynamics, complexities, and contingencies of such relations, attention is paid to the controversy's detailed time line and legal framing, as well as to ontological shifts of snail and habitat and snail metrics. This analytical focus highlights the shifting quality of ideas about how the snail and its habitat are understood as entangled in fraught and mutating strategies of translocation that are played out in a particular regulatory setting. It also provides insights into international geographical efforts to re‐shape environmental governance and management.     

Carbon and nitrogen isotope signals in eel bone collagen from Mesolithic and Neolithic sites in northern Europe

Carbon and nitrogen isotope analysis was undertaken on collagen extracted from eel bone from six Mesolithic and Neolithic sites in northern Europe. The results were compared with data obtained on other archaeological fish remains and modern eel caught in fresh and brackish water and from the sea. The possibility of discriminating between freshwater, brackish and marine signals in archaeological eel bone is evaluated and the implications for archaeology discussed. Our data suggest that eel found at coastal Mesolithic and Neolithic sites have carbon isotope signals consistent with a marine origin with no evidence of freshwater residency. The sample of eel bone from one inland site is small but indicates carbon isotope values more consistent with freshwater residency or at least values intermediate between freshwater and marine carbon pools.     

COMPOSITIONAL VARIATIONS IN AGED AND HEATED PISTACIA RESIN FOUND IN LATE BRONZE AGE CANAANITE AMPHORAE AND BOWLS FROM AMARNA,EGYPT*

This study examines resinous deposits from the interior surfaces of sherds of imported Canaanite amphorae and locally produced bowls from the 18th Dynasty site of Tell el‐Amarna, Egypt. Archaeological evidence indicates that the Canaanite amphorae were used for resin transport, whilst the bowls are associated with burning resin as incense. A number of characteristic triterpenoids identify all the resinous deposits from both vessel types as Pistacia spp. No other resins were observed and there was no evidence of mixing with oils or fats. The composition of the archaeological resins is more complex than that of modern pistacia resin, due to degradation and generation of new components. Experimental heating alters the relative abundance of the triterpenoid composition of modern pistacia resin. One component, the triterpenoid 28‐norolean‐17‐en‐3‐one, is produced by such heating; however, an increase in its relative abundance in ancient samples is not matched by the archaeological evidence for heating. It is therefore not possible to use this component reliably to identify heated resin. However, additional unidentified components with a mass spectral base peak at m/z 453 have been associated with seven (out of 10) bowls and are not observed in resins associated with Canaanite amphorae. It is proposed that these components are more reliable molecular indicators of heating.     

The ‘Semblance of Immortality'? Resinous Materials and Mortuary Rites in Roman Britain

There is increasing evidence for complexity in mortuary practices in Britain during the Roman period. One class of burials demonstrates an association between inhumation in stone sarcophagi or lead‐lined coffins, ‘plaster’ coatings, textile shrouds and natural resins. It has been suggested that this ‘package’ represents a deliberate attempt at body preservation. Fragments with a resinous appearance found in one such burial from Arrington, Cambridgeshire, UK were analysed using gas chromatography–mass spectrometry. The triterpenic compounds identified are biomarkers for the genus Pistacia and provide the first chemical evidence for an exotic resin in a mortuary context in Roman Britain.     

New investigations into the Uluburun resin cargo

Resin found within Canaanite amphorae from the Late Bronze Age shipwreck discovered off the coast of southwest Turkey at Uluburun has previously been identified as Pistacia sp. Although evidence from Egypt suggests that this resin was in high demand and typically transported in such amphorae, it has also been proposed that the amphorae contained wine, with the resin used to seal the interior surfaces and to flavour and/or preserve the wine. To attempt to resolve this question, we have analysed five samples of pistacia resin found in amphorae from the shipwreck using a range of analytical techniques which have used in the past for the analysis of wine residues: spot tests, FT-IR, and HPLC-MS-MS. As well as the archaeological samples, we have analysed modern samples of pistacia resin, leaves and fruit to determine the effectiveness of each technique and to exclude the possibility of false positive results. In addition to the analyses for wine we also detail analysis (GC-MS) of the terpenoids for the purpose of further molecular characterisation of the resin. Bulk stable isotope analysis was used in comparison with similar resins to attempt to identify the geographical origin of the resin.     

A systematic approach to the recovery and identification of starches from carbonised deposits on ceramic vessels

Starch granules are being successfully recovered from an increasing range of artefacts. Here we present the recovery of starches from carbonised ceramic ‘foodcrusts’ from late Mesolithic–early Neolithic residues at the site of Neustadt in northern Germany. A method for investigating background loading of residues with contaminant starches is proposed by comparing interior ‘foodcrusts’ versus exterior ‘sooting’, for the purposes of eliminating samples with insignificant quantities of grains from subsequent identification procedures. The classification of starches to plant taxon is traditionally achieved by manual observations and measurement of nominal and ratio morphological variables. Here, we present a method for the automated classification of granules, using software developed in-house. The results show that when multiple granules are considered, the species selected as modern reference examples can be classified to high levels of specificity. When applied to the archaeological samples we show that wild plant resources persist in importance across the transition to agriculture, with high proportions of granule forms consistent with acorn (Quercus sp.) occurring in all samples. Hazelnut (Corylus avellana) types are less well-represented suggesting it was not an important food in the context of pottery, and may have been over-represented in the repertoire of hunter–gatherer resources. Cereals are not represented in any of the samples, supporting the notion that their adoption may have been a slow process, occurring more gradually than for other domesticated foods, or that they were not initially processed in ceramic vessels.     

Exceptional preservation of a prehistoric human brain from Heslington,Yorkshire, UK

Archaeological work in advance of construction at a site on the edge of York, UK, yielded human remains of prehistoric to Romano-British date. Amongst these was a mandible and cranium, the intra-cranial space of which contained shrunken but macroscopically recognizable remains of a brain. Although the distinctive surface morphology of the organ is preserved, little recognizable brain histology survives. Though rare, the survival of brain tissue in otherwise skeletalised human remains from wet burial environments is not unique. A survey of the literature shows that similar brain masses have been previously reported in diverse circumstances. We argue for a greater awareness of these brain masses and for more attention to be paid to their detection and identification in order to improve the reporting rate and to allow a more comprehensive study of this rare archaeological survival.     

Application of lipid biomarker analysis to evaluate the function of ‘slab-lined pits’ in Arctic Norway

Gas chromatography–mass spectrometry (GC–MS) and bulk carbon isotope determinations have been performed on samples (‘cemented organic residues’, charcoal, sediment and fire-cracked rock) excavated from 12 slab-lined pits from various locations in Arctic Norway to test the premise that these archaeological features were used for the extraction of oil from the blubber of marine mammals, such as seal, whale and walrus. A wide range of lipid compound classes were detected especially in the cemented organic residues and in the charcoal samples. The presence of long-chain unsaturated and isoprenoid fatty acids together with oxidation and thermal alteration products of unsaturated acids such as dicarboxylic acids, dihydroxyfatty acids and ω-(o-alkylphenyl)alkanoic acids suggests that these features were used for marine oil extraction at elevated temperatures. Notably the location of the hydroxyl groups in the dihydroxyfatty acids provides a record of the positional isomer of the precursor fatty acid and allows confirmation that 11-docosenoic (cetoleic) acid, the most abundant C_22:1 isomer in marine oil, was a major component of the original lipid. Further information was provided by the presence of long-chain fatty acyl moieties in surviving triacylglycerols and the presence of cholesterol. A fungal metabolite, mycose (trehalose), was found in all samples apart from a fire-cracked rock and points to microbiological activity in the pits. Bulk isotope analysis conducted on the ‘cemented organic residues’ is consistent with modern reference samples of blubber and oil from seal and whale. These data provide clear analytical evidence of the function of slab-lined pits in the archaeological record and suggest widespread exploitation of marine mammals for producing oil for heating, lighting and myriad other uses in the past.