Holocene sulphur-rich palaeochannel sediments: diagenetic conditions,magnetic properties and archaeological implications

Extensive aggregate extraction in the middle Trent valley, England, has revealed a sequence of Holocene palaeochannels associated with nationally important, and predominantly organic, archaeological remains. This paper reports observations of hyper-acidity (below pH 2), high natural magnetism and metallic sphaerules (framboids) in Holocene palaeochannel sediments at two sites in the middle Trent valley. These properties are associated with high natural remanent magnetism which has allowed the successful palaeomagnetic dating of palaeochannel fills at one of these sites (Hemington). These sediment properties are the result of the formation of ferromagnetic iron sulphides, including griegite, under conditions of high sulphur availability (from groundwater) in the presence of metallic ions and organic matter under low redox conditions, with later oxidation producing the extreme natural acidity through oxidation of disulphide (pyrite). These findings explain why, under certain groundwater conditions, alluvial palaeochannel sediments can carry post-depositional remanent magnetisation and be suitable for palaeomagnetic dating. The low pH may also be beneficial in the initial stage of wood preservation and if the sediments remain waterlogged, but probably not retard decomposition after drainage and acidification, a process that is increasingly being recognised as a threat to archaeological sites in wetland environments.     

On the intrinsic accuracy and precision of luminescence dating techniques for fired ceramics

Luminescence dating techniques have been used extensively for archaeological and geological samples. Such techniques are based on thermally or optically stimulated signals. This paper presents simulations of several luminescence techniques for equivalent dose (ED) estimation for ceramic materials containing quartz. The simulations are carried out using a recently published comprehensive kinetic model for quartz, consisting of 11 electron and hole traps and centers. The complete sequence of the experimental protocols for several thermoluminescence (TL) and optically stimulated luminescence (OSL) techniques are simulated using the same set of kinetic parameters. The specific simulated protocols are: additive dose TL protocol, predose technique (both additive and multiple activation versions), phototransfer protocol, single aliquot regenerative optically stimulated luminescence (SAR-OSL) protocol, and SAR thermoluminescence protocol (SAR-TL). One hundred random variants of the natural samples were generated by keeping the transition probabilities between energy levels fixed, while allowing simultaneous random variations of the concentrations of the 11 energy levels. The relative intrinsic accuracy and precision of the protocols are simulated by calculating the equivalent dose (ED) within the model, for a given natural burial dose of the sample. The intrinsic accuracy of these techniques is estimated by simulating natural irradiation of the samples with a known burial dose, followed by simulation of the luminescence method used to recover the estimated dose ED. The percent difference between the burial dose and the ED value represents the simulated accuracy of the luminescence technique. The relative intrinsic precision of these techniques is estimated by fitting Gaussian probability functions to the ED values obtained with the 100 model variants. It is found that the various techniques can reproduce natural paleodoses in the range 10 mGy–10 Gy with a typical intrinsic accuracy of +1 to 10%. Techniques based on single aliquot protocols were found in general to be more precise than techniques requiring the use of multiple aliquots. In addition, techniques based on interpolation of experimental data were found to be consistently both more precise and accurate than those based on extrapolation of experimental data.     

Archaeomagnetic research in the Andean highlands

Eleven archaeomagnetic samples were collected from several sites near Porco, Bolivia as part of the Proyecto Arqueológico Porco-Potosí. These samples were collected in order to 1) explore the availability of appropriate sample materials in the Bolivian Andes, and 2) assess the feasibility of pursuing reference curve research for this region. In addition, this research explored the archaeomagnetic dating application of reference curves constructed from the global geomagnetic field model gufm1 (Jackson et al., 2000), which covers the period from AD 1590–1990. This model is particularly applicable to our project, since many of the project sites are late prehispanic (pre-AD 1532) and early historic (ca. AD 1532–1825) in age. Of the 11 samples, three appeared to contain an insufficient amount of ferromagnetic minerals to provide reliable results, while eight samples produced acceptable-to-good results. The data from the eight good samples were compared to a reference curve for the period of AD 1600–2000 that was calculated for this project from the global field model, gufm1. The archaeomagnetic dates obtained for two of the samples agreed with archaeological expectations, while those for four other samples marginally or greatly postdated the archaeological age expectations. Two additional samples produced significantly different directions and could not be dated against the reference curve. It is likely that the age discrepancies for four of the samples stem from inaccuracies in the archaeomagnetic data, the archaeological age expectations, the calculated reference curve, or some combination of these factors.     

Cave occupations in Southeastern Arabia in the second millennium BCE: Excavation at Mugharat al-Kahf,North-Central Oman

This paper reports the results of excavation at Mugharat al-Kahf (WTN01) in Wādī Tanūf, North-central Oman. It also provides information on the nonmortuary and nonsedentary activities in central Oman during the Wādī Sūq period (2000–1600 BCE), as the subsistence and social arrangements of this period are the subject of much debate. Previous surveys had discovered a substantial amount of Wādī Sūq pottery at the site. This project took forward the excavation for further exploration. The excavation at Test Pit 1 identified Layers Ia and Ib, wherein pottery sherds, charred date stones and other samples for radiocarbon dating were discovered. These prove the cave's occupation during the early third millennium BCE, early second millennium BCE and the Islamic period. The analysis of artefacts and floral remains provided insights into the sojourn, storage and consumption of dates in the cave, and the mobile lifestyle in central Oman.     

Optically stimulated luminescence dating of the city wall system of ancient Tayma (NW Saudi Arabia)

In addition to a series of chronological markers (artefacts, pottery) in the archaeological contexts of ancient Tayma (NW Saudi Arabia), optically stimulated luminescence (OSL) and radiocarbon dating techniques were applied to generate reliable ages for the city wall system of the oasis. A massive aeolian sand deposit burying the oldest part of the outer wall of Tayma was sampled to obtain a minimum age for the construction of this wall. The sequence of OSL ages from the inactive dune (ID) (4900 ± 300 a, 5100 ± 400 a, 4400 ± 300 a, 3900 ± 200 a, 4000 ± 200 a) is in full accordance with ¹⁴C-AMS ages of charcoal embedded into the same dune (4190–4420 cal BP, 3870–4080 cal BP). Underlying alluvial samples from the inactive gravel sheet (IGS) in contrast give maximum ages for the construction which scatter between 6600 ± 300 a and 4900 ± 400 a. The new dating sequence provides evidence that the oldest part of the ancient city wall system already existed in the 2nd half of the 3rd mill. BC which is earlier than expected thus far from archaeological and architectural interpretation.     

Modelling site formation dynamics: geoarchaeological,chronometric and statistical approaches to a stratified rockshelter sequence,Polynesia

Formation processes and chronology are central to many archaeological endeavours, and accuracy in the latter is dependent on control of the former. Here we consider how to integrate geoarchaeological and chronometric evidence to better understand the formational history, along with the timing and duration of cultural activities, at a regionally significant site in the southern Cook Islands (Polynesia) which dates from ∼12th century AD. Initially we model natural and cultural processes of deposition using geoarchaeological evidence. The results are integrated with 21 radiocarbon dates, including nine new AMS results on identified medium and short-lived materials. Sample outliers are identified manually and statistically and a Bayesian analysis helps to refine age estimates for the site's 12 stratigraphic zones. The timing and rate of sediment accumulation is further considered through an age–depth model. Finally, the chronology developed from these combined approaches is used to address three key processes: 1) initial site use, potentially relevant to human colonisation of this Polynesian island and archipelago; 2) on-site activities and patterns of resource use; and 3) major marine deposition events which disrupted cultural activities and may have palaeoclimatological significance. The approach developed here potentially has utility elsewhere, particularly where human activities are recurrent and of limited duration.     

Seasonal dating and the valve-pairing technique in shell-midden analysis

Three-dimensional excavation of 23 artifact fragments and 4382 shells was carried out in the shell layer of an abandoned dwelling pit. Principal component analysis using three locational variables was used for drawing the central axes and the regression plane of the shell layer. Valve-pairing carried out on the clam Meretrix lusoria indicated that 380 pairs could be established among a total of 2089 unbroken valves. Preservation of shells was estimated at 70% by comparing the number of shells found in the shell layer with the clam population size which was in turn calculated by a probability formula using paired valves among samples. In addition to these data, the distance separating pairs gave some idea of the movement of shells. Seasonal dating by daily growth line counting showed that the shell layer could be subdivided into at least three main seasonal layers and that the period of accumulation was approximately 500 days.     

Growth of the Lichen Buellia albula and its Potential for Lichenometric Dating in South‐eastern Australia

Lichenometric dating is a cheap, relatively rapid means of dating rock surfaces, which has generally been overlooked in Australia. While lichenometry finds its greatest application in arctic and alpine geomorphological studies, there has been limited application to archaeological studies. This project set out to test the technique in south‐eastern Australia, and assess its usefulness for dating post‐settlement artefacts. The diameters of Buellia albula lichens growing on well‐dated memorials in the Bendigo cemetery were measured, and the relationship between age and lichen diameter established. The results indicate that B. albula can be used to determine the age of exposed cement surfaces from the 1890s to the present. The positive results suggest the technique should be investigated in other applications and environments in Australia, particularly where alternative dating techniques cannot be used.     

Tunnel engineering in the Iron Age: geoarchaeology of the Siloam Tunnel,Jerusalem

The Siloam Tunnel (ST) is the best-identified biblical structure that can be entered today. We use geological, structural, and chemical features of ST and its internal deposits to show that it is an authentic engineering project, without any pre-existing natural conduit that could have guided its excavators. Radiometrically and historically dated to ∼700 BCE, ST pinpoints the technological advance in leveling techniques that was essential for the construction of such a long tunnel without intermediate shafts. A combination of geological and archaeological evidence demonstrates that the circuitous route of ST and the final meeting of the two excavating teams are associated with continuous modifications of the plan to allow acoustic communication between hewers and the surface teams. Hydraulic plaster was applied throughout the tunnel in order to seal voids of dissolution and tectonic origin. Organic material accidentally entrapped in the plaster was carbon 14 dated, and speleothems were dated by U–Th, both corroborating the historic and epigraphic evidence ascribing the engineering advance in tunneling techniques to the Judahite King Hezekiah.     

Thorium-230 coral chronology of a late prehistoric Hawaiian chiefdom

Documenting the history of settlement in Hawaii during the last few centuries before European contact, is crucial to charting the evolution of the most complex chiefdom in Polynesia. It is precisely this period that Hawaii, and many Polynesian societies, underwent their most rapid changes in political, economic and social organisation. The last ∼500 to 300 years in the ¹⁴C calibration curve is problematic with wide fluctuations often rendering large age spans that do not precisely date single events, especially troubling with a culture-historical record of ∼1000 years duration. Here we present an extremely high precision ²³⁰Th chronology for archaeologically constrained coral samples from a range of occupancy sites. Our high precision dates allow the time of site use to be clearly demonstrated. They also provide the first dates for habitation sites in Hawaii that clearly show contemporaneous occupation—the major problem in settlement pattern archaeology. We demonstrate that two sites were occupied within the same year. Our refined chronology, provides new and exciting opportunities for tracking sociopolitical and economic developments during the last few centuries—the crucial period in the evolution and transformation of Polynesian societies.