基于X射线断层扫描技术的金漆葫芦式盒工艺研究

对漆器文物的内在结构及表面漆层的观察分析,是研究文物病害形成原因和传统制作工艺的重要途径。通过X射线成像技术,可在不损伤文物的情况下,观察文物内在的纹理结构,分析其原工艺制作方法。故本研究通过对文物X射线图像进行解析,分析金漆漆盒的胎体结构和文物的伤况成因,并对比文献记载中漆器胎底制作的差异性,尝试通过重构3D模型图片的方式直观展现文物木胎结构。研究漆器制作工艺和表层病害,有利于分析漆器文物制作工艺对文物病害的影响。相关的研究成果在日后文物保护中可以有针对性地用于分析文物伤况并制定科学严谨的修复方案,还可为以后的文物研究和工艺分析提供资料。     

安徽霍山县戴家院遗址木器表面富集物研究

利用X射线荧光能谱和化学定性手段分析了安徽霍山县戴家院遗址木器表面析出的蓝色物质。结果表明,蓝色物质为亚铁化合物,表面覆盖的黄色物质为三价铁的化合物,其形成过程与木材中的微生物有直接关系,与周围土壤成分的关系不大。     

数字X光照相技术在木雕造像上的应用

X光照相是一种传统的无损检测技术,广泛应用于各类文物的检测分析中。近年来,随着数字成像技术的逐步兴起,大大简化了X光照相的操作过程,得到的数字图像更容易观察、使用和存储,图像的编辑也成为可能。X光照相技术因此有了更大的发展空间。以一尊木雕造像为例,介绍了数字X光照相的操作过程,X光片经过编辑处理,最终得到了检测对象的X光照相三视图,并对其进行了分析和讨论。     

X射线荧光光谱技术与拉曼光谱技术在齐家文化玉器研究中的应用

为分析判断齐家文化玉器的材质,利用X射线荧光光谱技术对宁夏博物馆藏5件齐家文化玉器进行无损检测分析。结果表明,5件玉器所含元素及相对含量与和田玉相似。再借助齐家文化历史史料的有关信息,可推断为和田玉成分;利用拉曼光谱技术测得5件样品的拉曼光谱图,通过与和田玉样品拉曼光谱图比对,最强及次强特征峰位整体与之相似。可以明显看到透闪石矿物的特征峰,两种检测分析结果相互验证。研究结果为探索齐家文化玉器的玉质和玉料来源提供了重要的科学依据和准确的数据支撑。     

A study by thermal treatment and X-ray powder diffraction on burnt fragmented bones from tombs II,IV and IX belonging to the hypogeic necropolis of “Sa Figu” near Ittiri,Sassari (Sardinia,Italy)

In the course of an anthropological investigation of three tombs of the hypogeic necropolis of “Sa Figu” (near the village of Ittiri in North Sardinia, Italy), numerous burnt bone fragments were collected. In particular, from the whole necropolis we selected a tenth of long bones from tomb IV, a small fragment of femur from tomb II and four fragments belonging to tomb IX. The aim of this work is to determine a temperature range to which the bone fragments were heated, in order to assess a funerary cremation which was presumably used at that time to quickly and hygienically eliminate the flashy parts of deceased people rather than a purification rite with fires inside the sepulchres. We attempted to evaluate the range of temperature to which the bones were likely subjected, making a joint use of thermal treatment and powder X-ray diffraction investigations. From our X-ray line broadening results carried out with a modern approach (Rietveld method), it emerged that a group of five fragmented burnt bones (one specimen belonging to tomb IV, the other four from tomb IX) were subjected to a heat treatment in a temperature range from 600 and 750 °C. Conversely another group of bones (belonging to tombs II and IV) turned out to be subjected to temperatures not higher than 250 °C.     

Technological examination of Neolithic-Bronze Age pottery from central and southeast Europe and from the Near East

Scanning electron microscopy is used to examine sequences of pottery sherds from central and southeast Europe, Greece and the Near East spanning the period from the Neolithic to the Bronze Age, in order to obtain information on the ceramic technologies employed in antiquity. On the basis of the vitrification observed and the chemical composition, the types of clay and firing procedures (temperature and atmosphere) employed in the manufacture of the pottery are defined. Two under-lying trends in the associated ceramic technologies are thus identified. The first is based on the use of non-calcareous or “unstable” calcareous clays fired in a reducing atmosphere at temperatures below 800 °C and the second on the use of “stable” calcareous clays fired in an oxidizing atmosphere at temperatures in excess of 800 °C.     

Testing the accuracy of portable X-ray fluorescence to study Aztec and Colonial obsidian supply at Xaltocan,Mexico

This article demonstrates the accuracy of non-destructive portable X-ray fluorescence (pXRF) for the study of obsidian in central Mexico. Obsidian sources were identified for a sample of 103 artifacts from the site of Xaltocan, which spanned the rise and fall of the Aztec empire and the first centuries of Spanish colonial rule (AD 900–1700). Sources were assigned by comparing pXRF measurements with previously published source data and were verified using the standard techniques of laboratory XRF (lXRF) and instrumental neutron activation analysis (INAA). Additional tests of potentially confounding factors show that neither length of read time, presence of surface residue, nor incomplete detector coverage due to small artifact size compromised our ability to attribute sources to artifacts. Concave surfaces did decrease the accuracy of readings because of the greater distance between the artifact and the detector. Our results provide new insight into the stability of supply networks and markets well into the Colonial period as well as the homogenizing tendencies of the Aztec market system.     

Using photography in research with young migrants: addressing questions of visibility,movement and personal spaces

This article discusses the experience of using photography in a research project with young (prospective) migrants in Ghana and Italy. Photography can be an empowering research tool, one that offers young participants a degree of control over the research process and thus allows their points of view to emerge. However, researchers need to consider that the choice of subjects may be influenced by the children’s desire to avoid taking photographs in public, as they may attract attention and the act of pointing a camera may provoke unwanted questions and comments. Moreover, young people often lack the means to move independently, and this may further restrict the subjects they are able to photograph. Finally, they may resent adults’ intrusion into their free time and therefore see taking photographs as a chore. I argue that all these factors need to receive greater attention when choosing photography in research with young participants.     

Protecting a ‘Homeric landscape’: The making of the Butrint National Park,Albania

Abstract

This paper will present research on the vulnerability mapping of coastal archaeological sites currently being undertaken in Northern Ireland. The ultimate aim of this research is improve current predictions of where archaeological sites and landscapes will be at risk in the future from coastal erosion. The initial stage of this approach uses a suite of oblique aerial photographs to construct a baseline of eroding locations and coastal geomorphology. The erosion baseline can then be integrated with existing historic environment records to obtain a coarse first-pass archaeological vulnerability assessment. Subsequent stages can then use this assessment to prioritize future mitigation such as field surveys or monitoring exercises, or conduct further refinements of vulnerability classifications by incorporating information on site type and positioning on a local scale.     

Decorated prehistoric pottery from Castello di Annone (Piedmont,Italy): archaeometric study and pilot comparison with coeval analogous finds

Prehistoric pottery decorated with incisions or impressions filled with white and seldom coloured inlays is well documented in the archaeological literature, but the related in-depth archaeometric studies are sporadic. 43 decorated ceramic shards, dating from the Neolithic to the Bronze Age, and an Iron Age fibula from the archaeological site of Castello di Annone (Piedmont, North-Western Italy) were analysed with FTIR, Raman and XRPD for characterization of the ornamental pigments forming these inlays. Few white components were used as fillers, namely talc and bone ash (hydroxyapatite – Bone White), often as a mixture and seldom accompanied by other pigments (i.e. kaolinite and presumably secondary calcite). Comparison with freshly-heated biogenic hydroxyapatite proved that ancient Bone White pigment was calcined at about 900 °C. Such a process was kept separate from pottery firing as these white mixtures show absence of talc degradation by-products and sporadic presence of kaolinite, implying these ceramics were decorated only after firing in furnace. Actual presence of fluorapatite in bone ash could allow dating with the Fluorine Method, but lack of fluorine detection with SEM-EDS causes such an attempt to be impracticable so far. A pilot comparative study with a restricted but representative group (11) of coeval finds from other sites of Piedmont suggests that while recurrence of talc prevails in Castello di Annone from the Neolithic throughout the Bronze age, massive use of bone ash (Bone White) becomes widespread in the close Iron Age settlements, possibly consequent to a more efficient handling of its production technology.