Stable carbon isotope ratios and their relevance to the determination of accurate radiocarbon dates for lime mortars

Attempts have been made to date mortar by radiocarbon analysis. Potential problems are discussed, and the possible use of stable carbon isotopes to detect contamination by geological carbonates is investigated.     

Stable isotopic analysis of human bones from Jiahu site,Henan, China: implications for the transition to agriculture

We have investigated change in subsistence during the transition to agriculture in the site of Jiahu, Henan Province, China, using stable isotopic analysis of collagen and apatite in human bones. Millet agriculture is well documented at drier high latitudes of the Yellow River Valley, while rice agriculture predominated at wetter lower latitudes of the Yangtze Valley region. The early Neolithic site of Jiahu lies near the boundary between the drier north and wetter south. Archaeobotanical evidence shows that rice was a significant component of diet at Jiahu, but its δ¹³C value is similar to that of other foods, and therefore cannot be conclusively identified by carbon isotope analysis. Foxtail and broomcorn millets are the only C₄ crops known for the Chinese Neolithic. Because of their high δ¹³C values, their consumption can be evaluated by stable carbon isotope analysis of human bone. Collagen reflects mainly the δ¹³C value of dietary protein, and apatite accurately records that of the whole diet. Isotopic analysis of 15 well-preserved samples from three periods shows that collagen δ¹³C values were very low for almost all individuals, suggesting C₃-based foods dominated their diets. However, apatite carbonate δ¹³C values and δ¹³C spacing between collagen and apatite (Δ¹³C_ap-co) indicate that millet may have been a minor component of the diet in this region. Individuals, who consumed the smallest amounts of animal protein, as indicated by low δ¹⁵N, generally had the highest apatite δ¹³C values. Archaeobotanical evidence for millet at Jiahu is needed to support this interpretation.     

From Traditional Farming in Morocco to Early Urban Agroecology in Northern Mesopotamia: Combining Present-day Arable Weed Surveys and Crop Isotope Analysis to Reconstruct Past Agrosystems in (Semi-)arid Regions

ABSTRACT

We integrate functional weed ecology with crop stable carbon and nitrogen isotope analysis to assess their combined potential for inferring arable land management practices in (semi-)arid regions from archaeobotanical assemblages. Weed and GIS survey of 60 cereal and pulse fields in Morocco are combined with crop sampling for stable isotope analysis to frame assessment of agricultural labour intensity in terms of manuring, irrigation, tillage and hand-weeding. Under low management intensity weed variation primarily reflects geographical differences, whereas under high management intensity fields in disparate regions have similar weed flora. Manured and irrigated oasis barley fields are clearly discriminated from less intensively manured rain-fed barley terraces in southern Morocco; when fields in northern and southern Morocco are considered together, climatic differences are superimposed on the agronomic intensity gradient. Barley δ¹³C and δ¹⁵N values clearly distinguish among the Moroccan regimes. An integrated approach combines crop isotope values with weed ecological discrimination of low- and high-intensity regimes across multiple studies (in southern Morocco and southern Europe). Analysis of archaeobotanical samples from EBA Tell Brak, Syria suggests that this early city was sustained through extensive (low-intensity, large-scale) cereal farming.     

Lead Isotope Analysis of Tooth Enamel from a Viking Age Mass Grave in Southern Britain and the Constraints it Places on the Origin of the Individuals

Lead analysis of tooth enamel from individuals recovered from a Viking Age burial pit in southern England provides further evidence for their childhood origins outside Britain. All except one of the men have very low Pb concentrations that exclude anthropogenic Pb exposure. Strontium and oxygen isotope compositions identify a core group of men who have Pb isotope compositions of ²⁰⁸Pb/²⁰⁶Pb = 2.065 ± 0.021 (n = 20, 2SD) that, when compared with data from European soils, appear to exclude a childhood in the Scandinavian countries of Norway, Sweden and Finland, whereas areas of Northern continental Europe cannot be excluded.     

Application of Kernel Density Estimates to Lead Isotope Compositions of Bronzes from Ningxia,North‐West China

The aim of this paper is to apply kernel density estimates (KDEs) to the visualization and interpretation of lead isotope data from bronze assemblages found along the northern border of central China, here designated as the Arc. New lead isotope analyses of 30 leaded tin–bronze artefacts from the Wangdahu cemetery (c.500–300 bc ) in the Ningxia Hui Autonomous Region, north‐west China, provide the basis for the discussion. By using multivariate KDEs and the calculated likelihood of the overlap, the present work shows that the Wangdahu objects feature a unique linear array of isotope ratios, representing an important element of overall bronzes from the Arc in the first millennium bc . This characteristic isotope signature is fundamentally different from that of Dajing ores in north‐east China, as well from that of early Qin bronzes in Shaanxi and Gansu provinces. This suggests that a variety of metal resources were utilized by peoples living in the Arc. The KDE approach thus proves effective at presenting and comparing lead isotope data.     

Stable Isotope Analysis Reveals Variations in Human Diet at the Poundbury Camp Cemetery Site

Stable isotope analysis was undertaken on 48 individuals from Iron Age, Roman and Post-Roman periods of the Poundbury Camp Cemetery, Dorchester, England. Variations in diet, reflected by the stable isotope values, were observed between individuals from the different time periods. Differences in diet within the Late Roman period were particularly interesting, as we found that the isotope values could be related to burial type. We also found evidence of possible immigrants at Poundbury; individuals that may have come to the site from a warmer climate.     

A Multi‐Method Database of the Black and White Marbles of Göktepe (Aphrodisias), Including Isotopic,EPR, Trace and Petrographic Data

A database of the ancient marbles of Göktepe near Aphrodisias is reported, and includes 160 white, black and bichrome samples from 13 quarries and two waste deposits. The quarries are grouped into four districts. Districts 1 and 2, to the north, produced exclusively black or dark grey marbles (nero antico). Districts 3 and 4 produced white statuary marble. Nero antico and a black and white stone were also quarried in district 4, where the black marble surfaces again. The samples were characterized using petrography, isotopic analysis, EPR spectroscopy and trace analysis. The Göktepe white exhibits an unparalleled combination of fine grain, low EPR intensity and high strontium concentration that often allows easy identification. The isotopic values are less distinctive and similar to those for Carrara. In most cases, however, they are tightly grouped and also quite indicative. The black marbles exhibit a much weaker metamorphic overprint. With respect to the white marbles, they show analytical similarities but also notable differences. Therefore, establishing their provenance can be more difficult and may require the support of petrographic analysis. The results suggest that the Göktepe marbles were among the most prized and widespread statuary marbles used in Roman times, particularly from the early second century ad onwards.     

Life and Death in Neolithic Southeastern Italy: The Strontium Isotopic Evidence

There is a strong relation between people's structured identities and their chemical biographies: these can reflect the way individuals choose to reside and/or move. The strontium isotope ratio (⁸⁷Sr/⁸⁶Sr) of skeletal remains is considered a useful proxy to assess residential mobility and social practices in past populations; however, so far, it has only occasionally been applied to prehistoric contexts in the Mediterranean. In this paper, we present ⁸⁷Sr/⁸⁶Sr data of human and animal samples from several Neolithic sites in the Apulian Tavoliere (southeastern Italy), namely, Grotta Scaloria, Passo di Corvo, Masseria Candelaro and La Torretta/Poggio Imperiale. Data obtained from dental enamel reflect the local origin of the individuals and allowed us to differentiate function and meaning of the sites examined. In particular, within a generally homogeneous background of Sr signatures, the range of ⁸⁷Sr/⁸⁶Sr at Scaloria Cave is greater than at the other sites, with variation likely to be related to funerary practices. We interpret this as the evidence of the ritual use of the cave, which implied the gathering of people of different origin. The relative variation of the Sr signature among individuals, either intersite or intrasite can be tentatively associated with mobility during life as well as with social practices, such as access to foods from geologically different environments. Copyright © 2015 John Wiley & Sons, Ltd.     

Raising Practices of Neolithic Livestock Evidenced by Stable Isotope Analysis in the Wei River Valley,North China

Although a patchwork of projects shows a process of agriculture intensification in North China during the Neolithic, the impact of cereal farming on animal husbandry and their mutual interaction remain cloudy. This study reports bone collagen δ¹³C and δ¹⁵N of humans and animals from Wayaogou (ca 6.5–6.0 kyrs bp ) and Dongying (ca 5.9–5.6 kyrs bp , 4.6–4.0 kyrs bp ) to explore temporal trend of livestock raising and particularly the importance of millet fodder to stock raising practices in the Wei River valley, North China. The isotopic evidence overall shows that millet products increased in human and domestic animal diets during the mentioned chronological span. δ¹³C values of pigs and dogs at Dongying are higher than those at Wayaogou, implying that the importance of millet nutrients increased to animal husbandry diachronically. Interestingly, δ¹³C results of domestic cattle of Dongying late phase (−14.1 ± 1.1‰, N = 5) are more enriched than Wayaogou wild Bos (−17.8 ± 0.3‰, N = 3), indicating that millet fodder had taken a significant place in early cattle husbandry. Besides, differences between Bos species of the two periods also imply that δ¹³C values of bone collagen constitute a potential indicator for tracing the origin of cattle husbandry in North China. In addition, domestic sheep at Dongying produced similar isotope data to wild ovicaprid at Wayaogou, suggesting that they possibly had grazed for the most in grassland and therefore experienced a different lifestyle from cattle. Copyright © 2014 John Wiley & Sons, Ltd.     

Kings and commoners at Copan: Isotopic evidence for origins and movement in the Classic Maya period

Eight human interments were excavated in the 1990s beneath the Acropolis at the Classic Maya site of Copan in Honduras, which was the capital of a Maya kingdom from ca. AD 400 to 800. These human remains come from both royal tombs and less elaborate burials dating to the early part of this period and lie deep in the accumulated architectural layers of the Acropolis. We present a brief summary of the context, contents, and external links represented by these interments. Several lines of evidence point to connections between early Copan and Teotihuacan in the Central Highlands of Mexico, and Tikal in the central Maya lowlands of the Petén in Guatemala.