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141.
The quantitative analysis of glass, ceramics and related silicate systems by means of energy dispersive X-ray fluorescence spectrometry is considered and problems arising from the selective absorption of X-rays in multi-element specimens are discussed. A computer programme written in FORTRAN and based upon a “semi-fundamental parameters” approach to the correction of matrix effects in glass and chemically similar materials is fully described. Model data are provided to enable the programme to be run and tested. An “empirical coefficients” computer programme for the quantitative analysis of silicate systems is outlined and the limitations of this type of programme are pointed out. The importance of adequate sample preparation prior to X-ray spectrometric analysis is stressed. 相似文献
142.
青花瓷器产地判别研究 总被引:2,自引:0,他引:2
本项研究以江西省景德镇、云南省玉溪、建水、福建省平和的青花瓷器为主,结合香港清代碗窑以及德国、日本、泰国的现代青花瓷器,用能量色散X射线荧光(EDXRF)分析方法,在无损的情况下对其元素含量进行分析,得到了Ti、Mn、Fe、Co、Ni、Cu、Zn、Ga、Pb、Rb、Sr、Y、Zr13个元素的含量结果。用主成分分析方法对数据进行处理,利用第1主成分、第2主成分、第3主成分在三维座标系中绘制散点图,所得类群关系与已知情况完全相符。研究结果表明本文的研究方法可用于青花瓷器的产地判别。 相似文献
143.
Isotopic analysis of skeletons excavated during the 1950s has confirmed that they are the remains of shipwreck victims: slaves on board the Portuguese slaving brig Pacquet Real when it sank on 18 May 1818. Twenty-five slaves drowned and the remaining 133 became Prize Negroes at the Cape. The isotopic signatures are consistent with values expected for people living in an African village eating a terrestrially based diet. Analyses of different skeletal elements, i.e., teeth, long bone, and rib, are shown to be a valuable tool in tracing change or consistency in diet during a person's life, because different skeletal elements form at different stages of life and, subsequently, remodel at different rates. A comparison of isotope ratios from different skeletal elements indicates a change in diet in all these individuals, probably coincident with their enslavement. Variation between individuals in the isotopic composition of diets eaten early in life is sufficiently large to deduce heterogeneous origins for the group. 相似文献
144.
145.
Jongjit Rittirong 《Asian Population Studies》2016,12(2):187-202
This study deployed statistical and spatial (GIS) analyses to test the effects of geographic, demographic and occupational factors in predicting health centre visits among the elderly (≥60 years) with chronic ailments in Kanchanaburi Province, western Thailand. Datasets from the Kanchanaburi Demographic Surveillance System (2004 baseline survey and a 2006 project follow-up) comprised five land-use landscape and occupational strata: urban/semi-urban (industrial), rice field, plantation crop, upland and mixed economy. Travel distance to the nearest health centre was calculated following transportation routes and the GPS coordinates of individual home locations, and the number of healthcare visits under the national free universal coverage (UC) scheme reported for the previous year was used as a dependent variable in regressions. Broadly, the study found that distance was not a significant predictor of the rate of elderly health centres visits for those with co-residing spouses and/or adult children (77% of sample), and for the elderly still working (48% of the sample) who were the least likely to access healthcare. Owning motorised vehicles did not encourage visits, which also varied by land-use and occupational strata. 相似文献
146.
21世纪以来,城市网络研究成为全球和区域城市体系研究关注的焦点,但当前对国家层面城市网络空间结构演变的研究还较少涉及。基于2001—2016年间中国商业银行网点空间分布变化数据,运用社会网络分析方法,对中国城市网络空间结构的时空演变特征进行了研究。研究结果显示:中国城市网络结构由等级化向网络化转变,具体表现为在轴辐结构基础上向连通性更强的链锁网络演进;与此同时,城市网络同时呈现少数城市网络连接度的极化以及多中心扩散的特征。区域层面,东部沿海地区,特别是长三角、京津冀和珠三角三大区域的城市网络发展较为完善,与其它区域的差距持续拉大,但山东、东北和福建等省份与区域内外的联系增长也较快。大多数城市的出度和入度差异明显,但这一差异正在逐渐缩小。 相似文献
147.
河南省荥阳官庄遗址发现了用于制陶的粘土原料以及未烧制的陶坯,这为研究西周中期以后中原制陶技术提供了不可多得的研究资料。为此,本研究利用能量色散X射线荧光光谱仪、X射线衍射分析仪分析了部分原料和陶坯,并使用马弗炉对其中的陶泥进行了烧制实验。结果发现,官庄遗址的制陶原料含铁量较高,烧制过程中析出磁铁矿等铁类矿物,且烧成陶色偏深;此外,制陶原料和同期陶片之间物相的趋同性和化学成分的聚类性,显示陶器本地生产的特性。研究结果为研究西周晚期至春秋早期时期制陶技术提供了基础材料。 相似文献
148.
青海瞿昙寺壁画颜料的研究 总被引:3,自引:0,他引:3
通过对青海瞿昙寺画郎和建筑彩绘所用的22个绘画颜料样品的 x-射线衍射和同位素 x 荧光分析.共分析出20多种无机矿物颜料,此外.还有蓝钯、黄钯有机颜料。本文对这些颜料的分析结果进行丁综合论述.并与敦煌石窟、麦积山石窟、炳灵寺石窟等的彩绘颜料进行了研究。 相似文献
149.
陕西安康紫阳北五省会馆壁画颜料分析研究 总被引:3,自引:3,他引:0
陕西安康紫阳北五省会馆壁画是目前陕西省境内发现的最大的一处建筑壁画,为了解其颜料组成,本工作采用X射线荧光、偏光显微镜、X射线衍射、激光显微拉曼光谱及扫描电镜能谱分析相结合的分析方法,对颜料样品进行了分析。结果表明,北五省会馆壁画除正殿发现一处红色染料外,其他均为无机颜料;红色颜料主要是铅丹、朱砂、铁红;绿色颜料为氯铜矿、石绿、斜氯铜矿;蓝色颜料的主要成分是普鲁士蓝、smalt、石青;黄色颜料为雌黄、铁黄;褐色颜料的主要成分是铁红及铅丹的变色产物二氧化铅;黑色为炭黑;白色颜料主要是铅白,且多使用铅白作为调色颜料。研究结果对于了解清代民间壁画的制作工艺,丰富对陕西建筑壁画的认识具有重要意义。 相似文献
150.
B. F. Leach J. M. Davidson L. M. Horwood 《International Journal of Osteoarchaeology》1997,7(5):481-496
Twenty-four measurements were taken on five of the paired cranial bones and the otoliths of a modern sample of 177 blue cod. Parapercis colias. Regression analysis was performed on these measurements to estimate live fork length and ungutted weight. A number of regression models were examined (linear, logarithmic, exponential and power curve) to work out the optimum estimator for each bone measurement. It was found that live fork length of this species can be estimated with a standard error of less than ±28 mm, and the weight to less than ±140 g. Coefficients are provided for 48 equations linking bone size to live characteristics. This is followed by a study of blue cod from an archaeological site at Waihora in the Chatham Islands. Measurements were made on 8036 archaeological bones with a minimum number of individuals of 2547. It was found that the blue cod catch had near normal characteristics, with a mean fork length of 327 mm and SD of 57 mm. The mean body weight was estimated at 569 g. The usable meat weight represented by these fish is estimated to be 1.0 t. © 1997 John Wiley & Sons, Ltd. 相似文献