GEOCHEMICAL CHARACTERIZATION OF ARCHAEOLOGICAL LIME MORTARS: PROVENANCE INPUTS*

Chemical and mineralogical analyses were carried out on historical lime mortars from the parish church of Santa María La Real (Guipúzcoa). The study included various periods ranging from Roman to modern times and allowed the identification of various types of raw materials. In order to obtain pure binder, free of carbonate aggregates and charcoal particles, an innovative binder separation method was implemented. The chemical composition of the binder allows discrimination of different provenance areas for the raw materials, although those areas do not correlate with specific historical periods. In addition, the influence of burial processes on the primeval chemical features has been assessed and reveals that modern mortars display greater chemical modification than the Roman mortars.     

PINE RESINS AND POTTERY SEALING: ANALYSIS OF ABSORBED AND VISIBLE POTTERY RESIDUES FROM CENTRAL NEW YORK STATE*

Analysis was performed on absorbed and visible residues from 21 New York State prehistoric pottery sherds dating from 2905 ± 35 bp (Intcal04) (1256–998 cal bc ) to 425 ± 40 bp (Intcal04) (1417–1626 cal ad ). The use of pine resin was detected in 10 of 12 absorbed residue samples and 11 of 17 sherds subjected to visible residue analysis. It seems likely that the pots were resin‐sealed to make them more impermeable, constituting the first chemical evidence of extensive resin‐sealing in North America. A comparison of the results of absorbed and visible residues from eight of the sherds indicates that the two kinds of residue provide complementary evidence of vessel use.     

THE TRADING OF ANCIENT GLASS BEADS: NEW ANALYTICAL DATA FROM SOUTH ASIAN AND EAST AFRICAN SODA–ALUMINA GLASS BEADS*

The occurrence of similar glass beads at archaeological sites in Africa and Asia bears witness to the trade relationship between the two continents. This paper reports elemental analysis results from a recent in‐depth laser ablation – inductively coupled plasma – mass spectrometry (LA–ICP–MS) study of a group of archaeological glass beads with a specific alumina‐rich composition from East Africa, India and Sri Lanka. Based on the concentrations of the trace elements, two different subgroups were identified. One subgroup occurs at early periods (fourth century bce to fifth century ace ) in South India and Sri Lanka. The second subgroup appears at later dates in Africa and was identified at different Kenyan sites dated from the ninth to the 19th century ace , and at the contemporaneous site of Chaul in western India.     

Some spatial analyses of Chalcolithic settlement in Southern Israel

This paper is a brief investigation of one of the outstanding problems in Chalcolithic archaeology in the Negev desert of Israel: that of the spatial distribution of sites and the possible relationships between these sites that may be inferred. Although the region is rich in archaeological data for the Chalcolithic period, very little work has thus far been undertaken in terms of the quantification of the archaeological data – a necessary prerequisite for complex spatial analysis. Nevertheless, simple analysis of settlement patterns using the data presently available for 403 Chalcolithic sites in the Negev is given as an example. Autocorrelation tests measuring clustering and dispersion of sites show that the overall impression of clustering is a factor of access to farming land, water, grazing and Mediterranean maquis, but that smaller scale analysis suggests that settlement patterns were essentially random. This makes it difficult to argue in favour of settlement hierarchies or structured settlement of any kind.     

Chemical analyses of the earliest pigment residues from the uttermost part of the planet (Beagle Channel region,Tierra del Fuego,Southern South America)

This paper presents the results of chemical analyses of the organic and inorganic fractions of pigment residues found in three archaeological sites located in the Beagle Channel region, Tierra del Fuego, Southern South America. Twenty-one archaeological samples have been analysed through XRD, SEM–EDX, FT-IR and GC–MS in order to characterise their inorganic colouring components and to search for the presence of organic substances used as binders. Lipids found in some samples are considered as potential binders. These organic components are compared to those found in archaeological sediment samples from the same layers where the pigments have been found, in order to search for potential taphonomic contaminations of the latter by the former. Results show that such contaminations are unlikely, hence the lipid contents are deemed of anthropic origin. The pigment sample results are also compared to data from analyses of natural sediment samples collected in several localities of the Beagle Channel in order to search for potential natural pigment sources. Results show that organic and inorganic components of these sediments are not the same than those present in the archaeological pigment samples, hence the pigment raw material sources have not been yet located. All these data provide for the first time evidence of the existence of ancient activities of pigment sourcing and paint preparation with organic binders which range from 6000 BP to 1900 BP in the southernmost region of the planet.     

The circulation of precious metals in the Arab Empire: the case of the near and the Middle East*

The analysis by nuclear activation techniques and by inductively coupled plasma mass spectrometry combined with an UV laser of a large number of gold coins issued in the Arab Empire from the seventh to the 12th century ad showed that several different supplying sources were used, according to the region and to the period. The aim of this paper is to point out the circulation of gold in the Near and Middle Eastern mints of the Arab Empire and to make a parallel with the mints’ policies running in the other regions of the Empire, such as North Africa, the Iberian Peninsula and the Sicily. The identification of different gold ores by means of characteristic trace elements indicated recycling of the ancient coinage and, after ad 750, the minting in the entire Arab Empire of different new gold ores: Egyptian type, North Eastern type and West African type. The analysis of a small number of silver coins from the same periods and regions also showed a change in the ore supply after ad 750.     

Stylistic variability of stemmed obsidian tools (mata’a), frequency seriation,and the scale of social interaction on Rapa Nui (Easter Island)

Easter Island, or Rapa Nui, has been the focus of much research and speculation, particularly with reference to the island’s hundreds of giant, enigmatic statues and the set of conditions that supported their construction and transportation. In this paper, we analyze an abundant class of lithic artifacts, mata’a, to study of patterns of cultural transmission with implications for the evolution of groups, competition, and scale of socio-political organization among this island population. While these kinds of studies often draw upon assemblages of decorated ceramics, here we show how analysis of variability unconstrained by performance allows us to measure aspects of inheritance related to the manufacture of these artifacts. In the case of mata’a from Rapa Nui, we demonstrate that it is possible to reach falsifiable conclusions about the evolutionary dynamics that shaped the remarkable archaeological record on Rapa Nui.     

How flakes shatter: a critical evaluation of quartz fracture analysis

Despite its worldwide use as a stone tool raw material, quartz is known to be a difficult material for archaeologists. The main reason for this is the tendency of quartz flakes to fragment during detachment, which complicates the use of traditional lithic analyses. In this article we present an experimental study of quartz flake fragmentation. We evaluate the method called fracture analysis that has been developed and used explicitly for the study of quartz assemblages. The method assumes high predictability of quartz flake fragmentation, but our experiments show that there is significant variation in fragmentation that fracture analysis does not take into account. Our results indicate that this variation is partly explained by indenter hardness, the relative thickness of the detached flake, as well as individual knapper-related factors. These results undermine the applicability of quartz fracture analysis in its current form. In addition, we discuss the effects of flake fragmentation on the technological organisation of prehistoric quartz users and suggest that it has affected reduction strategies as well as blank and tool dimensions. We also suggest that there should be mobility-related differences in archaeological assemblages in terms of the quality of the quartz raw material and that the curation of quartz should be low in relation to better quality raw materials used parallel with it.     

The meals in a Tuscan building yard during the Middle Age. Characterization of organic residues in ceramic potsherds

The characterization of organic residues found in ceramics objects coming from the Carmine Convent in Siena (Central Italy), probably built in the second half of the 13th century, is described. The nine objects analyzed in this study are pots, casseroles, and lids and they were used as filling material of the vault of one room of the convent.