Archaeometallurgical Investigations in Nakhchivan,Azerbaijan: What Does the Evidence from Late Chalcolithic Ovçular Tepesi Tell Us about the Beginning of Extractive Metallurgy?

The Late Chalcolithic (4400–3950 b.c.) occupation levels from Ovçular Tepesi have yielded a significant assemblage of copper objects and remains of copper production. Together with ore finds, two fragments of nozzle, crucible remains, and a number of small metal artifacts, this assemblage includes the unexpected discovery of three copper axes in an infant burial jar. These axes are the earliest examples of large copper tools known to date in southwestern Asia, whether it is in the Caucasus, Iran, or the Anatolian highlands. More importantly, the fact that these objects were locally produced suggests that significant metallurgical activities were being carried out at Ovçular as early as the second half of the 5th millennium b.c. After presenting the evidence from Ovçular Tepesi, this paper will proceed to a reassessment of the available archaeological and geochemical data concerning the emergence of extractive metallurgy in the southern Caucasus.     

The function of Chalcolithic metalwork in Italy: an assessment based on use-wear analysis

This paper presents results of the use-wear analysis of Chalcolithic copper-base metalwork from the Italian peninsula. Previous research led to contrasting scholarly opinions regarding the function of early metal axes, daggers and halberds from this region. Whilst some authors interpreted these objects as utilitarian tools and weapons, others saw them as symbolic signifiers of social status and personhood. The analysis conducted here shows that this is a false dichotomy as all classes of metalwork seem to embody to some extent both utilitarian and non-utilitarian values. In particular, axes were primarily used for woodworking and other practical tasks, but were mostly withdrawn from circulation when still usable. This suggests that deposition practices bore a loose relationship, if any, with the functional value of the tools. Daggers were employed in a range of symbolically charged practices that left little wear on cutting edges. These probably included the sacrificial slaughtering and skinning of large animals such as cattle and horses. Halberds were utilised as weapons in champion’s duels in which display of combative skills and prowess would have been far more important than killing the opponent. This explains the relatively low rate of damaged blades in the record. Regardless of their practical function in lifetime settings, these objects were all similarly employed in burial to reproduce core social values such as gender and age. Importantly, this study contributes to debunking undemonstrated assumptions concerning the function of early metalwork in European prehistory. It also defines a replicable analytical protocol for the use-wear analysis of ancient copper-alloy artefacts.     

Geometric architectural pattern and constructive energy analysis at Los Millares Copper Age Settlement (Santa Fé de Mondújar,Almería,Andalusia)

Enclosure walls from late IV to II millennium are an important archeological feature in southeast Iberia and south Portugal. These enclosures were considered to be fortified settlements but have more recently been interpreted as the result of general processes of social complexity, symbolism, monumentality, interaction, and space demarcation, among others. Metric and geometric studies associated with architectural concepts are very important tools to analyze prehistoric communities and bring their own perspective to bear. The planning of monuments or even whole settlements includes a more general perception of space, determined by mythology, topography, taking of place, and social hierarchy, among others.     

First evidence of Equus asinus L. in the Chalcolithic disputes the Phoenicians as the first to introduce donkeys into the Iberian Peninsula

Two equid species have been documented in the Pleistocene of the Iberian Peninsula, the horse Equus caballus, and the Eurasian hemione Equus hydruntinus. While the former survived the Holocene–Pleistocene until now, the timing for the extinction of the latter is unclear. Scarce, fragmented archaeological remains assess the presence of small equids living in the Holocene of Iberia. Those could possibly correspond to the Eurasian hemione although unambiguous morphological identification is often not possible. With the find of an equid tooth from Leceia, a Chalcolithic fortified site in Portugal, and using both morphological and mitochondrial genome analyses, we demonstrate for the first time the presence of a new equid species in Holocene Iberia, namely a donkey (Equus asinus). Radiocarbon dating of the tooth to Cal 2340–2130, and 2080–2060 BC with 95% probability, demonstrates that donkeys were present in Iberia well before the arrival of Phoenicians in the first quarter of the first millennium BC (900–750 years BC), which were considered so far as the first who introduced donkeys in the region.     

Geochemical discrimination of basaltic sources as a tool for provenance analyses of bifacial tools in the southern Levant: first results from the Jezreel Valley,Israel

The determination of groundstone tool sources bears the potential to examine aspects like raw material selection and preference, mobility, trade and exchange patterns, control over resources and long term use of raw material sources. The discovery of the Neolithic/Chalcolithic basanite bifacial quarry of Giv'at Kipod in the Jezreel Valley, Israel, provides the opportunity of raw material centred provenance studies of bifacials in the southern Levant. The basis for reliable provenance analyses is a clear geochemical characterization of the extraction site and its discrimination from other potential sources. To achieve this, the Miocene magmatic rocks of the Jezreel Valley were sampled and analysed by XRF and La-ICP-MS. The geochemical evaluation, combined with cluster analyses, resulted in a clear discrimination of the Giv'at Kipod lava from other basaltic sources in the area. Based on the geochemical field data, a Giv'at Kipod provenance for six bifacial tools found in three archaeological sites dated to the Neolithic and the Chalcolithic periods was established. The results suggest that the quarry was in use for several millennia. This pilot study demonstrates that for provenance analyses lava outcrops in the southern Levant can be geochemically discriminated from each other on a very small spatial scale, on the basis of a detailed field sampling and the application of multivariate methods.     

The role of arsenic in Chalcolithic copper artefacts – insights from Vila Nova de São Pedro (Portugal)

The Castro of Vila Nova de São Pedro (VNSP) is an emblematic settlement located at Azambuja, Portuguese Estremadura. It was occupied during the third and second millennia BC, predominantly during the Chalcolithic period. A diversified collection of 53 copper-based artefacts (most part in a fragmentary condition), belonging to an extensive metallic collection recovered during excavations carried out in VNSP, was studied using micro-EDXRF spectrometry, optical microscopy and SEM-EDS. Additionally, Vickers microhardness measurements were performed to establish the effectiveness of the thermomechanical treatment in the hardness of the artefacts. Results show that the Largo do Carmo, artefact collection is mainly composed of copper or arsenical copper, being 37% of the artefacts made of copper alloyed with arsenic (As > 2%). A statistically significant association was found between copper alloyed with arsenic and artefacts classified as tools/weapons (arrowheads, daggers and knives). In several cases, the presence of arsenic rich phases in the microstructure, resulting from an inverse segregation phenomenon, shows no evidence of chemical homogeneity control during the artefact manufacture. Microstructural analyses also show that the majority of this group (73%) was shaped with forging plus annealing operation cycles and 23% of the artefacts received a final cold hammering after the forging and annealing. An association between the presence of a final forging treatment and artefacts presenting higher arsenic contents was also identified. Nevertheless, no direct correlation was found between the arsenic content of the alloy and its hardness. Also no direct correlation was found between the hardness and a final forging operation. However, it was observed that a harder forging was applied to the cutting edge of the artefacts and consequently a high hardness in this area was obtained despite the arsenic content of the alloy. Concerning arsenical copper alloys, all evidences point out that the potential for obtaining a harder material was not recognized by the ancient metallurgists and the selection of the alloy was possibly made based on colour.     

Fuelwood,crops and acorns from Iritegi cave (Oñati,Basque Country)

Abstract

We present the analyses of plant macroremains from Iritegi, a cave from Northern Iberia with archaeological levels dated from the Chalcolithic to the Iron Age. Wood charcoal assemblages are dominated throughout the sequence by Fraxinus. Other important taxa are Quercus subg. Quercus, followed by Corylus avellana, Fagus sylvatica, Ilex aquifolium, Taxus baccata and Ulmus. Acer, Alnus and Maloideae occur in very low numbers. The high percentages of Fraxinus are possibly result from the selection of ash for fodder. Evidence for the use of crops (Hordeum vulgare, Triticum aestivum/durum) comes only from the Chalcolithic contexts. The identification of acorns in one Chalcolithic hearth shows that roasting of these nuts was taking place maybe to improve taste and to facilitate further processing or to improve storage conditions. The results show that plant food gathering still played a role within the subsistence of farming human groups in the region.     

A truly refractory crucible from fourth millennium Tepe Hissar, Northeast Iran

From the Early Chalcolithic to the Late Iron Age, melting and smelting crucibles were usually made from non-refractory ceramic fabrics, which required heating of the charge from within the crucible to avoid collapsing the ceramic itself. In this paper, an unusual melting crucible from Northeast Iran, radiocarbon-dated to the Late Chalcolithic (ca. 3600 BCE), will be presented that significantly changes our understanding of the development of technical ceramics in Southwest Asia. This crucible, made of a highly refractory talc-based ceramic held together by an outer layer of traditional non-refractory ceramic, is to our knowledge unprecedented at such an early date. As will be argued, this ancient crucible was heated from the exterior or from below and not from the interior. This method of firing, combined with the highly-specialized construction technique, makes this crucible so far unique in prehistoric metallurgy, and forces us to re-examine traditional models for the development of technical ceramics and metallurgical practices in the Old World.     

The contents of unusual cone-shaped vessels (cornets) from the Chalcolithic of the southern Levant

Cornets are cone-shaped ceramic vessels, characteristic of the Chalcolithic period (ca. 4700–3700 BC) in Israel and Jordan. Their contents and use are unknown. Gas chromatography with flame ionization and mass-selective detection, showed that extracts of cornets from five different sites with different related activities (domestic, habitation cave and a cultic complex) all contain the same assemblage of mainly n-alkanes adsorbed within their walls. This assemblage differs from those found in other types of ceramic vessels from the same sites, as well as from the residues found within the associated sediments. The assemblage of odd and even-numbered n-alkanes found in the cornets is almost identical to that found in the residues of beeswax heated on modern ceramic fragments, as well as in a beehive from the Iron Age IIA strata at Tel Rehov, Israel. Thus the cornets are most likely to have contained beeswax. The presence of beeswax in the cornets contributes to our understanding of the Chalcolithic period; a time when secondary products such as milk, olive oil and wine are thought to have come into use.     

Evidence of interpersonal violence at the Chalcolithic village of Shiqmim (Israel)

Three circumscribed depressed fractures were found on the skull of an adolescent boy recovered from a primary intramural burial at the Chalcolithic site of Shiqmim, northern Negev, Israel dated to (∼4500–3200 BCE). The fractures were located on the left side and back of the skull. They are circular in outline and have sharp margins containing numerous small bone fragments. These indicate that the skull was fractured when the bone was still fresh and were the probable cause of death. The location of the fractured areas is typical of blows inflicted by a right‐handed individual in face‐to‐face conflict. The size and shape of the fractures, suggests that they were inflicted by a blunt instrument, possibly a mace head. The absence of any signs of healing or infection indicates that all fractures occurred within a short space of time and resulted in death. Neither biological characteristics nor burial pattern show any unique features that distinguish this individual from others recovered at this site. Copyright © 2003 John Wiley & Sons, Ltd.