ARCHAEOMETRIC INVESTIGATIONS OF SGRAFFITO CERAMIC TILES (FIFTEENTH‐SIXTEENTH CENTURIES) RECOVERED FROM EXCAVATIONS IN UDINE (NORTH‐EAST ITALY)*

Most of the Renaissance sgraffito tiles excavated in Udine (Italy) constitute a homogeous group, the tile body having a CaO/MgO molar ratio ?= 3:2. They were produced using a dolomite‐ and calcite‐containing clay fired at 900–950°C. A small group of samples, with a lower firing temperature and a CaO/MgO ratio ?= 2:3, was probably produced in a different factory. Slip and transparent glaze, characterized by optical microscopy and inductively coupled plasma atomic emission spectrometry, are an illite‐rich clay and a lead silicate, respectively.     

A COMPARISON OF METHODS FOR ESTABLISHING FATTY ACID CONCENTRATION GRADIENTS ACROSS POTSHERDS: A CASE STUDY USING LATE BRONZE AGE CANAANITE AMPHORAE*

Canaanite amphorae fragments in fabrics believed to be associated with the bulk transport of vegetable oils from the fourteenth‐century BC site of Amarna, Egypt, have been examined. A comparison is made between solvent extraction, saponification and the use of TMTFTH (m‐trifluoromethylphenyl)trimethylammomum hydroxide, used here for the combined extraction and derivatization of ceramic‐absorbed organic residues. Extracts were studied using gas chromatography and gas chromatography‐mass spectrometry. The extraction of fatty acids from small ceramic samples has established concentration gradients of absorbed organic matter from the inner to the outer surfaces of the sherds.     

NEW ARCHAEOINTENSITY RESULTS FROM GREEK MATERIALS*

This paper reports palaeointensity results from Greek materials from EC and AD periods, recently obtained in the Sofia palaeomagnetic laboratory. The classical Thellier method was applied and of 26 specimens studied 20 gave acceptable results. The paper aims to compare the newly obtained results with previously published ones from Greece and neighbouring territories relating to the same period of time. The trend of palaeointensity obtained for the period 2900–1700 BC coincides well with the Bulgarian intensity variation curve, while the younger period, 1900–1200 BC, needs further investigation because of the contradictory results obtained by different authors. It is also established that the bricks from the church of Agios Ioannis are earlier than the date of the building's construction and are reused.     

Composition of the Lustre Pigment Used in the Production Of 13th Century AD Raqqa Lustreware from Syria

The very rare find of the relic of the original lustre pigment attached to the glazed surface of a sherd of 13th century ad Raqqa type lustreware from Syria has been analysed using a combination of analytical scanning electron microscopy (SEM), micro‐X‐ray diffraction (XRD) and Rutherford backscattering spectroscopy (RBS). The composition of the pigment relic inferred from these analyses is shown to match those of recipes for lustre production given in the early treatises by Jazbir Ibn Hayyan (c. ad 721–c. ad 815) and Abū'l Qasim (ad 1301). Similarities and differences between this 13th century ad Syrian pigment and pigments used in the ninth century ad in Iraq, in the 14th century ad in Islamic and Hispano‐Moresque Spain, and in the 16th century ad in Renaissance Italy are discussed.     

NEUTRON ACTIVATION ANALYSIS OF INCA AND COLONIAL CERAMICS FROM CENTRAL HIGHLAND ECUADOR

Fifty‐three ceramic samples were collected in the area of the colonial city of Riobamba, Ecuador (today Sicalpa/Cajabamba). Neutron activation analysis was used to attempt to establish elemental compositions, and from these gain information on the manufacturing locations of these samples. Colonial samples imported from Panama were separable by their high Cs contents, and can be sorted into glazed and unglazed industries based on As and Cs. High As concentrations in several sherds indicate an origin near Cuenca, in the Southern Highlands of Ecuador, for both colonial and Inca samples. Inca and colonial Quito samples from the north of the country are identifiable through high Na combined with low Sc and Cr concentrations. Locally produced Puruhá, unglazed colonial and majolica samples form a group indicative of local Riobamba elemental composition.     

Trude Dothan (1922–2016): In Memoriam

Abstract

This paper sheds new light on the most common type of pottery associated with advanced phases of Early Bronze I (EB I) in the southern Jordan valley: the distinctive family or group known as Um Hammad Ware, or Proto-Urban D (PUD) Ware. To date, this kind of pottery was thought to be concentrated mostly around the site of Tell Um Hammad. This study presents new evidence suggesting that this ware was dispersed over a region considerably wider than previously understood, and that the centre of its manufacture was probably in the region of western Wadi Far'ah. This paper also explores the possibility that the origins of this family are to be found in the pottery traditions of the Golan region during the Chalcolithic period.     

ceraDAT—PROTOTYPE OF A WEB‐BASED RELATIONAL DATABASE FOR ARCHAEOLOGICAL CERAMICS

The prototype of a relational database for archaeological ceramics is presented. At this stage, the ceraDAT database contains the elemental compositions of several thousand ceramic artefacts from the Eastern Mediterranean, analysed by neutron activation analysis (NAA) at different laboratories. The data have been calibrated on the basis of the analytical routine and can be accessed via a web application. Apart from the elemental compositions, the database contains reference patterns of specific sites, metadata concerning archaeological information, the geographical distribution, literature references and former statistical evaluations. Due to the database design, the structure can be extended in future towards petrographical and mineralogical information.     

Dental microwear study of pigs from the classical site of Sagalassos (SW Turkey) as an aid for the reconstruction of husbandry practices in ancient times

Abstract

Microwear analysis of pig teeth from the classical site of Sagalassos (SW Turkey) is undertaken to obtain insight into pig management strategies in this region from the 1st to 7th centuries AD. Earlier research on modern pigs revealed significant differences in microwear patterns between stall-fed and free-ranging, rooting individuals. A comparison of the microwear data of the Sagalassos pig with those from archaeological and modern pigs with a known or presumed type of management shows that the microwear of the Sagalassos pigs is very different. It is suggested that the Sagalassos pigs had a very soft, non-abrasive diet, that in the first instance cannot be attributed to either management type. Therefore, the nature of the substrate on which the animals were foraging and its impact on microwear are considered and the microwear data are compared with the results of previous archaeozoological research carried out at the site. Further, diachronic changes in microwear patterns are investigated.     

The production technology of Iznik pottery—a reassessment*

Previous research has established that Iznik pottery differs from other Islamic stonepaste pottery in that its stonepaste bodies contain lead oxide as well as soda and lime, and that a significant proportion of the tin oxide in its glaze is present in solution rather than as tin oxide particles. In order to better understand these distinguishing features, the chemical compositions and microstructures of Iznik pottery and tile samples, together with those of lumps of glass found in association, were investigated using both scanning electron and optical microscopy. These data have been supplemented by the study of replicate lead–alkali glazes produced in the laboratory with a range of different compositions. The results demonstrate that separate soda–lime and high‐lead glasses were used in the production of Iznik stonepaste bodies, and that the total glass contents of the bodies were significantly higher than those quoted by Abū’l‐Qāsim, who was writing in about ad 1300. The very high purity of the lead–soda Iznik glazes indicated that the alkali flux used was either a purified plant ash or an as yet unidentified mineral source of soda. Replication experiments established that the high solubility of tin oxide in the glaze was due to the high purity of the glaze constituents. Furthermore, it is suggested that tin oxide was added to the glaze in order to give it a very slight opacity and thus obscure any blemishes in the underlying body.