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Ancient mortars from northern Italy, dating from the fifth to the seventeenth century AD, were examined in order to formulate an hypothesis regarding the origin of the white lumps often observed in these mortars and in other samples of the same geographical provenance. Various characterization techniques were employed, including scanning electron microscopy, X-ray powder diffraction and Fourier transform infrared (FTIR) and micro-FTIR spectroscopy. 相似文献
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QUANTITATIVE ANALYSIS OF COPPER-TIN BRONZES BY MEANS OF GLOW DISCHARGE OPTICAL EMISSION SPECTROMETRY
Glow discharge optical emission spectrometry (GDOES) has been used for obtaining calibration curves for copper, tin, lead, silver, antimony, arsenic, zinc and iron from standards including copper-base alloys (Cu 61.33-99.95%) and from bronze Punic coins. The GDOES results were calibrated using atomic absorption spectroscopy with inductively coupled plasma atomization (ICPAAS) to analyse the standards and coins. For all these materials, the results show that via GDOES it is possible to obtain reliable and reproducible calibration curves for copper, tin, lead, zinc and iron with a linear behaviour as a function of the content. The quantitative GDOES and ICPAAS data for the coins have been also compared with those obtained via X-ray fluorescence (XRF) and it is shown that GDOES, ICPAAS and XRF agree well with one another considering that the bronze coins are inhomogeneous to some degree. As an example of GDOES analytical features, a depth concentration profile through a thin bronze patina is shown and briefly discussed. 相似文献
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The repeated failure to design and appropriately target policies and interventions which address the needs of rural peoples in Africa suggests that something may be wrong with our understanding of the way that these peoples live their lives. Perspectives which focus on intra-household processes, and on gender issues in particular, represent useful advances in the way that the social and economic lives of Africa's rural peoples are conceptualized. However, this article questions the value of adopting development planning, policy and project approaches based on the rigid identification of `gender roles'. By reference to field research undertaken in northern Ghana, the paper aims to demonstrate that other social constructs, such as marital status and seniority, may be as important as gender in determining the roles and status of individuals in African rural societies. The article concludes by highlighting a number of practical implications of this finding in terms of the structuring of development-oriented research and the targeting of policy and interventions. 相似文献
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Ceramic vessels from Later Stone Age sites in the Seacow river valley, South Africa, were heavily tempered with C4 grasses. However, most δ13C values of the temper fall between the known δ13C ranges for C4 and C3 grasses. Among possible C3 additives that could skew the signal, ground bone, animal dung, alpine grass, Karoo scrub ash, and humic acid contamination are eliminated. The sherd surfaces yield fatty chars with C3-like values. Although these are not enough to account for all the skewing, they represent only the final cooking event. They were preceded by many such events in which fat was absorbed into the C4 grass then charred to soot by later periods in the fire. Thus organic carbon with the isotope composition of the fat built up while the vessel remained in use. 相似文献
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The characterization of various samples of white marble from the archaeological site of Tharros (Sardinia) is the starting point for the reexamination of the capabilities of electron spin resonance (ESR) spectroscopy as a tool for identifying the quarries of origin of ancient marble artefacts. Existing methods and data bases are employed for the assignment of our samples, but also reviewed to see if a more extensive use of the technique is feasible. It turns out that ESR spectroscopy, coupled with other available methods, may readily provide valuable information, often yielding the final answer to the problem of marble provenance. However, it is also clear that much work has still to be done to standardize the data collection and analysis procedures and to expand the available data base. 相似文献
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A combination of analytical techniques, including thin-section observations, scanning electron microscopy, X-ray diffraction and X-ray fluorescence analysis, was applied to study the nature and origin of an adhesive used for mounting flint sickle blades to a wooden handle, recovered from early Eighteenth Dynasty culture layers of the multi-layer settlement at Tell el Dab'a, Lower Eygpt. The results obtained from these investigations led to the conclusion that the adhesive is a pure lime plaster, thus providing the oldest evidence for the use of this material as a binding agent so far known in ancient Egypt. 相似文献
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Jean-Marc Drouin Patrick Gautier Dalché Fabien Chareix Charles Lenay Monique Cottret Bernard Vandewalle François Laplanche Françoise Waquet Agnès Spiquel Ariane Poulantzas Olivier Martin Sophie Roux Ilana Löwy Françoise Waquet Isabelle Brian Michel Cassan Jean-Marc Rohrbasser Jean-Michel Vienne Marc Renneville Bernard Lahire Mikhaäl Xifaras Bertrand Binoche Stéphane Haber Jean-François Pradeau Noël Bonneuil Marie Jaisson 《Revue de synthèse / Centre international de synthèse》1997,118(4):551-613