Archaeomagnetic versus luminescence methods: the case of an Early Byzantine ceramic workshop in Thessaloniki,Greece

In this contribution, we present a combined archaeomagnetic and luminescence study of archaeologically dated structures. The investigated area is a ceramic workshop comprising several Early Byzantine kilns. Based on (a) the archaeological–anthropogenic stratigraphy of the site, (b) the structural characteristics of the kilns and (c) the few ceramic findings revealed within their context, the operation of this brick and tile factory is approximately dated between the middle of the fifth century until the first decades of the sixth century AD. Three of the well-preserved workshop kilns have been studied archaeomagnetically. The full vector of the geomagnetic field, accompanied by rock magnetic analyses of the studied material, has been defined. The archaeomagnetic study revealed similar directions among the three kilns indicating and confirming their contemporary use. Additionally, several luminescence measurements were obtained on material from the same kilns. The dating of the site was performed with both methods. The archaeomagnetic dating is convergent with the archaeological estimation only when its upper limit is considered. Concerning the luminescence dating, the calculated ages (corrected for anomalous fading and for the ⁴⁰K content) with their standard deviations are convergent with the archaeological estimations for the first kiln, while for the other two, the results seem to be incompatible. The possible factors that provoked this divergence are thoroughly discussed.     

Innovation and tradition in the fourth century mosaic of the <Emphasis Type="Italic">Casa delle Bestie Ferite</Emphasis> in Aquileia,Italy: archaeometric characterisation of the glass tesserae

The present paper focuses on the archaeometric characterisation of 38 glass tesserae of various colours from an in situ mosaic in Aquileia, Italy, dated to the second half of the fourth century AD. The examination of the textural, mineralogical and chemical features, conducted by means of a multi-methodological approach (optical microscopy (OM), scanning electron microscopy-energy dispersive X-ray spectroscopy (SEM-EDS), electron probe micro analysis (EPMA), X-ray diffraction (XRD) and Fibre Optic Reflectance Spectrophotometer (FORS)), has provided valuable insights into the changes in the production technology during the transition between the Roman and the Late Antique periods. The assemblage is heterogeneous, and each chromatic group is composed of tesserae produced with different base glasses and colouring/opacifying techniques, suggesting diverse supplies. A small group of tesserae shows strict links to the Roman tradition in terms of both base glass and colouring/opacifying techniques and was probably obtained by re-using tesserae from older mosaics. Conversely, a larger group of tesserae shows textural and chemical evidence of recycling and indicates the prompt use of “new” opacifying technologies (such as the use of tin compounds) or uncommon technological solutions (such as the use of quartz and bubbles as opacifiers or the addition of metallurgical slags in red tesserae), suggesting a specific production in the fourth century AD.     

Micro-CT investigation of ostrich eggshell beads collected from Locality 12, the Shuidonggou site,China

Ostrich eggshell (OES) beads are an important kind of human ornaments, because their production reflects the development of modern human behavior, thinking ability, and cognitive level. Although the manufacture procedure of OES beads has been reconstructed in some Later Stone Age sites and early Neolithic sites, little information is known about detailed drilling technologies. In this study, synchrotron radiation micro-CT (SR-μCT) was firstly used to scan OES beads to understand microstructure, drilling marks, and perforation shape in a non-destructive mode. In contrast to other method to research drilling technologies, SR-μCT has a unique advantage that it could eliminate the influence of the adhering soils in a perforation in case that they are not easily removed. The results indicate that (1) SR-μCT could differentiate the eggshell species between Struthio camelus and Struthio anderssoni in terms of pore distribution. Compared to other destructive methods, including the anatomical method, DNA and protein analysis, the species identification through SR-μCT is non-destructive and faster; (2) the outer and inner surface of OES could be non-destructively judged according to OES microstructure, which would help infer the drilling direction; and (3) the perforation shape and drilling marks are distinct between the discontinuous twisting drilling and the multi-rotary drilling methods on the basis of replication experiments. According to these criteria, SR-μCT was applied to examine OES beads found in Locality 12 of the Shuidonggou (SDG) site in China, which were probably discarded in 1.1 k yr BP. The results show that most of ancient beads were firstly drilled from inside. According to the perforation shape and drilling marks, both the twisting drilling and the multi-rotary drilling method with different kinds of drill bits were used in working beads. Therefore, the people in SDG site mastered a few drilling technologies in the early Holocene, and the use of the multi-rotary drilling method reflects the technical development of ancient people. Up to our knowledge, it is the earliest known evidence of the application of the multi-rotary drilling method in China. Furthermore, this study will provide a new approach and important reference to understand drilling technologies of much older OES beads in the Later Stone Age or Upper Paleolithic Age.     

Mud-brick composition,archeological phasing and pre-planning in Iron Age structures: Tel ‘Eton (Israel) as a test-case

The eighth century BCE city at Tel ‘Eton (Israel) was destroyed by the Assyrian army, probably during Sennacherib’s campaign of 701. Building 101, sealed within the heavy conflagration caused by this destruction, was uncovered almost in its entirety on the top of the mound. From the beginning, it was apparent that the structure had two major building phases, and while its initial construction was of high quality, later additions were much inferior. Analyses of mud-brick walls for firing temperatures, texture, carbonate content, color, and dimensions approved the observation regarding the differences between the two phases, but consistently pointed out that one wall, initially attributed to the first phase, was analytically different, comprising an intermediate phase. This conclusion not only altered our understanding of the building construction, adding heretofore unknown building phase, but also gave us insights into the pre-planning of Building 101, indicating that some rooms had originally two doorways. Such a configuration allowed easy subdivision of spaces according to needs, without harming the overall structural stability. Differences in inner division of similar Iron Age houses were identified in the past and were attributed to differences in the life cycles of families. The evidence from Tel ‘Eton suggests that such future changes were taken into considerations when the structures were built.     

Non-destructive in situ analysis of polychromy on ancient Cypriot sculptures

The study focuses on the characterization of polychromy on limestone sculptures from Cyprus, attributed to the Cypro-Archaic—end of the Hellenistic periods. Polychromy components were identified by integrating digital microscopy, imaging under ultraviolet (UV) light, visible-induced luminescence (VIL), X-ray fluorescence spectroscopy (XRF) and fibre optics reflectance spectroscopy (FORS). Data acquisition was performed directly in exhibition rooms at the Cyprus Museum (Nicosia) and the Paphos District Archaeological Museum (Paphos). Among the identified materials, there are iron-containing (red, yellow, green) and copper-containing (green and blue) pigments. The precision of pigment identification by non-destructive techniques is discussed, and specific pigment names are proposed: red iron oxide, yellow iron oxide-hydroxide, green earth and Egyptian blue. Interesting results were obtained by VIL, which allowed identifying traces of Egyptian blue otherwise undetectable with the naked eye. Complementary, this study discusses advantages and problems of combined and separate use of portable XRF and FORS, raising the question of their complementarity and interchangeability for the purposes of pigment identification.     

Diet in transitory society: isotopic analysis of medieval population of Central Europe (ninth–eleventh century AD,Czech Republic)

Dietary behavior in the context of the formation of state structure, Christianization, and significant urbanization was studied, using the Great Moravian Empire (ninth–tenth century AD, Czech Republic) as a representative example. We also analyzed the impact of the disruption of social structure at the beginning of the tenth century and subsequent recovery of society during the eleventh century. Carbon and nitrogen isotopic values were measured in 189 adults (both sexes) and 74 animals representing different socioeconomic contexts (power centers/hinterlands) and chronology (Great Moravian/Late Hillfort period). Statistically significant differences in animal protein consumption were observed between centers and hinterlands. For centers, significant relationship was found between nitrogen isotopic values and socioeconomic status in males but not for females. Diachronic diet changes were observed, with the eleventh century diet characterized by higher millet consumption in both sexes and lower consumption of animal protein in males. These results confirm that Great Moravia represented a highly stratified society socioeconomically. Social status appears to determine the consumption of animal protein much more in males than in females. The diet of females also proved to be more uniform in the diachronic frame. The diachronic change in dietary behavior suggests that through the apparent recovery in the eleventh century, Moravian society did not reach its original level of welfare at least in terms of the quality of diet.     

Taxonomic reassignment of the Paleolithic human navicular from Cueva de los Torrejones (Guadalajara,Spain)

Evidence of human activity and hominin remains are very scarce inland on the Iberian Peninsula. This fact raises the issue of the scarcity of evidence that Paleolithic Homo sapiens occupied this area outside of the littoral margins (Atlantic, Cantabrian, and Mediterranean coasts). Here, we comparatively describe a human right adult navicular bone recovered in the Cueva de los Torrejones site, located in the village of Tamajón (Guadalajara, Spain). This fossil was preliminarily established as belonging to Homo cf. neanderthalensis, due to the late Pleistocene faunal association, mainly because of the presence of Crocuta crocuta and Panthera pardus. The metrical and morphological study of the navicular T93-S3.27 from Cueva de los Torrejones clearly differentiates it from Neandertals and their ancestors, the hominins from Sima de los Huesos, allowing for this fossil to be taxonomically assigned with confidence as H. sapiens. The navicular from the Cueva de los Torrejones is absolutely and relatively medio-laterally narrow with a low wedging index as those of fossil and modern H. sapiens, and clearly different of Neandertals. The increased discoveries and publications of new naviculars belonging to genus Homo, together with the findings of P. pardus and C. crocuta in more recent chronologies in the Iberian Peninsula, are compatible with this reevaluation. We propose a probable chronology for this fossil between 12 and 15 ka and ca. 25 ka, based on the biostratigraphy and the oldest presence of H. sapiens in the Iberian Peninsula. This work confirms the human presence within the Iberian Peninsula during the Upper Paleolithic and reopens the question of the peopling of the inner Peninsula during this period.     

Biological differences related to cultural variability during the Neolithic in a micro-geographical area of the Iberian Peninsula

This paper presents dental morphological data of Neolithic, Chalcolithic and Bronze Age populations from the Catalan Pre-Pyrenean area. The Neolithic group, in particular, differs from those of surrounding areas in its funerary culture: the building of cists, which is not present in the Sepulcres de Fossa Culture. A minimum number of 118 individuals from this area were studied for this work, and the data were compared with those of other Iberian and European groups. The results indicate that the two micro-regional groups from the Catalan area (Pre-Pyrenean and Pre-Coastal) were biologically different during the Neolithic and the Chalcolithic, but not in the Bronze Age, when they also appeared to be more homogeneous culturally. In addition, both areas differ biologically from coetaneous Italian groups, although those closer to the coast show slightly smaller differences. Finally, the Bronze Age groups also present fewer differences with regard to the Italian Bronze Age’s group. Therefore, the results suggest that the Catalan Neolithic population had two separate origins, related to cultural patterns, and that differences between the groups decreased within time, probably due to trade-related activities. Moreover, the fact that the difference with Italian populations decreased during the Bronze Age suggests major population movements through the Mediterranean that would affect the biological composition of the human groups.     

Skeleton decay of <Emphasis Type="Italic">Cervus elaphus hispanicus</Emphasis> carcasses in Mediterranean ecosystems: biostratinomy at Sierra Norte of Seville natural park (SW Spain)

Taphonomic studies of faunal assemblages from archaeological and palaeontological sites need biostratinomy research to endorse their results. Many papers have studied the relationship between the differential conservation of anatomical parts and the animal responsible for the deposits. In this paper, we present the biostratinomy results from 18 Cervus elaphus hispanicus carcasses (Hilzheimer 1909) in a Mediterranean ecosystem (the Sierra Norte Mountains in Seville Natural Park). We also describe the skeleton decay related to scavenger community, where Sus scrofa (Linnaeus, 1758) is maybe the most important bone scavenger in our study area. These results of this research were compared to those obtained from a similar study carried out in Doñana National Park (Huelva) and confirmed that post-mortem tendencies are similar in both ecosystems.     

New insights into Byzantine glass technology from loose mosaic tesserae from Hierapolis (Turkey): PIXE/PIGE and EPMA analyses

This study focuses on the Byzantine glass tesserae from Hierapolis (Phrygia, central Turkey). Fifty-seven samples of loose tesserae from two sites in the town (the theatre and the church of St. Philip) are analysed by particule-induced X-ray emission and particule-induced gamma ray emission and electron probe X-ray microanalysis to obtain the chemical composition and identify the colourants and opacifiers. The aims are to add new information to the scant knowledge of the Byzantine glassmaking technology, to constrain the chronology of the mosaics and to trace the supply routes of the tesserae. In the destruction layers of the theatre, tesserae produced following the Roman glassmaking technology (natron glass opacified by calcium and lead antimonate) were found. They were made using a Levantine 1 raw glass, generally attributed to the early Byzantine period (fifth to sixth c.). In the church, the samples attest a technological change from Roman tradition, and a complex pattern according to building history (two phases are attested, probably in the sixth and eighth to ninth c.), and a multiplicity of supply. Three glass types and some recipes not attested before in this chronological range for the production of tesserae are documented, such as the use of a local low-chlorine natron glass for the production of black and red tesserae, the blue colouring by a source of cobalt with zinc in a natron glass tessera and the opacification with tin oxide (both in a lead-free and in a high-lead natron glass), as well as with quartz.