Orientation of the Romanesque churches in the region of Val d’Aran,Spain (11th–13th centuries)

This study examines an ensemble of Romanesque churches in the region of Val d’Aran in the Spanish Pyrenees, built between the 11th and 13th centuries. Seven topographical studies performed between 2014 and 2015 examined these churches systematically using terrestrial laser scanning (TLS) as a data‐acquisition technique. The data obtained allowed for a geometrically accurate analysis of the orientation of these churches based on four Romanesque liturgies: Gemma animae (c.1120), by Honorius of Autun; Rationale divinorum officiorum (c.1150), by Jean Beleth; Mitralis de Officio (1190), by Sicard, Bishop of Cremona; and Prochiron, vulgo rationale divinorum officiorum (1291), by Guillaume Durand.     

NMR as a new tool for cultural heritage application: The provenance of ancient white marbles

Identifying the origin of marble used in antiquity brings back to light details of the economic, social and political organization of classical societies, and characterizing in depth the chemistry of marble is key to discovering its provenance. Beyond X‐ray diffraction, which could reveal the presence of discriminant secondary crystalline phases and the quantification of accessory minerals combined with a multivariate analysis approach, solid‐state nuclear magnetic resonance (NMR) enables one to recognize the local structure arrangement of both crystalline and amorphous materials by looking at one or more selected atoms. In present paper targets the ¹³C nuclide, and thus the major component of marble, calcium carbonate. Whatever their geological origin, marbles ¹³C‐NMR spectra present only one resonance corresponding to the carboxyl function whose intensity and line width vary from one marble to another. If the variation of the NMR signal intensity observed is the result of great T1 variations (from 220 to 5300 s) and is linked to iron content, the line width reflects defects in the calcite crystal in which calcium has been replaced by another element such as magnesium, aluminium or strontium. The specific profile of the NMR signal has been used successfully to help determine the origin of some archaeological items.     

Recycled Blessings: An Investigative Case Study of a Rewrapped Egyptian Votive Mummy Using Novel and Established 3D Imaging Techniques

This case study was the first of its kind, where neutron computed tomography (CT) was applied to a wrapped mummified animal. Conventional X‐ray CT was also used to allow for meaningful comparison, and complementary data for a comprehensive investigation. Previous applications of both techniques are limited to metallic objects, such as bronze Buddhas. The mummy used in this study (IA.2402) is dated between the Third Intermediate Period (1069–664 bce ) to Late Period (664–332 bce ) according to the wrapping style, and was originally believed to contain a complete skeleton of a feline. However, precise date and provenance were unknown. Our results prove the presence of only partial juvenile feline remains, and provide a date range for artefact creation (900–804 bce ± 30) and alteration (367–204 bce ± 30). Therefore, this study implements an established imaging technique (neutron CT) in a novel way, while preserving and conserving the intrinsic value of the artefact through non‐destructive investigation.     

Justification for reassessing elemental analysis data of ceramics,sediments and lithics using rare earth element concentrations and ratios

The mensuration of multi‐elemental concentrations from assorted archaeological materials has always required great care and attention to detail to ensure good‐quality data and their ensuing interpretations. Although most suspect data were generated before the wide use of computers, error‐free data are not still a certainty. This paper presents the geochemical rationale for a proposed chemical data‐assessment process, using a globally dispersed collection of ceramic, sediment and lithic data. It is argued that this process can allow archaeologists and archaeometrists to investigate systematically older and current data sets and, if need be, alter them to the reliable values they were originally intended to include.     

The technology and production of glazed ceramics from Middle Islamic Jerash,Jordan

Jerash in northern Jordan was, despite a focus on its classical heritage, also active in the Middle Islamic period, but little is known about actual developments during this period. This study represents the first study on the Middle Islamic glazed pottery from the site using scanning electron microscopy energy‐dispersive spectrometry (SEM‐EDS) and thin‐section petrography. The results show that two production traditions existed, each with different provenances. The local production is characterized by a non‐calcareous ceramic body and the use of a high‐lead glaze coloured with iron and copper oxides, whereas the turquoise‐glazed samples, likely imported from Mesopotamia, have a calcareous ceramic body and alkali or alkali‐lead glaze.     

The Finishing Technique of the Stone Monuments of Persepolis: Further Studies and New Findings Through the Use of Non‐Destructive Analytical Techniques

The studies on the finishing technique of the stone monuments in Persepolis (Iran) are part of the archaeological project jointly launched in 2008 by Iran and Italy, named ‘From Palace to Town’. The first experimental results, obtained on a very limited number of samples, revealed that the Achaemenid builders and sculptors used a white pigment, a kind of bone white, calcium fluorapatite, obtained by burning animal bones, to hide the dark grey colour of the stone. In order to verify these unexpected results, a new campaign was implemented to analyse a much larger number of samples. XRF spectrometry, a non‐destructive technique, was used and the experimental results were further elaborated by PCA. The presence of a white superficial layer was confirmed, and the use of fluorapatite was confirmed as well, but only on monuments attributed to the Xerxes period or later, while in the earlier monuments the white layer was obtained using gypsum.     

Mining Archaeology and Micro‐Raman Analysis Associated with ESEM‐EDX: Toward a Chrono‐Spatial Definition of Ore Consumption in a Pyrenean Medieval Workshop, 14th–16th Centuries

The rapid expansion of non‐ferrous metallurgy in the late Middle Ages (14th–15th centuries) enhanced ore demand, which was supported by mining intensification. Metallurgical workshops developed various supply strategies based on geological, political and economic constraints. This is particularly true for the Pyrenean multi‐metals workshop of Castel‐Minier (Ariège, France), where recent excavations unearthed an exceptional corpus of non‐ferrous ores. A specific analytical methodology combining micro‐Raman spectroscopy and environmental scanning electron microscopy with energy dispersive X‐ray (ESEM‐EDX) was set up to study these artefacts. This composite methodology permitted the fast characterization of both mineral and gangue as well as a discussion of their economic potential. Ores identified were compared with ancient mines in neighbouring mining districts in order to sketch a geography of the mineral resources available to medieval metallurgists. Moreover, a chrono‐stratigraphic study of ore distribution in Castel‐Minier revealed the supply strategies, technological choices as well as spatializing of copper and lead metallurgies.     

Non‐Destructive Survey of Early Roman Copper‐Alloy Brooches using Portable X‐ray Fluorescence Spectrometry

This paper argues that portable X‐ray fluorescence spectrometry (pXRF) is a suitable elemental measurement technique to study the production of copper‐alloy artefacts. However, rather than try to imitate the accuracy and precision of laboratory techniques, it is more beneficial to deploy it in a survey role, one that attempts to model chronological and geographical changes within large quantities of artefacts. To achieve this, it was investigated to what extent corrosion and the issues surrounding surface measurements affect the potential of this type of research. Analyses on early Roman period brooches gathered in the Nijmegen region of the Netherlands were subsequently compared with published data.