Formation of Fluid Inclusions during Heat Treatment of Barremo‐Bedoulian Flint: Archaeometric Implications

At the end of the fifth millennium bc , the development of a specialized lithic industry in the Chassey societies of south‐eastern France and its dissemination as far as Catalonia and Tuscany attest to important socio‐economic changes in the Mediterranean Neolithic societies. The lithic production was made on barremo‐bedoulian flint that was heat‐treated to improve the sharpness of the tools produced. Microscopic observations of archaeological and geological, heated and unheated barremo‐bedoulian flint samples allowed us to highlight the heat‐induced formation of fluid inclusions. Microthermometry analyses showed that these inclusions contain pure H₂O, most probably resulting from the dehydration of length‐slow (LS) chalcedony and the closure of narrow pores, according to the model proposed by Schmidt et al. ( 2012 ). Our results enable us to estimate the heating temperatures used by Chassey artisans to ≈ 230°C. We also propose the ‘pressure cooker’ model to explain the migration of liquid water in flint nodules heated to 230°C. Then, we discuss the ability of a particular type of flint to be heat‐treated, and hence its value for Neolithic society, which depends on: (1) the amount of LS chalcedony that ensures the water release at relatively low temperature; and (2) on the total volume of porosity available to store the dehydration water.     

Well preserved non‐collagenous extracellular matrix proteins in ancient human bone and teeth

Ancient bones in a good preservation state, ascertained by microscopic techniques, conserve extracellular matrix proteins over thousands of years. With new techniques, intact extracellular matrix proteins from ancient bones and teeth are extracted and separated by one‐dimensional and two‐dimensional electrophoresis. Proteins were identified in Western blots by special antibodies against different human extracellular matrix (ECM) molecules of bone. We have confirmed different types of ECM human bone molecules such as osteonectin, osteopontin, and alkaline phosphatase with specific antibodies in human bone samples from different age groups. Additionally, we selected bone samples from different cultural time periods, such as the Middle Ages, the Bronze Age and the Late Pre‐Pottery Neolithic Phase (PPNB), and teeth from individuals from the Early Middle Ages and from the Late PPNB. The survival of intact extracellular matrix proteins in ancient bones and teeth dating from recent times to the Late PPNB, and reliable techniques to identify these proteins, present a great challenge to further research. A Match Set with PD‐Quest 7.2 shows that only 16% of protein spots in the teeth are also found in the bone of the same individual. In combination with the results of macro‐ and microscopic investigation, biochemical techniques will help us in obtaining a better understanding of bone and teeth in health and disease. Copyright © 2006 John Wiley & Sons, Ltd.     

The MSA sequence of Diepkloof and the history of southern African Late Pleistocene populations

This paper presents the first multidisciplinary synthesis of the Middle Stone Age sequence of Diepkloof Rock Shelter (South Africa). We explore the main cultural changes that characterized southern African hunter–gatherer societies from OIS 5 to the beginning of OIS 3. We discuss the tempo of these changes, test the current interpretative hypotheses and explore an empirical model to explain the early appearance of symbolic marking within the Pleistocene hunter–gather societies of southern Africa.     

Optical dating of alluvial deposits at the orogenic front of the andean precordillera (Mendoza,Argentina)

Well constrained numerical ages of alluvial fan sediments are key to understanding the chronology of alluvial episodes and tectonic activity at the front of the Andean Precordillera. We tested the application of radiocarbon and optically stimulated luminescence (OSL) dating in the distal part of an alluvial fan five kilometers north of Mendoza. For OSL dating a large number of aliquots (n > 70) — each composed of ∼50 quartz grains — were measured in order to obtain reliable burial ages despite scattered dose distributions. Owing to a feldspar contamination in all samples, an infrared stimulation was inserted before each OSL measurement, which reduced the feldspar OSL signal successfully. By using the minimum age model we obtained stratigraphically consistent burial ages of alluvial deposits in a depth profile. The uppermost ∼1 m of sediment is composed of debris flow deposits buried 770±76 years ago. Three plant remnants used for radiocarbon dating from the same layer, however, yielded ages younger than 350 years, which are interpreted to underestimate the depositional age. Underneath the debris flow, a major unconformity cuts a series of distal alluvial fan sediments with interstratified floodplain deposits, which are composed of sandy and calciterich silt layers, respectively. Three samples from this unit which were distributed over one meter of sediment thickness yielded statistically concordant OSL ages of 12.3±1.2 ka, 12.3±1.2 ka, and 11.7±1.1 ka. The deposition of these sediments during the latest Pleistocene coincides with a phase of cool and humid climate, which occurred before the alluvial fan propagated farther into the foreland. The overlying debris flow sediments are associated with alluvial fan incision during the arid Late Holocene.     

Reviews

THE RELEVANCE of ‘closure theory’ to archaeology is discussed, and it is argued that the role of material culture in shaping medieval group identities was enhanced by taxation on movable property during the 13th century. Emphasis on monetary value led to concepts of ranking expressed in sumptuary laws and the use of symbols in late medieval contractual society.