Stability of IRSL signals from sedimentary K-feldspar samples

Recent work has identified IR stimulated luminescence signals at elevated temperature from both potassium- and sodium-rich feldspars that have much lower anomalous fading rates than the conventional signal measured using IR stimulation at 50°C. This paper examines the stability of these signals for potassium-rich sedimentary feldspars. We show that the natural post-IR IRSL (pIRIR) signal from a 3.6 Ma old sample is in apparent saturation on a laboratory generated dose response curve, i.e. it does not show detectable fading in nature although a low fading rate is observed on laboratory time scales. We show that the pIRIR signal has a greater thermal stability than the IRSL signal and that the trend in increasing thermal stability is mirrored by a decreasing fading rate. We also investigate the effect of preheat temperature and IR stimulation power on the decay shape and conclude that the data can be explained in terms of either a single- or multiple-trap model. We present evidence that may suggest that at least part of pIRIR signal is derived from a high temperature trap (∼550°C thermoluminescence (TL) peak), although again the data can also be explained in terms of a single-trap model. Finally, we present dose response curves and characteristic curvature constants (D₀) values for various IRSL signals and conclude that the more stable signals saturate more quickly than the less stable signals and that the initial and final signals saturate at approximately the same level.     

Holocene marine ingressions in the coastal zone of the pomeranian bay based on radiocarbon assays

In recent years, a team at the Geology and Paleogeography Unit, Marine Sciences Institute, University of Szczecin, has been performing geological, geochronological and paleogeographic surveys in (i) the Szczecin Lagoon and Świna Gate Sandbar and (ii) the estuary section of the Rega river valley near Mrzeżyno. These studies have helped to examine and identify not only the distribution of fossil marine sediments but also their lithological and sedimentological characteristics. The age of marine ingressions and regressions in the coastal zone of the Pomeranian Bay were determined using approximately 170 radiocarbon assays.     

Surface dating by luminescence: An overview

Daylight radiation resets luminescence ‘clock’ to zero on rock surfaces, but transmission depends on the transparency of the rock. On burial, surfaces are no longer exposed to daylight and accumulation of trapped electrons takes place till the excavation. This reduction of luminescence as a function of depth fulfils the prerequisite criterion of daylight bleaching. Thus rock artefacts and monuments follow similar bleaching rationale as those for sediments. In limestone and marble, daylight can reach depths of 0.5–1 mm and up to 16 mm respectively, while for other igneous rocks e.g. quartz in granites, partial bleaching occurs up to 5mm depth under several hours of daylight exposures and almost complete beaching is achieved in the first 1 mm within about 1 min daylight exposure. The ‘quartz technique’ for limestone monuments containing traces of quartz enables their dating with Optically Stimulated Luminescence (OSL) techniques. The surface luminescence (thermoluminescence, TL or OSL) dating has been developed and further refined on various aspects of equivalent dose determination, complex radiation geometry, incomplete bleaching etc. A historical review of the development including important applications, along with some methodological aspects are discussed.     

Infrared radiofluorescence (IR-RF) dating of middle pleistocene fluvial archives of the Heidelberg Basin (Southwest Germany)

The infrared radiofluorescence (IR-RF) dating technique was applied to eight fluvial samples that were collected from two sediment cores at the Heidelberg Basin located near Viernheim and Ludwigshafen in southwest Germany. Based on the IR-RF derived ages of the samples it was possible to establish a chronological framework for the Mid-Pleistocene fluvial deposits of the Heidelberg Basin. The results allow us to distinguish between four main periods of aggradation. The lowermost sample taken from 100 m core depth lead to an IR-RF age of 643 ± 28 ka pointing to a Cromerian period of aggradation (OIS 17–16). For the Elsterian it is now possible to distinguish between two aggradation periods, one occurring during the Lower Elsterian period (OIS 15) and a second during the Upper Elsterian period (OIS 12–11). For the so called Upper interlayer (or “Oberer Zwischenhorizont” — a layer of organic-rich and finer-grained deposits), the IR-RF results point to a deposition age of around 300 ka, with samples taken directly on top and out of this layer yielding IR-RF ages of 288 ± 19 ka and 302 ± 19 ka, respectively. Hence, the measured IR-RF ages clearly point to a deposition during the Lower Saalian period (OIS 9–8) whereas earlier studies assumed a Cromerian age for the sediments of the Upper Interlayer based on pollen records and also mollusc fauna. The new IR-RF dataset indicates that significant hiatuses are present within the fluvial sediment successions. In particular the Eemian and Upper Saalian deposits are missing in this part of the northern Upper Rhine Graben, as the 300 ka deposits are directly overlain by Weichselian fluvial sediments. It is obvious that time periods of increased fluvial aggradation were interrupted by time periods of almost no aggradation or erosion which should have been mainly triggered by phases of increased and decreased subsidence of the Heidelberg Basin.     

The thermoluminescence of meteorites: A brief 2010 perspective

Early work on meteorite thermoluminescence, influenced by pottery dating and dosimetry applications, demonstrated a relationship between natural thermoluminescence and (1) the orbital perihelion of a meteorite and (2) the terrestrial age (time since fall) of a meteorite. For 14 years natural TL measurements were routinely made on newly recovered Antarctic meteorites to help identify unusual thermal and radiation histories, and to sort them by terrestrial age and perihelion. Two examples of the value of such data are presented, an Antarctic meteorite that underwent a major orbit change prior to fall and the collection mechanics of meteorites at the Lewis Cliff collection site. A second major area of focus for meteorite TL, that has no non-meteorite heritage, is the use of their induced TL to provide an extraordinarily sensitive and quantitative means of exploring metamorphic intensity and palaeothermometry. While especially valuable for unequilibrated ordinary chondrites, these types of measurement have proved useful with virtually every major class of meteorite, asteroidal and planetary. The challenge now is to extend the technique to small particles, micrometeorites, interplanetary dust particles, and cometary particles.     

Geological importance of luminescence dates in Oman and the Emirates: An overview

In the Wahiba Sands of eastern Oman, luminescence dating of sands enables us to relate wind activity to climatic variations and the monsoon cycle. These changes resulted from Polar glacial/interglacial cyclicity and changes in global sea levels and wind strengths. Luminescence dates show that development of the Sands began over 230 ka ago when the sand-driving winds were the locally arid, northward-blowing SW Monsoon.     

Expectations of scatter in equivalent-dose distributions when using multi-grain aliquots for OSL dating

In the OSL dating of sediment, the scatter in equivalent dose (D _e) between grains is almost always larger than would be expected due to counting statistics alone. Some scatter may be caused by insufficient (partial) bleaching of some of the grains prior to deposition. In order to date partially bleached sediment, it is essential to estimate the amount of scatter caused by other processes (e.g. grain-to-grain variability in the natural dose rate). Measurements of such scatter are performed at the single-grain level; by contrast, most OSL dating is performed on multi-grain subsamples, for which grain-to-grain scatter is reduced through averaging.     

Traditional post-harvest processing to make quinoa grains (<Emphasis Type="Italic">Chenopodium quinoa</Emphasis> var. <Emphasis Type="Italic">quinoa</Emphasis>) apt for consumption in Northern Lipez (Potosí, Bolivia): ethnoarchaeological and archaeobotanical analyses

The aim of this paper is to generate information to assist in the archaeobotanical recognition of post-harvest processing activities related with different enhancement and consumption patterns of quinoa in the Central Andes. Enhancement of the grains involves what local people call “mejorado de los granos”. Their main purpose is to reduce as far as possible the presence of saponins, a toxic metabolite, in the grain. Ethnobotanical data were recorded in the village of Villa Candelaria (Southern Bolivian highlands) through the application of standard ethnographic techniques. The types of grain enhancement vary depending on the meal that people want to prepare. We registered three different quinoa enhancements based on intended consumption, (1) as a whole seed, (2) in soups or (3) as pitu (a kind of toasted refined flour). Laboratory analysis aimed at identifying distinctive features of grains in different processing stages, as well as evaluating the effects of charring. For both desiccated and charred remains, quinoa processed for pitu can be distinguished from that for whole seed/soup. As a case study, archaeological grains of the pre-Inka site of Churupata, located 3 km from Villa Candelaria, were interpreted as quinoa prepared for consumption as whole seed/soup.     

Collagen fingerprinting of archaeological bone and teeth remains from Domuztepe,South Eastern Turkey

We applied a recently developed method of collagen peptide mass fingerprinting for taxonomic identification in faunal remains to 111 specimens from the Neolithic site of Domuztepe in southeastern Turkey. Advances on the published technique allow us to move beyond the key domesticated fauna (sheep, goat, pig and cattle) to include non-domesticates (deer and gazelle, as well as humans). As the animal economy of Domuztepe was dominated by domestic sheep and goats, a large number of the samples tested were morphologically indistinguishable sheep/goat remains. A number of samples represented elements that provide information on age (i.e., mandibles) or sex (pelvis); thus, this represents the first major study to attempt to improve kill-off profiles using collagen fingerprinting. We also show that the collagen extracted from dentine is equally amenable to the proposed methodology as bone collagen.     

Stratigraphic and spatial variability in shell middens: microfacies identification at the ethnohistoric site Tunel VII (Tierra del Fuego,Argentina)

Based on ethnographic accounts from the eighteenth to the twentieth century, functional areas have been identified within Fueginian shell middens. In this context, archaeological microfacies acquire a functional meaning when the microscopic record is compared to information gathered from ethnology, macroscopic observations made during excavation, and experimental modern analogues. All these lines of evidence were combined for the first time at Tunel VII, an eighteenth/nineteenth century shell midden occupied repeatedly by Yamana people, the last hunter–gatherer–fisher groups of the Beagle Channel. The sampling strategy involved three sets of samples: (1) two stratigraphical columns taken from the hut “entrance” and from a portion of the shell midden (i.e., the surrounding refuse shell ring), (2) thin sections from five hearths representing successive phases of frequentation of the hut, and (3) experimental burnt valves of Mytilus edulis, the main malacological component of the site. Comparison of microfacies from groups (1) and (2) provided microscopic indicators to distinguish between shell dumping areas and occupation surfaces. Comparison of microfacies within columns from group (1) allowed recognizing periods of site abandonment and periods of more intense/longer site frequentation. The experimental samples from M. edulis served as a reference to characterize the five central hearths in terms of maximum burning temperatures reached. Different burning structures were correlated to the season of hut frequentation and to their location (and function) within different portions of the hut. The intra-site micromorphological comparison strategy within a well-documented ethnohistorical context provides valuable indicators for the identification of functional areas in archaeological contexts when ethnographical information is not available.