Thermal and Petrographic Characterization of Herculaneum Wall Plasters

Roman plasters sampled from different houses at the archaeological site of Herculaneum, Italy, (2010–12) were studied by means of petrography, thermal analysis and X‐ray fluorescence. Herculaneum plasters are composed by preparatory layers (arriccio) with a thickness of several centimetres and are based on a calcitic binder and volcanic scoriae as aggregates, covered by a thin final layer characterized by a low granulometry. Most of the sampled plasters can be placed into two groups based on the aggregate composition and classified as marmorino or intonachino. However, a similar aggregate composition did not induce superimposable thermal behaviour, thus suggesting that the samples underwent different ageing/weathering processes, with a consequent change of the ratio among the components.     

1500 Years of Pottery: Neutron Activation Analysis of Northern Chilean Domestic Ceramics from Caleta Vitor and Clay Samples from Nearby Valley,Coast and Highland Contexts

This paper presents the findings arising from neutron activation analysis (NAA) of northern Chilean domestic ceramic samples from Caleta Vitor (n = 38) and clay samples (n = 15) from nearby valley, coast and highland contexts. This study presents the first NAA data set of ceramics spanning a temporal period of 1500 years (c.2000 to c.476 bp ) from the Vitor Valley as well as the first attempt to use NAA to characterize potential clay sources in the region. On the basis of this study, we argue that the majority of domestic ceramics from Caleta Vitor share compositional similarities with clay samples collected from nearby valleys, allowing us to infer that the Caleta Vitor populations primarily procured their clay for domestic ceramics from local sources throughout a 1500‐year period. Thus, despite the fact that there were inter‐regional interactions during this period that included the influence of powerful Andean polities, it would appear that domestic ceramics continued to be produced locally, and by implication it can be argued that such interactions did not substantially affect this sphere of material culture production. Further, the apparent continuities in domestic ceramic production allow us to reflect on local decision‐making processes throughout the cultural phases considered in this research.     

Ancient ‘Black’ Decorative Stones and the Ephesian Origin of Sculptural bigio antico

Isotopic, EPR and petrographic studies aimed at establishing the provenance of sculptural bigio antico are reported, including 18 possible quarry sites and 21 ancient sculptures. The results demonstrate that the Belevi quarry, north‐east of Ephesos, above the more famous white marble quarry, was the major source of this marble. Nineteen artefacts belong to Belevi, whereas the precise origin of the remaining two is unknown, but must probably be found within the same area. The peculiar distribution of δ¹³C values both for Belevi and artefacts was crucial for inferring the correct provenance, subsequently confirmed by additional analytical and petrographic data.     

First Evidence Of The Use Of Freshwater Pearls As A Cosmetic In Ancient China: Analysis Of White Makeup Powder From A Northern Song Dynasty Lv Tomb (Lantian,Shaanxi Province,China)

The Lv family tombs in Lantian, Shaanxi Province are one of the most important archaeological sites of China in recent years, providing numerous objects and a wealth of information for the study of the history of the Northern Song dynasty. There were a large number of exquisite cultural relics unearthed from the tombs, including one porcelain box containing white powder, which was identified as women's makeup. The phase composition, microstructure, thermal properties and characteristics of the trace elements in the unearthed white cosmetic powder were comprehensively analysed by X‐ray diffraction (XRD), scanning electron microscopy (SEM), differential scanning calorimetry – thermogravimetry (DSC–TG), Fourier transform infrared (FT–IR) microscopy and inductively coupled plasma atomic emission spectroscopy (ICP–AES). The white makeup powder was determined to be a product made from high‐quality freshwater pearls. These results, for the first time, showed evidence that freshwater pearl powder was used as a cosmetic in ancient China using archaeological objects, providing scientific evidence and new clues to enrich and expand research into the ancient Chinese cosmetic materials.     

Fuel For Lamps: Organic Residues Preserved in Iron Age Lamps Excavated at the Site of Sahab in Jordan

Five Iron Age ceramic lamps from a tomb at the site of Sahab in the south‐eastern part of central Jordan were analysed using gas chromatography – mass spectrometry (GC–MS). The results of this study provide data on the type of fuel used in three of these lamps. The study proposes that animal fat, possibly of ruminant origin, was used in three Early Iron Age II lamps. The material used in the other two Iron Age I lamps could not be determined due to the absence of diagnostic biomarkers. The data obtained from the lamps can be put in conjunction with the archaeological evidence on the availability of domestic animals and, most probably, use of their products at the site of Sahab during the Iron Age.     

A Pigment Characterization Approach to Selection of Dating Methods and Interpretation of Rock Art: The Case of the Mikinak Site,Lake Wapizagonke,Quebec, Canada

Dating is perhaps the most frequently asked question in rock art studies, but still one of the most difficult to answer. However, chronology is vital in order to understand and interpret rock art sites. Unfortunately, attempts at dating the Mikinak site, at Lake Wapizagonke, Quebec, Canada were unsuccessful. But a multi‐instrumental protocol applied to characterize paintings shows that at least three different paint recipes were employed to create the site. These may reflect three different phases of paintings, and that at least three different artists contributed to the production of this site.     

Compositional Analysis of Ceramics from Goguryeo Fortified Sites in Central Korea

The aim of this paper is to investigate whether the ceramics from the Goguryeo fortified sites of the Han River region in central Korea were manufactured and consumed locally during the southern expansion of the Goguryeo State (475–551 ce ). For this research, 88 ceramic samples from seven contemporary sites in the southern territories of Goguryeo were sampled and analysed by ceramic thin‐section petrography and neutron activation analysis (NAA). In addition, to establish a possible chemical fingerprint at Hongryeonbong Fort 2, five clay specimens were also gathered and analysed from the pottery firing structure. The results of this analytical study indicate that the majority of the ceramics from the Goguryeo fortified sites of central Korea were produced and circulated within this newly acquired region. In addition, it is highly probable that Hongryeonbong Fort, which contains the remains of what may be ceramic firing architecture, is the place of production for the ceramics.     

The White Marble of the Arch of Augustus (Susa,North‐Western Italy): Mineralogical and Petrographic Analysis for the Definition of its Origin

The Arch of Augustus in Susa (north‐western Italy) was built in 9–8 bc by King Cottius, to celebrate the treaty between the Romans and the Gauls. It is made of white marble, which was considered for a long time to be locally extracted, but no archaeometric studies have been performed up to now. Therefore, a multi‐analytical study based on petrographic (optical and scanning electron microscopy), electron microprobe and stable isotope analyses was carried out on the marble from the arch and from reference samples, with the aim of defining the provenance. All the data confirmed that white marble belonging to the metamorphosed carbonate cover of the Dora Maira Massif, known as Foresto marble, was used for the Susa Arch. This choice was probably made for economic reasons, but also due to the relative independence of the ruling family of the Alpes Cottiae, which was obviously interested in promoting a local marble.     

A Rock‐Magnetic Quest for Possible Ore Sources for the Ancient Iron‐Smelting Industry in the Olkhon Region (Lake Baikal,Siberia)

Rock‐magnetic techniques were used to examine the topsoil layer of Kurma archaeological site (in the Olkhon region, on the north‐western coast of Lake Baikal, Siberia) in an effort to determine the possible sources of iron ores for iron‐smelting centres (at about the bc /ad boundary). Measurements have shown a magnetic enhancement of the topsoil due to magnetite grains resulting from weathering of strongly magnetic crystalline rocks. They have also revealed a preliminary picture of the distribution of strongly magnetic topsoils around the ancient iron‐smelting centres. Perhaps, in addition to traditional sources of raw materials, the ancient metallurgists used black sand talus as an ore deposit.