Flint and Quartzite: Distinguishing Raw Material Through Bone Cut Marks

Since the 1980s, several experimental analyses have been able to differentiate some lithic tool types and some of their raw materials according to the morphology of cut marks imprinted by such tools when used for butchering activities. Thus, metal tool use has been differentiated in contexts with an abundance of lithic tools, or even the use of hand axes has been documented in carcass processing, in contrast with simple unretouched or retouched flakes. As important as this information is, there are still other important aspects to be analysed. Can cut marks produced with different lithic raw material types be differentiated? Can cut marks made with different types of the same raw material type be characterized and differentiated? The objective of this study is to evaluate if cut marks resulting from the use of different flints and different quartzites are distinguishable from each other. In the present work, an experimental analysis of hundreds of cut marks produced by five types of flint and five varieties of quartzite was carried out. Microphotogrammetry and geometric–morphometric techniques were applied to analyse these cut marks. The results show that flint cut marks and quartzite cut marks can be characterized at the assemblage level. Different types of flint produced cut marks that were not significantly different from each other. Cut marks made with Olduvai Gorge quartzite were significantly different from those produced with a set comprising several other types of quartzites. Crystal size, which is larger in Olduvai Gorge quartzites (0.5 mm) than Spanish quartzites (177–250 μm), is discussed as being the main reason for these statistically significant differences. This documented intra‐sample and inter‐sample variance does not hinder the resolution of the approach to differentiate between these two generic raw material types and opens the door for the application of this method in archaeological contexts.     

Flint procurement strategies in the Late Lower Palaeolithic recorded by in situ produced cosmogenic 10Be in Tabun and Qesem Caves (Israel)

The in situ produced cosmogenic beryllium isotope, ¹⁰Be, in flint artifacts from different layers in prehistoric caves can provide information on flint procurement. The buildup of ¹⁰Be in a flint matrix is related to the exposure time of the flint to cosmic rays. Although this exposure history can be complex, the ¹⁰Be content of flint assemblages can show whether the raw material was obtained from shallow mining and/or surface collection as opposed to sediments two or more meters below the surface. Flint artifact assemblages from two Palaeolithic caves in Israel, Tabun and Qesem, were analyzed.In Tabun cave the flint artifacts from Lower Layer E (Acheulo-Yabrudian, around 400 000–200 000 yr) contain very small amounts of ¹⁰Be, which is consistent with flint procured from sediments two or more meters deep. Artifacts from above and below Tabun Lower Layer E show a more complex distribution, as do artifacts from all layers of Qesem cave (Acheulo-Yabrudian). This is probably due to the fact that they were surface collected and/or mined from shallow (less than 2 m) depths. We show here that artifact assemblages have different concentrations of ¹⁰Be, indicating different raw material procurement strategies.     

An investigation of the fractal properties of flint microwear images

This paper reports on an investigation into the fractal dimensions of flint microwear images which has been carried out in an attempt to resolve the existing controversy over the possibility of identifying microwear types from visual inspection of high magnification images, and describes a new method for flint microwear image analysis based on fractal geometry. Fractal dimensions of surface images, which are known to relate well to human visual perception of roughness, have been computed for various types of microwear. No significant correlations have been found between the fractal properties of the digital flint images and the contacted materials.     

What causes failure (overheating) during lithic heat treatment?

Heat treatment of lithic raw material, i.e. the intentional alteration of silica rocks for improving their knapping quality, is a process that may require great care and precisely controlled conditions in order to avoid failure due to overheating. The physical causes of overheating remain poorly understood leading to problems in the interpretation of heat-treated artefacts and/or fire-related taphonomic alteration of different types of silica rocks. This driving force of overheating is investigated by a set of experimental heat treatment sequences with different ramp rates and different volumes of flint with a well-defined mineralogical composition, porosity and water content. The results of this experiment show the main cause of heat-induced fracturing to be the vapour pressure in fluid inclusions within the rocks. Heterogeneous thermal expansion could be discarded. The interdependence between volume and heating rate is also shown. These results have implications for the study of archaeological heat-treated rocks, the understanding of taphonomic heat-induced fracturing of silica rocks and experimental flint knapping.     

Heat treatment of Polish flints

In Poland three types of flint (chocolate, spotted and banded) were intensively mined from the Terminal Palaeolithic to the Early Bronze Age. Although heating of flint to improve its flaking properties was practised across the world from ∼110,000 years ago to the recent, particularly in southwestern Europe, heat treatment of flint in Poland is known from only two sites.     

POWER AND INFLUENCE IN THE LATE STONE AGE. A DISCUSSION OF THE INTERPRETATION OF THE FLINT DAGGER MATERIAL

Summary. In this study, the flint daggers in three areas on the Swedish West Coast are used to show the connection between powerful and influential groups and warlike activities. The variations within the flint dagger material are interpreted in terms of social status and the current flint dagger typology is rejected.     

Raw stone material supply for Upper Pleistocene settlements in Sierra de Atapuerca (Burgos,Spain): flint characterization using petrographic and geochemical techniques

Microscopy, mass spectrometry and X-ray diffraction methods were used to analyse 415 samples of natural and archaeological flint from Sierra de Atapuerca (Burgos, Spain) in order to define the different types from Neogene and Cretaceous formations in the study area, infer their genetic context and ascertain the supply sources used by hunter-gatherers who exploited this area in the Upper Pleistocene. A statistical classification model was also designed using linear discriminatory analysis and support vector machines which permitted the differentiation of the flint on an age basis.     

FLINT PROCUREMENT AND NEOLITHIC AXE PRODUCTION ON THE SOUTH DOWNS: A RE-ASSESSMENT

Summary. This paper reviews the evidence for Neolithic flint axe production on the South Downs in the light of recent chemical analysis of axes and the author's own research involving surface flint collections. The organisation, status and chronology of the Sussex flint mines is discussed and the distribution of flint axes described. Late Neolithic/Early Bronze Age settlement is shown to concentrate on the clay-with-flints which is also a major flint source. It is argued that the production of axes from mined flint was replaced by utilisation of surface deposits in the later Neolithic and case studies are presented.     

PREHISTORIC FLINT MINES AND THEIR IDENTIFICATION AS SOURCES OF RAW MATERIAL

This paper is a statistical and geological study of the results of analysis of flint from British and West European flint mines, carried out by emission and atomic absorption spectroscopy. Groups of flint specimens were studied from each geographically separate flint mining area. Flints were analysed for a group of easily measured trace elements shown by previous work to be generally present. The ratios between the trace elements form a consistent pattern for each flint mine and statistically valid differences of pattern can be recognized between different flint mines. A geological investigation shows that the measured trace elements may be derived from clay minerals and explains geographical and statistical variation in the composition of flint in terms of its mode of origin in the chalk. An advanced statistical technique allows individual flint specimens of unknown origin to be attributed by their composition to one or other of the identified flint sources. The archaeological implications of this study are discussed.     

PAUL‐LOUIS CYFFLÉ'S (1724–1806) TERRE DE LORRAINE: A TECHNOLOGICAL STUDY

Fragments of four Terre de Lorraine biscuit figurines were subjected to porosity analysis, X‐ray fluorescence analysis, X‐ray diffraction analysis, backscattered‐electron image analysis—coupled with energy dispersive spectrometry—and electron backscatter diffraction analysis to determine the porosity, bulk, major, minor and trace element compositions, and the composition and the proportion of their constituent phases. Cyfflé's Terre de Lorraine wares embrace two distinct types of paste, a calcareous and an aluminous–siliceous one. Both are porous (9–25% water adsorption). The former consists of a mixture of different proportions of ground quartz or calcined flint, ground Pb‐bearing glass and calcium carbonate with a refractory clay. The firing temperature was between 950 and 1050°C. For the latter, Cyfflé mixed ground pure amorphous SiO₂, ground quartz or calcined flint, ground porcelain, ground Na–Ca‐glass and coarse‐grained kaolinite with a fine‐grained kaolinitic clay. The figurines were fired below 1000°C. The result was a porous, hard paste porcelain‐like material. Cyfflé's recipes for both pastes can be calculated from the chemical and the modal analyses.     

MICROSTRUCTURE OF FLINT AND OTHER CHERT RAW MATERIALS*

The crystallite size, microstrain, stacking disorder and moganite content of flint and other chert raw materials were studied by X‐ray powder diffraction profile analysis. The broadening of the X‐ray reflections of all microfibrous quartz varieties is due to both anisotropic small crystallite size and anisotropic microstrain. The microstructure varies for samples of different origin. The moganite content and the number of structural defects are higher in flint than in older chert and petrified wood. The X‐ray diffraction pattern of the cortex of flint differs from that of the core material, whereas those of the patina and the unweathered interior of the rocks do not.     

Microwear study of quartzite artefacts: preliminary results from the Middle Pleistocene site of Payre (South-eastern France)

Preliminary functional results obtained from the quartzite assemblage of the Early Middle Palaeolithic site of Payre (South-eastern France) are presented. In an area rich in flint, hominins at Payre also collected quartzite in their local environment, specifically along the Rhône River banks. Although the Payre lithic assemblage is largely composed of flint, quartzite was introduced in the site mainly as large cutting tools knapped outside. This fact pointed out an apparently highly differential treatment of the raw material types available in the region. A major concern is to understand the reason why. Is there any functional reason for the introduction of those artefacts, perhaps to perform specific activities related to the toughness of quartzite? Or is there any functional differentiation among the various raw materials? Use-wear analysis is a useful tool for better understanding human technological choices and strategies of lithic raw material management. Before attempting to extensively apply use-wear analysis on the quartzite assemblage, we analysed a limited sample to evaluate the general surface preservation. A specific experimental programme with the same local quartzite was carried out in order to provide a reliable comparative reference for interpreting use-wear evidence on archaeological implements. Methodological difficulties related to use-wear analysis applied to quartzite artefacts are also discussed. Both Optical light microscopy (OLM) and Scanning Electron Microscopy (SEM) were employed in this study; however, interpretations were elaborated considering principally SEM micro-graphs.The analysis of the archaeological material showed a good state of preservation of the surfaces with a low incidence of post-depositional alterations. The documented use-wear allowed us to identify the active edges, the kinematics and, more rarely, the worked material. Chopping activities were documented on two large artefacts suggesting a specific utility of those tools.     

Debitage variability among multiple flint knappers

Five flint knappers produced both multidirectional cores and early stage bifaces. The debitage assemblages were compared to evaluate if, and to what degree, the debitage created by one flint knapper varies from that of other flint knappers. The debitage from these reduction episodes was then analyzed with commonly used and replicable debitage attributes. Each knapper was evaluated in terms of his/her individual consistency, and the debitage produced was tested for each ratio scale debitage attribute to ensure that the variability found between knappers was not a product of variation within the assemblages of the individual knappers. The debitage from the individual flint knappers was found to be highly variable between knappers for both technologies.     

Heat treatment in the South African Middle Stone Age: temperature induced transformations of silcrete and their technological implications

It was recently found that silcrete raw material was heat-treated during the South African Middle Stone Age (MSA) for altering its flaking properties. This finding led to hypotheses about the implications for the MSA hunter-gatherers such as the cost of thermal treatment in terms of investment and firewood. To date, these hypotheses lack a solid basis, for data on the thermal transformations of South African silcrete and, hence, the necessary heating procedure and heating environment, is missing. In order to produce such data, we conducted an experimental study within the framework of the Diepkloof project. This work is based on the petrographic, mineralogical and structural analysis of South African silcrete from the West Coast and its thermal transformations. Our results shed light on the nature of these transformations, the ideal heating temperatures and the tolerated heating speed. The processes occurring in silcrete are comparable to flint, i.e. the loss of chemically bound ‘water’ and the formation of new Si–O–Si bonds, but their intensity is less pronounced. Effective heating temperatures are significantly higher than for flint and the heating speed tolerated by South African silcrete is relatively fast. These findings imply that silcrete heat treatment cannot be directly compared with flint heat treatment. Unlike flint, heating silcrete does not require the setup of a dedicated heating environment and may have been performed in the same time as other fire related activities. This would represent only a minor supplementary investment in time and firewood. These results have broad implications for the discussion about technological evolution and the acquisition of specialised knowledge in the MSA.     

MICRODENTICULATES OF THE FUNNEL BEAKER CULTURE: LITHIC ATTRIBUTE ANALYSIS,USE‐WEAR ANALYSIS,AND CONTEXTUAL ANALYSIS

In a study published in 1994, Helle Juel Jensen observed that microdenticulates are tools whose function is difficult to assess. She calls the use of the tools “an unresolved functional puzzle”. This study proceeds from that conclusion. Based on attribute and use‐wear analyses together with contextual studies the results show that microdenticulates are complex tools, in which other parts of the flake besides the denticulated edge were used. The result also show that other flint objects from the flint asemblage were used for the same operations as the microdenticulates. The work comprised a conceptual action in which the production, use, and deposition of the material were all parts of the same process. The task was given in advance. The work probably consisted of preparing or treating plant fibres in some way in order to make thread, rope, bast, or the like. The result shows that seemingly simple tools like microdenticulates were a part of the materiality of the south Scandinavian Funnel Beaker complex. The work conducted using the microdenticultates and the tool box associated with them was associated with concepts shared by people over large areas (present day south Sweden and Denmark) over hundreds of years (from Early Neolithic to Middle Neolithic AI).     

A NEW THERMOLUMINESCENCE DATING TECHNIQUE FOR HEATED FLINT*

A new thermoluminescence (TL) technique for determining the age of heated flint artefacts from archaeological sites is presented. It is a variant of the SAR protocol, which is usually used for OSL dating of sediment, but it is not based on a presumed model for fitting the dose–response curve. Dose recovery tests as well as comparisons with standard protocols show the accuracy of the new technique. It is found that the sensitivity of the thermoluminescence (TL) signal of flint in the orange–red waveband does not show severe changes due to the heating process while measuring the TL. This allows the application of a short SAR procedure, which requires only two dose points. The technique does not require as much instrument time as other SAR techniques, and thus is advantageous for dating very old samples. The major advantage of this new technique is the small amount of sample material required, which allows the dating of samples that are too small for standard TL dating techniques.     

Notices of New publications

This paper records the excavation of a ploughed-out round barrow (ring-ditch) at Ravenstone, Buckinghamshire (SP 8535 4895). The circular ditch (12.0 m diameter) was broken by four narrow causeways. Two graves were located at the centre of the monument. The primary grave was apparently a cenotaph, for although a coffin, an antler spatula and a flint fabricator were discovered, no skeletal material was found. The secondary grave contained the crouched inhumation of a woman, accompanied by grave goods. Finds from both graves suggest leather-working. A four-post structure (3.60 m square) may have existed on the site prior to the barrow's construction. A substantial quantity of worked flint came from the excavated area, and small pits contained flints of late Neolithic and pottery of Iron Age date. The excavation records are housed at the Buckinghamshire County Museum, as CAS 2555 in the Sites and Monuments Record, and the finds as L.301.     

A REVIEW OF THE LATER UPPER PALAEOLITHIC IN THE ODER AND VISTULA BASINS IN THE LIGHT OF RECENT RESEARCH

Summary. The withdrawal of the Vistulan ice-sheet some 15,000 years ago permitted colonisation of the Oder and Vistula basins by a succession of Late Upper Palaeolithic peoples, amongst whom various distinct groups can be recognised. Magdalenian, Shouldered Point, Curved Back Point and Tanged Point technocomplexes are distinguished by the author, who discusses them with reference to the salient features of the archaeological assemblages, comments on the dating evidence, and considers both internal variability and possible relationships with industries in Western and Eastern Europe. The populations of this region, which coincides approximately with the boundaries of modern Poland, were hunter-gatherers exploiting late glacial and early postglacial game resources, but there is evidence that systematic use was made of other local resources, such as ochre (mined at Rydno), Jurassic flint and the chocolate flint of the Holy Cross Mountains. In this process some of the Late Upper Palaeolithic peoples travelled long distances and established wide contacts. Use of the chocolate flint by Swiderian groups of the Tanged Point technocomplex is proving to be a particularly worthwhile study: flint of this kind is found at some 300 out of 700 Swiderian sites. Actual quarrying places are known in the source area, with working and living sites occurring at various distances from them, offering considerable potential for a study of contemporary economic and social organisation and seasonal migration.     

PROVENANCING FLINT ARTEFACTS WITH ICP–MS USING REE SIGNATURES AND Pb ISOTOPES AS DISCRIMINANTS: PRELIMINARY RESULTS OF A CASE STUDY FROM NORTHERN SWEDEN

Archaeological flint artefacts from the late Mesolithic/early Neolithic site of Vuollerim, northern Sweden, have been geochemically investigated with ICP–SFMS and MC–ICP–MS in search for the geological/geographical origin of the non‐local flint. The Vuollerim flints were compared with reference samples from Denmark (Cretaceous/Tertiary flint) and Russia (Carboniferous flint). Elemental concentrations as well as elemental ratios for REEs and isotopic ratios for Pb and Sr are presented. Significant differences were found between different geological/geographical contexts. Two of the Vuollerim samples can be ascribed a South Scandinavian origin. Possibly also eastern flint is present, although the results are not conclusive in this case.     

The red-stained flint crescent from Gesher: new insights into PPNA hafting technology

A red-stained flint crescent found in the Pre-Pottery Neolithic A (ca. 9000 BC) site of Gesher, Israel, provides us with a unique opportunity to study the hafting technology of a particular tool type in the Levant. We present here a reconstruction, based on chemical and mineralogical analyses, of the hafting technologies and materials employed in the process. Use will also be made of relevant studies of the archaeological record. Local material was used for the production of an elastic adhesive paste, mud plaster, which was then hardened to hold the crescent securely in the haft. The study contributes insight into the hafting technology that was most probably implemented in the production and maintenance of composite tools during the Early Neolithic period.