A comparison of the treatment of errors in radiocarbon dating calibration methods

The application of radiocarbon dating to archaeological samples generally requires calibration of ¹⁴C dates to calendar ages and interpretation of dating errors. In this paper, four recent methods of age calibration are assessed, particularly with regard to their quality of error treatment. Recent experimental research has suggested that commonly quoted errors on “raw” ¹⁴C dates may require enlargement to more realistic levels, which, when incorporated in the calibration schemes, produce a considerable increase in the size of the typical calibrated interval. A general decrease in the sensitivity of ¹⁴C dating using single, “normal precision” dates is implied. Thus typical calibrated age intervals range from 300 to 1300 years (approximate 95% confidence level), with little improvement resulting if “high precision” calibration systems are used to correct “normal precision” dates. Of the four methods considered here, that proposed by Neftel is found to provide the most objective, flexible, comprehensive and “easy to use” scheme. This method is particularly recommended for its treatment of errors both on the dates to be calibrated and on the calibration curve itself.     

江西仙人洞遗址两万年前陶器的年代研究

陶器的出现使得人类生存和社会行为发生了重要转变。我们对江西万年仙人洞遗址出土陶器进行了年代研究、对陶片和碳十四测年样品层位关系开展地层显微结构分析,结果显示遗址出土最早的陶片年代为距今19,000～20,000年,比东亚和其他地区的陶器早了2000～3000年。洞穴内遗存证明这些陶器是在末次冰盛期由采集狩猎者所制造,可能被用做炊煮器。说明陶器在农业出现以前一万年甚至更早就被制造和使用了。     

Reassessing the Developmental and Chronological Relationships of the Formative of Coastal Ecuador

The Ecuadorian Formative was initially interpreted as a result of long-distance diffusion, and migration, more recent research has changed our perception of the Valdivia, Machalilla, and Chorrera culture complexes. In this analysis, these archaeological investigations are reassessed in order to reevaluate our understanding regarding the nature of these prehistoric cultures. Formative chronologies, distributions, interrelationships are reviewed in the light of Pre-Hispanic occupations in El Oro Province. Previous investigations on the Ecuadorian littoral are examined. Results indicate (1) Valdivia and Machalilla are part of the same ceramic tradition and (2) the interrelationships of these complexes to Late Formative Period ceramic sequences are more complex than previously assumed. (3) A major adaptive shift related to an increased dependence upon agriculture occurred during Valdivia VI–VIII, and continued into the Late Formative with the widespread distribution of Chorrera related material culture. (4) Long-distance interaction with the Ecuadorian highlands resulted in the spread of what may be termed a Chorrera horizon and formed the basis of subsequent Andean cosmology where it was symbolically represented according to local and regional artistic canons and over a vast area of Andean South America.     

Sample preparation for accelerator-based radiocarbon dating

Although several efficient sample preparation methods have been devised for conventional radiocarbon dating, the advent of the accelerator mass spectrometer (AMS) dating technique with its much smaller sample requirement and different counting method has meant that new preparation routes have had to be developed. Techniques used for the Oxford AMS system are described in this paper.     

Ford revisited: A critical review of the chronology and relationships of the earliest ceramic complexes in the New World, 6000-1500 B.C.

In 1969, Ford offered a comprehensive model for the diffusion of ceramic production and Formative lifeways in the New World. Although criticized as simplistic, it was echoed by other unitary models, such as Lathrap's spread of Tropical Forest culture outward from a lowland South American hearth. Radiocarbon dates suggest that the earliest American pottery appears in the Amazon basin as early as 6000 B.C. However, there is little support for an ex Amazonas lux spread of pottery technology. Diffusionary models predict early complexes will resemble one another at first and then diverge over time, but comparative analysis reveals substantial variability even at the earliest time level. Heterogeneity among the earliest complexes indicates several likely hearths for the independent evolution of ceramic production, including (1) lowland Brazil, (2) northern Colombia, (3) coastal Ecuador, (4) coastal Peru, (5) central Panama, (6) southern Mesoamerica, (7) the southeastern United States, and (8) the central United States.     

A red deer (Cervus elaphus L.) skeleton from seamer carrs, Cleveland, England: Provenance of the skeleton and palaeoecology of the site

A Red deer, Cervus elaphus L., skeleton from Seamer Carrs was excavated and the collagen fraction of one of the bones dated to 4330 ± 100 bp (Birm. 977). The bones were embedded in a limnic sediment that was dated to 7360 ± 120bp(Birm.882). This date was confirmed by the pollen assemblage, which indicated a Flandrian I/II chronozone age. The date of the Cervus bone is explained by its movement vertically downwards in the limnic sediment. Attention is drawn to the number of large mammalian skeletons that have been recovered from Seamer Carrs during drainage operations and subsequently, and to the mesolithic and neolithic artifacts recovered from the slopes around the Carrs.     

Debates over Palaeolithic chronology – the reliability of C is confirmed

The debate about the complex issues of human development during the Middle to Upper Palaeolithic transition period (45–35 ka BP) has been hampered by concerns about the reliability of the radiocarbon dating method. Large ¹⁴C anomalies were postulated and radiocarbon dating was considered flawed. We show here that these issues are no longer relevant, because the large anomalies are artefacts beyond plausible physical limits for their magnitude. Previous inconsistencies between ¹⁴C radiocarbon datasets have been resolved, and a new radiocarbon calibration curve, IntCal09 (Reimer et al., 2009), was created. Improved procedures for bone collagen extraction and charcoal pre-treatment generally result in older ages, consistent with independently dated time markers.     

Comparison of fluoride and direct AMS radiocarbon dating of black bear bone from Lawson Cave,Missouri

Abstract

After a 20-year hiatus (1955–1975) during which few archaeologists discussed fluoride dating, the method again received attention in the 1980s and 1990s when some argued for its validity. As a dating method, fluoride dating depends on the rate at which fluorine ions replace hydroxyl ions in osseous tissue. The rate of replacement is influenced by the properties of the skeletal part (SP), sediment chemistry (K), and sediment hydrology (H), and the replacement rate influences estimates of time. Calibrated AMS radiocarbon assays of 10 black bear (Ursus americanus) femora from a natural-trap cave in central Missouri are weakly correlated with fluorine concentrations, determined by neutron activation analysis in the 10 femora. Despite minimal variation in SP, K, and H, results indicate fluoride dating can be considered a valid dating method only in cases when the chronological validity of its results are confirmed with independent chronometric data. As similarities in fluorine amounts across specimens increase, provenience information and bone orientation data as well as fine resolution data on K and H become critical to the application of fluoride dating.     

The archaeology of radiocarbon accelerator dating

Accelerator mass spectrometry (AMS) allows radiocarbon dating to be carried out by direct counting of¹⁴C atoms, rather than the conventional counting of radioactive disintegrations. The result is that samples up to 1000 times smaller can be handled. The approach was tested in principle by 1977 and for archaeological operation by 1983. More than 2000 samples per year are now being dated worldwide. The machines can now operate to about ± 80 years or better. Dates older than 40,000 years have not yet been achieved, but the ability to use small samples has already had considerable impact on dating the period 10,000–30,000 years ago. Bone is an ideal material for the new technique, since amino acids can normally be isolated and purified from gram-size samples. Studies of the origins of domestication are aided by the dating of individual grains and seeds. Because small samples can be mobile in the soil, careful sample selection strategies and procedures are required. The full impact of the technique can be assessed only through the rapid and comprehensive publication of archaeological results.     

Radiocarbon Chronology of the Siberian Paleolithic

We have compiled 462 C-14 determinations for 120 Paleolithic and Mesolithic sites from Siberia and the Russian Far East. The Mousterian sites are dated to ca. 46,000–28,500 BP. The Middle–Upper Paleolithic transition dates to ca. 43,300–28,500 BP. Although there are a few earlier sites, most of the Upper Paleolithic sites are dated to the time interval between ca. 34,000 BP and 10,000 BP. The earlier Upper Paleolithic stage is characterized by macroblade technology and is radiocarbon-dated to ca. 34,000–20,000 BP. The earliest microblade technology occurs in the late stage of the Upper Paleolithic, dated to ca. 23,000–20,000 BP, but the majority of microblade sites is dated to ca. 20,000–11,000 BP. The Final Paleolithic (Mesolithic) sites date to ca. 12,000–6000 BP. At ca. 13,000–11,000 BP, the earliest Neolithic appeared in both the Russian Far East (Amur River basin) and the Transbaikal. The Paleolithic–Neolithic transition occurred ca. 13,000–6000 BP.     

Radiocarbon dating of bone by accelerator mass spectrometry

A companion article describes the sample preparation method used in the production of graphite targets for the Oxford accelerator mass spectrometer (AMS) system. The chemical pretreatment developed for the dating of bone, ivory and tooth samples is described in this paper.     

A Spanish Man‐o‐War in New Zealand? The 1864 wreck of Grafton and its lessons for pre‐Cook shipwreck claims

This paper considers the 1864 wreck of Grafton in the Auckland Islands, and its implications for wreck analysis and pre‐Cook exploration claims. The captain of Grafton, Thomas Musgrave, stated that the schooner was built from the wreck of a Spanish man‐o‐war, and archaeological analysis of the wreck found that the timbers are a tropical South American species, and had possibly been reused. The implications of this are clear; it is possible that timbers that originated in pre‐Cook (1769) ships lie in New Zealand, but without a full understanding of the historical and archaeological context of any such timbers, including their reuse in later ships, it is not possible to claim proof of pre‐Cook European exploration of New Zealand.