Development and application of methods used to source prehistoric Southwestern maize: a review

Archaeological cobs free of mineral contaminants should be used to source the soils in which they were grown. Mineral contaminants often contain much higher concentrations of metals than vegetal materials and can alter a cob’s apparent metal and heavy-isotope content. Cleaning a cob via immersion in an acid solution for more than a few minutes will result in the incongruent and sometimes complete leaching of metals, including strontium (Sr), from the cob. When using ⁸⁷Sr/⁸⁶Sr to determine the location of potential agriculture fields, it is best to either integrate several depth-integrated soil samples or to integrate several vegetation samples from individual fields. Biologically labile Sr in semi-arid Southwestern soils largely originates from eolian source or sources and usually is not derived from underlying bedrock. Existing Sr-isotope data indicate that archaeological cobs from Aztec Ruins came from either the Mesa Verde-McElmo Dome or Totah areas, that Pueblo Bonito and Chetro Ketl cobs, from Chaco Canyon that predate A.D. 1130, probably came from the Rio Chaco corridor, and that cobs from Chaco Canyon, that postdate A.D. 1130, probably came from either the Totah or Zuni areas.     

Possible sources of archaeological maize found in Chaco Canyon and Aztec Ruin,New Mexico

Maize played a major role in Chaco's interaction with outlying communities in the southern Colorado Plateau. This paper seeks to determine where archaeological corn cobs brought to Chaco Canyon were grown. Strontium-isotope and trace-metal ratios of 180 soil-water and 18 surface-water sites in the Southern Colorado Plateau have revealed possible source areas for some of 37 archaeological corn cobs from Chaco Canyon and 10 archaeological corn cobs from Aztec Ruin, New Mexico. The most probable source areas for cobs that predate the middle-12th-century drought include several Upper Rio Chaco sites (not including Chaco Canyon). There are many potential source areas for cobs that date to the late A.D. 1100s and early 1200s, all of which lie in the eastern part of the study area. Some Athapascan-age cobs have potential source areas in the Totah, Lobo Mesa, and Dinetah regions. One Gallo Cliff Dwelling cob has a strontium-isotope ratio that exceeds all measured soil-water values. Field sites for this cob may exist in association with Paleozoic and Precambrian rocks found 80–90 km from Chaco Canyon. Potential source areas for most Aztec Ruin cobs (many of which were found in rooms dating to the first half of the 13th-century) appear to be associated with a loess deposit that blankets the Mesa Verde and McElmo Dome regions.     

Oxygen isotopes in cellulose identify source water for archaeological maize in the American Southwest

Maize (Zea mays) was a primary food crop for aboriginal societies of the arid American Southwest. Water used for maize production in these arid zones could have come from precipitation and runoff during the summer monsoon, from perennial streams and springs, or from stored soil water fed by snowmelt. The oxygen stable isotope ratio (δ¹⁸O) of summer and winter precipitation on the Colorado Plateau naturally differ by more than 10‰ providing a powerful tool for distinguishing winter- from summer-derived water sources used in cultivation of maize. We investigated whether variation in δ¹⁸O of potential source waters is preserved in the δ¹⁸O of cellulose (δ¹⁸O_cellulose) of maize cobs by growing four aboriginal and one modern maize variety in pots irrigated with water of known δ¹⁸O composition. The δ¹⁸O_cellulose values of cobs ranged from 26.8 to 36.4‰ (averaged within varieties) and were highly correlated with δ¹⁸O values of the source irrigation water (−15.8 to −8.2‰). Cob δ¹⁸O_cellulose from five archaeological sites on the Colorado Plateau in southeastern Utah ranged from 27.3 to 34.6‰, closely matching the range of values observed in experimental plants. A δ¹⁸O_cellulose model developed originally for tree rings was parameterized and applied to the archaeological maize cobs. The model indicated that monsoonal precipitation accounted for 0–20% of the moisture for archaeological cob samples from a site adjacent to a perennial stream and 43–98% for samples from an upland site, more distant from a perennial water source. These results reveal the potential for using δ¹⁸O_cellulose to investigate prehistoric irrigation practices and source water used for maize production in the American Southwest.     

Fish bone chemistry and ultrastructure: implications for taphonomy and stable isotope analysis

This paper reviews the ultrastructure and chemistry of fish bone, with an emphasis on zooarchaeology and stable isotope analysis. On the basis of the chemical composition of the collagen and the relationships between the collagen and mineral phases, fish bone is more susceptible to biotic and abiotic degradation than mammalian bone and is therefore less likely to be recovered in archaeological deposits. The amino acid composition of fish bone differs from that of mammals, most notably with respect to hydroxyproline content. The C:N ratio of fish collagen is, however, very similar and slightly lower than mammalian collagen, and thus the traditional range of acceptable C:N ratios for archaeological bone collagen (2.9–3.6) should not be shifted or extended for fish on the basis of the amino acid composition of collagen. An extensive survey of published archaeological bone collagen C:N ratios demonstrates that fish collagen from archaeological contexts tends to have significantly higher C:N ratios than mammalian collagen. The elevated C:N ratios in fish bone collagen may be the result of abiotic degradation processes that occur within the bone after death, the presence of exogenous humic contaminants, or endogenous lipid contaminants.     

Quebrada Tacahuay,Southern Peru: A Late Pleistocene Site Preserved by a Debris Flow

Abstract

Here we describe the properties of a debris flow apparently generated by a warm phase El Niño event that buried an intermittently occupied Late Pleistocene forager site located in the southern coastal desert of Peru. Although the event deposited roughly one meter of sediment over the initial occupation, our analyses of debris flow dynamics and data from large scale archaeological investigations indicate that the earliest anthropogenic deposits at the site of Quebrada Tacahuay were preserved intact as a result of the burial episode; there is no evidence that the debris flow scoured or disturbed the cultural deposits. The event that buried the oldest archaeological contexts at Quebrada Tacahuay differs from other flood events that are characterized by turbulent, fast-moving floodwaters. Our data on debris flow dynamics and our results from excavation have implications for identifying, investigating, and interpreting other deeply buried archaeological sites both in the central Andes and in other geographic regions.     

Distinguishing Remains of Human Cremations from Burned Animal Bones

Abstract

Archaeological remains of human cremations, often consisting of a few calcined bone fragments unassociated with any other indicators of human mortuary behavior, are sometimes difficult to distinguish from mammalian remains representing ancient garbage. Although experimental and archaeological studies of human cremation may facilitate recognition of cremated or otherwise burned mammal bone, they do not provide the necessary criteria to distinguish cremation from other kinds of burning and, therefore, to recognize, immediately, a human cremation in archaeological context. Experiments were conducted to provide criteria for distinguishing the remains of cremated whole large mammals from intensively burned fresh, anhydrous, archaeological, boiled, and baked bones of large mammals. Results indicate that distinctive patterns of cracking, fracturing, and warping of calcined bone, and especially the absence of evidence of perimortem fracture, may alert the excavator to the possibility of a human cremation.     

Effects of Sodium Hydroxide Treatment and Ultrafiltration on the Removal of Humic Contaminants from Archaeological Bone

This study compared bone collagen extraction techniques that included treatment with sodium hydroxide and 30 kDa ultrafilters using a set of well‐preserved, humic‐contaminated archaeological marine mammal bones. Treatment with sodium hydroxide was effective at removing humic contaminants from archaeological bone, although yields were significantly decreased. Yields were also significantly decreased by ultrafiltration although this study produced no evidence that 30 kDa ultrafilters were effective at selectively removing humic contaminants from archaeological bone. The combination of sodium hydroxide treatment and ultrafiltration did not produce superior results to the treatment involving only sodium hydroxide. Archaeological samples exhibiting darker colouration indicative of humic contamination should be treated with sodium hydroxide to remove these contaminants. Copyright © 2017 John Wiley & Sons, Ltd.     

Fatty acid analysis of prehistoric burned rocks: a case study from central California

Although lipid analysis of archaeological residues has been utilized for almost three decades, it has rarely been applied to archaeological materials other than pottery. A 2001 study used lipid analysis of burned rocks (sandstone) and ground stone tools to interpret subsistence change at a south Texas site (M.J. Quigg, M.E. Malainey, R. Przybylski, G. Monks, No bones about it: using lipid analysis of burned rock and groundstone residues to examine Late Archaic subsistence practices in South Texas, Plains Anthropologist 46 (2001) 283–303). If such applications are reliable, insight into past subsistence practices could be greatly enhanced. The following study tested whether measurable amounts of lipids could be extracted from burned rocks (andesite) from a central California site and the ability of fatty acid analysis to reliably interpret those extracts. While results indicate that some of the burned rocks may contain lipids absorbed from cooking activities, lipids were also recovered from off-site rocks. Before reliable interpretations of culturally introduced lipids can be made, more thorough study of the types and amounts of lipids present in rocks due to natural processes is necessary.     

PEAT-BOG SITES IN THE EASTERN URALS

Peat-bog sites are unique archaeological sources due to their ability to preserve organic remains which otherwise decompose in mineral soils. This opens up a wide range of prospects for the use of science-based methods in paleoenvironmental research. Relatively few peat-bog sites are known in Russia; most are located in the Eastern Urals and in the forest zone of the Russian Plain. At the Uralian sites, anthropomorphic and zoomorphic sculptures, vessels, transportation means, hunting and fi shing tools, and details of structures made from organic materials have been discovered. All these are highly relevant to archaeological reconstruction. Along with fi nds from numerous sites in mineral soils they provide a basis for multidisciplinary approaches to reconstructing the environments, lifestyles, and ideologies of prehistoric Northern Eurasia.     

Erosion and Errors: Testing the Use of Repeated LIDAR Analyses and Erosion Modelling for the Assessment and Prediction of Erosion of Archaeological Sites?

Slope soil erosion is one of the main threats to archaeological sites. Several methods were applied to establish the erosion rates at archaeological sites. Digital elevation models (DEMs) from three different dates were used. We compared the elevations from these three models to estimate erosion. We also applied the landscape evolution model LAPSUS with the available DEMs as basis. Spatial processing errors and effects of tillage and harvesting practices explain most of the DEM elevation differences between the recordings. Increased DEM resolution does not result in more precise or reliable erosion. The present technological level of landscape evolution modelling makes it possible to indicate areas most vulnerable to soil displacement by surface runoff erosion and tillage. Future research, using sediment and surface dating techniques such as deposit of radionuclides, heavy metals and OSL dating will provide a more accurate estimation of erosion rates and the subsequent impact on archaeological sites.     

An experimental micromorphological investigation of bedding construction in the Middle Stone Age of Sibudu,South Africa

We conducted experiments to compare the micromorphological signatures of modern burnt sedge and grass bedding to laminated layers of carbonized material and phytoliths in Middle Stone Age deposits at the shelter, Sibudu. The experiments were designed to clarify the formation processes associated with the laminated layers and to investigate whether these previously identified layers of bedding were deliberately burned or not. The results indicate that the laminated layers were most likely produced by human activity related to the construction, maintenance and burning of bedding. Furthermore, our experiments demonstrate that large volumes of vegetal material could have produced the relatively thin, archaeological deposits of burnt bedding.     

Reburial and Analyses of Archaeological Remains in the Marine Environment — Investigations into the Effects on Metals

Abstract

The treatment and long-term storage of recovered cultural material from underwater heritage sites is becoming less cost effective, and reburial of archaeological sites and the associated artefacts in the marine environment is becoming increasingly common practice in managing the submerged cultural resource. Following recent large-scale underwater archaeological excavations in Marstrand harbour, Sweden, the majority of recovered finds were reburied in defined trenches in the harbour sediment. Subsequently, the Studio of the Western Sweden Conservators in conjunction with the Bohus County Museum initiated a fifty-year research project to evaluate reburial as an appropriate method of preserving waterlogged archaeological artefacts in the long term. The research project, entitled ‘Reburial and Analyses of Archaeological Remains’, was launched in 2002 and consists of six sub-projects. The main aims of these sub-projects are to analyse the extent of deterioration of the most common material types found on underwater archaeological sites, assess the stability of packing and marking materials used in archaeological documentation, and monitor the reburial environment.

The aim of the metals sub-project is to investigate the short- to long-term corrosion behaviour of metals buried in the marine environment by examining the deterioration of reburied and exposed modern metal coupons and eventually compare these results to the analysis of actual shipwreck artefacts. The environmental monitoring sub-project is designed to complement the other sub-projects by assessing the physico-chemical changes occurring in the reburial environment over time and the effect on the deterioration of the different reburied material types. In comparing the results obtained over the past seven years from both the metals and monitoring sub-projects, it should be possible to more accurately evaluate the effectiveness of reburial as a long-term in situ preservation strategy for metallic archaeological remains.     

Provenancing East Mediterranean cedar wood with the <Superscript>87</Superscript>Sr/<Superscript>86</Superscript>Sr strontium isotope ratio

⁸⁷Sr/⁸⁶Sr isotope ratios of cedar wood from forests in the East Mediterranean have been compiled in order to investigate the feasibility of provenancing archaeological cedar wood finds. Cedrus sp. forests furnished a great amount of wood in antiquity, for purposes ranging from ship to temple construction, and for fashioning cult statues and sarcophagi. The ⁸⁷Sr/⁸⁶Sr signatures of archaeological cedar samples may be compared with the preliminary dataset presented here to help determine the geographic origin of wooden artifacts. Sample sites include two forest areas in the Troodos Massif of Cyprus, five in the Lebanon, and two in Turkey’s Taurus Mountains. Sr ratios for wood varieties (i.e., early heartwood, late heartwood, sapwood, and twig wood) demonstrate relative uniformity between the xylem types frequently recovered from archaeological contexts. As such, this pilot study also assesses important issues of archaeological sampling and the geographical factors that influence Sr uptake in cedar trees of this region. While the regional signatures are distinct in most cases, small sample sizes and range overlap indicate the need for additional methods to make a case for a certain source forest. Alone, this method continues to be best used to disprove assumed wood provenances.     

Starch granules,dental calculus and new perspectives on ancient diet

Recent work in various parts of the world has suggested the possibility of ancient starch granules surviving and adhering to archaeological artefacts. Often this information is used to infer aspects of diet. One additional source for recovery of archaeological starch granules is dental calculus. The presence of plant food debris in dental calculus is well known but has not been not widely investigated using archaeological material. The extraction of starch granules from dental calculus represents a direct link to the consumption of starchy food by humans or animals. Using dental calculus also sidesteps many other questions still inherent in using starch granules to reconstruct aspects of ancient diet, such as the effects of diagenesis on their morphology; as the starches are trapped inside a concreted matrix they are less likely to alter over time. We used amylase digestion by a starch-specific enzyme to confirm the material as starch.     

Examining histology to identify burned bone

Early research suggests that examination of the microscopic internal structure is a valid method for distinguishing burned from unburned bone in the archaeological record. This study compares burned and unburned modern bones with archaeological bones from Sibudu Cave (ca. 60,000 years ago) and Cave of Hearths (over 200,000 years ago) to more fully describe the heat-induced histological changes to bone. We also explore the effects of diagenesis on those changes to determine if histological evidence of burning preserves through fossilisation and diagenetic processes and can be successfully used to identify ancient burning. Application of this technique can help in addressing various issues, including the origins of controlled use of fire and understanding animal butchery and disposal.     

The Freedom of the Seas: Untapping the Archaeological Potential of Marine Debris

The issue of marine debris is of a growing concern to present day society. Nonetheless, the occurrence of garbage on the sea floor is widely ignored by the marine archaeological body. The main purpose of this article is to discuss archaeological aspects of marine debris of the contemporary past. In particular, the article explores the phenomenon of marine dumping, the active use of raised debris for the sake of education and opinion forming and the human footprint of holiday boating. Drawing from this, it is argued that a maritime garbology—a maritime archaeology that intersects both with the archaeology of the contemporary past and the multidisciplinary field of consumption- and garbage studies—is not only possible but also a promising and relevant field of research.     

Mineral weathering in forest soils and its relevance to the preservation of the buried archaeological resource

There is more woodland in Britain now than for many centuries and considering many international climate change mitigation policies, woodland cover, both in Britain and internationally, is being promoted. However, neither the management of existing woodlands nor their expansion should be at the expense of important archaeological evidence. Due to the large number of known archaeological sites, the large areas of land with uninvestigated archaeological potential and the expanding woodland cover, suitable mitigation strategies need to be developed to allow preservation in situ of important sites. An understanding of how woodland soils and the buried archaeological resource interact is, therefore, essential. This paper utilises ongoing environmental research into the mineral weathering rates in forest soils and considers its application to artefact preservation. The study concludes that soil water pH, its movement, and the saturation of dissolved ions in the soil solution are major factors determining both mineral and artefact longevity. A simple guide to artefact longevity based on these properties is proposed and a geochemical model for predicting loss is tested. These tools could be applied to any soil or individual horizon irrespective of land-use.     

The taphonomy of cooked bone: characterizing boiling and its physico–chemical effects

Cooking is perhaps the most common pre–burial taphonomic transformation that occurs to bone, yet it is still one of the least understood. Little progress has been made in determining a method of identifying cooked bone in the archaeological record, despite its import for various branches of archaeology. This paper attempts to describe boiling in terms of its physico–chemical effects on bone, and uses a suite of diagenetic indicators to do this. It is shown that cooking for brief periods of time has little distinguishable effect on bone in the short term, but that increased boiling times can mirror diagenetic effects observed in archaeological bone. The relationship between the loss of collagen and alterations to the bone mineral is explored through heating experiments, and the results compared with archaeological data.The possibility of boiling being used as an analogue for bone diagenesis in future studies is raised, and the key relationship between protein and mineral is once again highlighted as vital to our understanding of bone diagenesis.     

Bower birds,bones and archaeology

Objects collected by the Australian great bower bird, Chlamydera nuchalis, may include artifacts and human food debris. The birds could affect the shape and interpretation of some archaeological assemblages. Bones from two bower collections are described according to: (1) their sizes and shapes; (2) the taxa and elements represented; and (3) marks and damage. The potential relevance of the birds for archaeological interpretation is assessed and ways of recognizing bias caused by the birds are discussed.     

Maize and Bone: Residues of Grinding in Northwestern Argentina*

Archaeometric and archaeobotanical analyses of grinding residues inside an archaeological milling stone tool from the Cueva de los Corrales 1 site in northwestern Argentina are shown. Multiple analytical techniques are used to identify ground substances, and their results are compared and complemented. They give direct and reliable evidence of maize (Zea mays L.) and burned bone grinding in the pre‐hispanic Argentine north‐west, although the latter is little related to milling tasks.