Thermoluminescent dating of the Late Bronze and Early Iron Age pottery on sites in Kłyżów and Jarosław (SE Poland)

The absolute chronology of Late Bronze and Early Iron Ages in Polish territories is a result of long-term and complex research. Here, we have investigated the absolute dating of two sites, namely K?y?ów, a cemetery of the Tarnobrzeg Lusatian culture, and Jaros?aw, a settlement spanning from the late phase of the former to Pomeranian culture, possibly with Jastorf elements. Having been spurred by promising results of thermoluminescence (TL) dating of medieval and Przeworsk materials, we have employed it in those situations, where no other chronometric methods seem to be efficient. TL dating has been combined with typological analysis of the dated pottery and, partially, with radiocarbon method. Albeit the produced TL dates do not represent the level of sought-for fine chronological resolution, they indicate the temporal trends and corroborate the typological research. Our study has shown the potential of TL dating for periods with plateaus on ¹⁴C calibration curve. We also have dealt with unexpected TL ages and suggested some solutions of the problem. Finally, we have demonstrated that the condition sine qua non for archaeological interpretation of TL dates is a thorough stylistic-chronological analysis of dated pottery and clear understanding of relations between chronometric dates and the archaeological event to be dated.     

New age constraints for hominid footprints found on Jeju Island,South Korea

In 2004 numerous hominid footprints, along with diverse animal footprints, were found in the Late Quaternary strata of Jeju Island, South Korea. However, the age of the sediments in which the footprints were found is still controversial. Previous age estimates included radiocarbon ages of ca. 15,000 yr BP (Late Pleistocene) and quartz optically stimulated luminescence ages of ca. 7000 yr BP (mid-Holocene). In this study we report on 11 AMS ¹⁴C dating results from a new set of samples collected from the footprint-bearing strata and from associated sediments. Despite some variations and age reversal, all samples collected from the footprint-bearing strata yielded ¹⁴C ages of late Pleistocene. These ages are comparable with previous radiocarbon dating results. Furthermore, the presence of the proboscidean footprints attributable to woolly mammoths in the footprint-bearing strata supports the radiocarbon dating results. Based on the new radiocarbon dates and the presence of the alleged mammoth footprints, the age of the hominid footprints found at Jeju Island is thought to be late Pleistocene (about 19,000–25,000 cal yr BP). Therefore, this is the second discovery of hominid footprints dated to the Pleistocene age in Asia, and the first to be discovered in Korea.     

Radiocarbon dating of prehistoric hearths in alpine northern Sweden: problems and possibilities

The chronology of prehistoric Sami settlement sites has previously been established by conventional radiocarbon dating of bulk charcoal samples associated with hearths from sunken hut floors (stállo-foundations). Here we present results of a comprehensive dating exercise of stállo-foundations in the alpine area of northern Scandinavia using Accelerator Mass Spectrometry (AMS) radiocarbon dating of charcoal. Over a 3 km² study area, AMS calibrated ages of hearth charcoal from 22 stállo-foundations across 12 sites securely date these features to between cal. AD 640 and AD 1180. Only small variations in age were found between charcoal samples from different areas of a given hearth. Statistical analysis of all the charcoal AMS radiocarbon dates obtained reveals that 12 stállo-foundations across nine sites are contemporaneous and date to the Viking Period (AD 800–AD 1050). The tightly constrained AMS-based chronology of stállo-foundations contrasts with the existing chronology based on conventional radiocarbon analysis, which places these features within a significantly greater time-frame of between AD 600 and AD 1900, with most dates ranging between AD 800 and AD 1350.This discrepancy is likely to result from the necessity of collecting composite hearth charcoal particles, which may originate from different phases of occupation, in order to achieve the required final carbon content for conventional radiocarbon analysis. We argue that the new AMS-based radiocarbon chronology of stállo-foundations presented here supersedes the existing chronology based on conventional (Gas Proportional counting) radiocarbon analysis and we advocate the use of AMS radiocarbon dating in future hearth investigations.     

Interpreting,dating, and reevaluating the botanical assemblage from tell Kedesh: a case study of historical contamination

Botanical assemblage including charred and mineralized macro plant remains were examined from tell Kedesh in the Upper Galilee, Israel. Flotation samples were collected from various contexts within and outside a large Persian-Hellenistic administrative building complex at tell Kedesh, dated to the 5th to the 2nd century BC, based on the archaeological material. Four AMS radiocarbon dates were obtained on plant macro remains recovered from the flotation samples from the complex. The radiocarbon dates range from the 9th century BC to 17th century AD. The discrepancy among the radiocarbon dates obtained from plant remains and those based on archaeological material can be attributed to bioturbation, including the deep burrowing of harvester ants. The study demonstrates the need for direct radiocarbon dating of the charred plant remains generally assumed to be of ancient origin. This research improves the understanding of depositional and postdepositional processes of plant macro remains and explains their mode of arrival, relevant for the sites with a long occupational history by humans and animals.     

PLASTER AND MORTAR RADIOCARBON DATING OF NABATEAN AND ISLAMIC STRUCTURES,SOUTH JORDAN*

The study aims to use lime mortars and plasters to radiocarbon date Nabatean and Islamic structures from Petra and Udruh, south Jordan. Fifteen samples from seven structures were characterized by thin‐section, scanning electron and cathodoluminescence microscopy. The lime binders of all the samples and the organic inclusions from nine samples were AMS radiocarbon dated. The dates and the historical data of the samples were compared with each other. The results showed an agreement between the radiocarbon dates of the lime binders and the organic inclusions and the historical data for most of the samples. The radiocarbon dates of the lime binders supported by the radiocarbon dates of the organic inclusions and the archaeological data were helpful in reconstructing a rather precise chronology of the studied structures.     

RADIOCARBON DATING OF MORTARS FROM ANCIENT GREEK PALACES

This study deals with radiocarbon dating of lime mortars which were used as supports for Mycenaean and Minoan paintings. The ¹⁴C dates are. on the whole, compatible with the historical data. and thus show that a large proportion of the Mycenaean surficial coatings can be dated by the radiocarbon method. However. in order to determine the age of the mortars accurately. it is necessary to evaluate the amount of sedimentary carbonate which may have been added to them. It is shown here that the oxygen and carbon isotope compositions of lime mortars are significant indicators that such a mixing actually took place.     

Dendrochronological and radiocarbon dating of subfossil wood from the Morava River basin

The paper deals with dendrochronological and radiocarbon dating of subfossil trunks found in the basin of the Morava River. The research into subfossil trunks had been conducted in the Czech Republic in the past but the research stopped in 2001. 160 records of measurements of subfossil, predominantly oak trunk samples, are preserved from that time. Three years ago the research was reopened and again the most trunks were found in the basin of the Morava River. 92 samples of oak trunks and 7 samples of other tree species (poplar, elm, maple, beech) were taken from selected sites. The samples were processed in compliance with the standard dendrochronological methodology. To date the samples, Czech, Austrian, Polish and German standard chronologies were used. In cases when the dendrochronological dating was unsuccessful, the samples were sent for radiocarbon dating. In total, 35 samples were dated, mainly by the radiocarbon method. Subfossil trunks from gravel pit Tovačov were dated and classified into 4 different periods, the oldest being from 2780–2190 BC. In Osek nad Bečvou, the samples were taken from two sites. Whereas from the 4 trunks taken in the river channel each was from a different period, the trunks from the gravel pit come from 981–1015 AD. The trunks found in the Morava River basin near Strážnice were dated to the 10^th–15^th century. In the future, we expect to extend the amount of the acquired samples with the aim to create a link to the existing standard chronology or to create a long floating average treering curve.     

Radiocarbon dating: Some practical considerations for the archaeologist

The article is divided into four main sections in each of which a key aspect of radio-carbon dating is discussed with emphasis on the practical implications for users of dates. The four topics which the article attempts to deal with are, in turn, (i) the effect on the radiocarbon timescale of the variations in atmospheric ¹⁴C now known to have occurred in the past and the role of other absorlute dating methods in investigating these, (ii) laboratory measurement of ¹⁴C, (iii) selection of optimum samples for dating and (iv) some of the limitations of the final dates. The theme is essentially that the technical difficulties of radiocarbon measurement in the laboratory have been overcome to the extent that the physical measurements can now be made with high precision, that is to within ±1% or better, as a routine. Thus, it is more important than ever (a) that only reliable samples having very firm associations should be dated and (b) that pretreatment of such samples by the dating laboratory to remove any age contaminants should be completely effective. However, in addition to the recognized statistical limitations, the absolute accuracy of radio-carbon dating is limited by the past ¹⁴C variations. Coupled with the requirements of proper association and pretreatment of samples is the long-term need to establish an overall correlation between radiocarbon and calendar years. At present this is still a matter for final agreement by the laboratories concerned. Meanwhile, when all possible steps have been taken to ensure the reliability of the date messurements, these can strictly only be compared with one another in terms of radiocarbon years bp. In practice this is often too restrictive but any attempts at calibration must be regarded as approximations for the time being. In this article the lower and upper case notation advocated in Antiquity46, 265, for radiocarbon and calendar years respectively has been followed.     

The 13th century polynesian colonization of Hawai’i Island

We assess 926 radiocarbon dates from Hawai’i Island, the largest assemblage of dates compiled from a single island in Oceania. Based on a classificatory approach that arranges the dates based on their reliability, accuracy, and precision, our results indicate that the most reliable estimate for the initial Polynesian colonization of Hawai’i Island is AD 1220–1261, ∼250 to 450 years later than the current consensus. This conclusion is strikingly convergent with recent estimates for the colonization of remote East Polynesia. Our analysis highlights the need for wood charcoal identification to insure selection of short-lived plants/plant parts for radiocarbon dating, and that a reliance on dating unidentified wood charcoal is a waste of resources that only serves to retard progress in refining the settlement chronology of Hawai’i Island and other locations.     

BAYESIAN ANALYSIS OF PLEISTOCENE CHRONOMETRIC METHODS*

Bayesian analysis of radiocarbon dates on Holocene archaeological sites has become well established. Application to Pleistocene sites dated by multiple techniques would be advantageous. This paper develops the necessary mathematical apparatus in the form of likelihoods for luminescence dating, and uranium‐series dating, and considers the possibility for amino‐acid racemization dating. Application of the new methods is illustrated using the stratigraphic sequences of dates from the sites of Saint‐Césaire and La Chaise‐de‐Vouthon. For application to amino‐acid racemization dating, fuller publication of data is found to be required.     

Palaeoenvironmental and chronological investigations of the Magdalenian sites of Goyet Cave and Trou de Chaleux (Belgium), via stable isotope and radiocarbon analyses of horse skeletal remains

Trou de Chaleux and Goyet are caves situated less than 30 km apart in Belgium that contain stratified Magdalenian artefacts and butchered faunal remains. Published radiocarbon dates suggest that both sites were contemporaneously occupied during to the Late-glacial interstadial. It has previously been suggested that the Trou de Chaleux Late-glacial faunal remains might be slightly older than those at Goyet Cave, and that Trou de Chaleux has two phases of occupation during the Late-glacial interstadial. However, the limited number of radiocarbon dates currently available makes it impossible to determine whether the sites are truly contemporaneous, and the assessment of their absolute chronologies is complicated by a plateau in the calibration curve. In this paper, bone collagen δ¹³C and δ¹⁵N signatures of horse bones from the two sites are used to reconstruct local palaeoenvironments. We hypothesise that if occupations at the two sites were contemporaneous, the horse collagen δ¹³C and δ¹⁵N isotope signatures from both sites will be similar, since comparable carbon and nitrogen isotopic values would reflect similar diets, ecologies and environments. To provide clear dating parameters, new AMS radiocarbon determinations are also presented. Results show that horse collagen δ¹³C and δ¹⁵N isotope signatures at the two sites are different, indicating that the populations were not subject to similar diets, ecologies and environments. The new radiocarbon dates confirm that the horse bones from Trou de Chaleux date to the Late-glacial interstadial, but they also show that in Goyet Cave Horizons 1 and 2, older horse remains dating to ca. 32?000–27?000 ¹⁴C yr BP are mixed with Late-glacial horse remains. The δ¹⁵N values of the Goyet Cave horse bones radiocarbon dated to the Pleniglacial are substantially higher than those that have Late-glacial radiocarbon dates. Therefore, we now hypothesise that the majority of the horse bones isotopically analysed from Goyet Cave Horizon 1 are Pleniglacial in age. Statistical analysis of the radiocarbon dates indicates that the Late-glacial occupation at the two sites was contemporaneous, and that while there may appear to be two phases of occupation at Trou de Chaleux, this may be an artefact of the radiocarbon calibration curve.     

Implications of a freshwater radiocarbon reservoir correction for the timing of late Holocene settlement of the Elk Hills,Kern County,California

Uncertainties regarding the magnitude of freshwater radiocarbon reservoir effects can introduce random errors into dates on archaeological freshwater carbonates. As a result, many archaeologists avoid dating freshwater shells unless no other datable materials are available. The chronology of prehistoric occupation of the former Naval Petroleum Reserve No. 1 (NPR-1) at Elk Hills, Kern County, has been established with 50 radiocarbon dates on freshwater mussels (Gonidea and Anodonta sp.). Characterization of any freshwater radiocarbon reservoir effect is crucial for the accurate interpretation of inferred settlement and subsistence changes on the Elk Hills. Paired charcoal and freshwater mussels sampled from closely associated contexts were dated to identify a freshwater reservoir effect. Paired Anodonta and Gonidea sp. shells were dated to investigate interspecific differences in fractionation. Results indicate that a 340 ± 20 ¹⁴C yr correction should be applied to conventional ¹⁴C dates on freshwater carbonates in the Buena Vista Basin before calendar calibration. Evidence of interspecific differences is inconclusive. Dates recalibrated with the reservoir correction indicate that widespread occupation of the Elk Hills is correlated with increasing precipitation towards the end of the Medieval Climatic Anomaly and during the Little Ice Age, suggesting that slough resource exploitation may have been driven by regional population pressure rather than drought-related declines in aquatic productivity.     

Radiocarbon Dating of Architectural Mortar: A Case Study in the Maya Region,Quintana Roo,Mexico

Abstract

The use of radiocarbon dating to analyze mortar and charcoal inclusions within mortar or plaster is a useful way to date the construction of architecture, particularly when options for other chronometric methods are limited. In the Yalahau region of northern Quintana Roo, Mexico, members of the Yalahau Regional Human Ecology Project have faced challenges in dating buildings made of large blocks of stone in the Megalithic architectural style. The Megalithic style poses serious problems for any analysis, as excavating into structures with stones weighing several tons can be dangerous, expensive, and time consuming. Additionally, there are no associated sculptures, texts with dates, or other traditionally accessible chronological markers. These factors have resulted in a reliance on a ceramic chronology despite the uncertainty of the dating of many ceramic types in this region, as well as the questionable contextual associations between recovered ceramics and architectural construction phases. Megalithic-style structures at the ancient Maya site of El Naranjal have residual mortar with charcoal inclusions left behind during the mortar-making processes that can be extracted and dated with AMS ¹⁴C methods. Several samples of mortar and charcoal were obtained from structures 1 and 10 from exposed exterior walls and an interior vault. The resulting dates confirm the date for the construction based on ceramics excavated from the same site.     

Problems in the interpretation of radiocarbon dates: the Pastoral Neolithic of East Africa

For the Pastoral Neolithic of East Africa radiocarbon dates suggest two apparent anomalies in the archaeological record: pastoralism in the Central Rift at perhaps 7000 bp, and the very long duration of particular pottery traditions. This paper examines the dating evidence closely, in particular the assertion that apatite gives more reliable dates than collagen. Both the assertion and the anomalies appear to be false. It is shown that there is no firm evidence for pastoralism in East Africa before about 4000 bp. Similarly, the Narosura tradition is of shorter duration and more recent than previously supposed. The meagre dating evidence for the Namoratunga sites and its implications are also assessed. Examination of the dates for the Pastoral Iron Age shows that the Turkwel tradition is dated only by a single date and that the appearance of twisted cord rouletted pottery in the present millennium post-dates the end of stone tool manufacture by several centuries. The paper concludes with a plea for more critical assessment of radiocarbon dates and for greater rigour in their presentation.     

New dates from Ushki-1, Kamchatka,confirm 13,000 cal BP age for earliest Paleolithic occupation

For many years cultural layer 7 at the Ushki sites, Kamchatka was considered to represent the earliest human occupation of Beringia, because four radiocarbon dates indicated an age of 16,000–17,000 calendar years ago (cal BP). In 2003, however, Goebel et al. reported that layer 7 more likely formed only 13,000 cal BP, nearly 4000 years later than N.N. Dikov, the site’s primary excavator, originally reported. Some researchers have downplayed the significance of the new dates, continuing to regard Dikov’s early dates as evidence that at least some of the hearth and dwelling features previously excavated at Ushki-1 date to as early as 17,000 cal BP. Here we present four new radiocarbon dates (and two previously unpublished dates) on curated charcoal from hearth features excavated at Ushki-1 more than 20 years ago. They indicate that these hearths and associated dwelling features date to about 13,000 cal BP. We now know 15 radiocarbon dates on charcoal from a variety of features and profiles across Ushki-1 and Ushki-5 that indicate the age of layer 7 is about 13,000 cal BP. We discount the four 16,000–17,000 cal BP dates, first, because two of them came from a deeply dug human burial pit and were likely secondarily introduced into the burial; second, because provenience data for the other two dated samples were never reported and do not exist in the records of the radiocarbon laboratories that produced them; and, third, because sediments immediately underlying layer 7 at Ushki-1 are only a few centuries earlier than 13,000 cal BP, providing an important lower-limiting age for the layer-7 occupation. We conclude that the age of all of the layer-7 features at Ushki-1 and Ushki-5 should be considered to be about 13,000 cal BP, at least until the earlier obtained old dates of 16,000–17,000 cal BP can be replicated.     

RADIOCARBON DATING ARCHAEOLOGICAL SAMPLES IN THE EASTERN MEDITERRANEAN, 1730 TO 1480 BC: FURTHER EXPLORING THE ATMOSPHERIC RADIOCARBON CALIBRATION RECORD AND THE ARCHAEOLOGICAL IMPLICATIONS*

The East Mediterranean Radiocarbon (Inter‐)Comparison Project (EMRCP) has measured time series of radiocarbon ages for known age samples of German oak (GeO) and for samples from the near‐absolutely placed Gordion juniper dendrochronology from central Anatolia. In this paper, we review the data for the calendar years from 1730 to 1480 bc , relevant in particular to controversy and debate concerning the absolute date of the Minoan eruption of the Santorini (Thera) volcano. We consider the issue of the radiocarbon (¹⁴C) dating of the Santorini eruption, and the problem of how this relates to the archaeological record and historical chronology of Egypt in light of the ¹⁴C data. We find that these ¹⁴C data, and other recent radiocarbon work, provide good grounds to be confident in the possibility of a robust radiocarbon‐based chronology for the eastern Mediterranean. In contrast, as the radiocarbon case becomes stronger, questions must be asked about some archaeological dating: in particular, at the site of Tell el‐Dab‘a in the Nile Delta of Egypt.     

Comments on relations West Norway ‐ Western Europe documented in petroglyphs

Dendrochronologic calibration of radiocarbon dates, which is of vital importance when such dates are compared with historical records, is discussed.

The nature and causes of variations in the past atmospheric radiocarbon content are briefly described. Different calibration curves are compared with available high‐precision data on radiocarbon in tree rings, and also with preliminary results from the joint efforts of U.S. scientists to establish an optimal calibration scheme.     

A NEW DIRECT RADIOCARBON AMS DATE FOR AN UPPER PALAEOLITHIC HUMAN BONE FROM SIBERIA

A new AMS radiocarbon date has been obtained from a Siberian human bone sample taken directly from a cranial fragment. The specimen comes from the north‐east Siberian site of Pokrovka 2 (55⁰19′46.30″N, 92⁰26′48.80″E). The remains consist of the anterior portion of the cranium or the superior part of the face; that is, the forehead and the roof of the eye sockets. Sadly, indifferent features of the frontal bone do not allow a confident diagnosis of the sex of the individual. The evidence suggests, however, that the remains are probably those of a young adult (teenager) and an anatomically modern human, rather than a Neanderthal. Radiocarbon dating was undertaken at the Oxford Radiocarbon Accelerator Unit (ORAU). The radiocarbon age determination of the bone fragment, 27 740 ± 150 bp (OxA‐19850), is one of the earliest direct dates for a modern human from Siberia. The Pokrovka cranial fragment dates to the middle Upper Palaeolithic of Eurasia and is broadly contemporary with the human remains from the famous eastern European site of Sunghir. When the radiocarbon age is compared with the Cariaco Basin ¹⁴C data set and the Greenland oxygen isotope record of NGRIP, it corresponds with Greenland Interstadial 5, a warmer phase of the Last Glacial period, although this is a preliminary conclusion, and is based on climate records that may or may not be wholly synchronous between the two locations.