Optically stimulated luminescence dating of Southern High Plains archaeological sites

The Southern High Plains of North America is rich in archaeological sites, but many are not well constrained chronologically, owing to a lack of material for radiocarbon dating. A program of optically stimulated luminescence (OSL) dating, applying mainly single-grain analyses, was therefore initiated. Many samples have independent age estimates from radiocarbon to check the OSL results, but OSL age estimates are also provided for those sites that otherwise lack secure chronological control. Sediment samples for OSL were obtained primarily from Paleoindian and Archaic localities, though include deposits of more recent age. Through the analysis of single grains, equivalent dose—the numerator of the age equation—is evaluated independently on numerous grains. The distribution of these values is relatively broad for some samples, and this is attributed to post-depositional mixing. Mixing is also evident in some samples with more narrow distributions. Selecting portions of the mixed distributions for age determination allows more accurate dating for some samples, but the nature of the distributions limits the resolution on others, conclusions that cannot be as easily drawn from multi-grain analysis. Where independent age control is available, most OSL results broadly conform; however, some samples show discrepancies that are not readily explained, but may relate to association or dose rate problems. This underscores the desirability of obtaining where possible suites of chronological evidence.     

Equivalent dose distributions from single grains of quartz at Sibudu,South Africa: context,causes and consequences for optical dating of archaeological deposits

Optical ages for 14 sediment samples collected from the post-Howiesons Poort, late Middle Stone Age (MSA) and final MSA deposits at Sibudu, KwaZulu-Natal, South Africa were reported in a companion paper (Jacobs, Z., Wintle, A.G., Duller, G.A.T., Roberts, R.G., Wadley, L. New ages for the post-Howiesons Poort, late and final Middle Stone Age at Sibudu, South Africa. Journal of Archaeological Science, 2008). These ages were based on equivalent dose (D_e) distributions that were overdispersed. In this paper, we investigate factors both internal and external to the grains that may contribute to such higher than expected overdispersion in single grain D_e values. Intrinsic factors accounted for some, but not all, of the observed scatter, and application of a set of rejection criteria filtered grains for which erroneous D_e values would otherwise be calculated. We investigated sediment mixing and differences in the beta dose received by individual grains in their burial environment as two likely reasons for the observed overdispersion. The scatter in D_e distributions for all the samples is best explained by grains that were deposited at the same time and which were well bleached, but that subsequently received a range of beta doses. A procedure is presented for adjusting the measured beta dose rate, and its associated error. We show that using a combination of single grain OSL measurements of D_e, the finite mixture model and adjustment of the beta dose rate, result in stratigraphically consistent ages. These ages are more consistent than the ages obtained from multiple grain aliquot D_e values and the average dose rates for each sample; the multiple grain ages are about 10% older, partly because of the variable dose rate and partly because these aliquots contained grains with undesirable OSL characteristics.     

On the intrinsic accuracy and precision of luminescence dating techniques for fired ceramics

Luminescence dating techniques have been used extensively for archaeological and geological samples. Such techniques are based on thermally or optically stimulated signals. This paper presents simulations of several luminescence techniques for equivalent dose (ED) estimation for ceramic materials containing quartz. The simulations are carried out using a recently published comprehensive kinetic model for quartz, consisting of 11 electron and hole traps and centers. The complete sequence of the experimental protocols for several thermoluminescence (TL) and optically stimulated luminescence (OSL) techniques are simulated using the same set of kinetic parameters. The specific simulated protocols are: additive dose TL protocol, predose technique (both additive and multiple activation versions), phototransfer protocol, single aliquot regenerative optically stimulated luminescence (SAR-OSL) protocol, and SAR thermoluminescence protocol (SAR-TL). One hundred random variants of the natural samples were generated by keeping the transition probabilities between energy levels fixed, while allowing simultaneous random variations of the concentrations of the 11 energy levels. The relative intrinsic accuracy and precision of the protocols are simulated by calculating the equivalent dose (ED) within the model, for a given natural burial dose of the sample. The intrinsic accuracy of these techniques is estimated by simulating natural irradiation of the samples with a known burial dose, followed by simulation of the luminescence method used to recover the estimated dose ED. The percent difference between the burial dose and the ED value represents the simulated accuracy of the luminescence technique. The relative intrinsic precision of these techniques is estimated by fitting Gaussian probability functions to the ED values obtained with the 100 model variants. It is found that the various techniques can reproduce natural paleodoses in the range 10 mGy–10 Gy with a typical intrinsic accuracy of +1 to 10%. Techniques based on single aliquot protocols were found in general to be more precise than techniques requiring the use of multiple aliquots. In addition, techniques based on interpolation of experimental data were found to be consistently both more precise and accurate than those based on extrapolation of experimental data.     

Investigation of past archaeological landscapes using remote sensing and GIS: a multi-method case study from Mount Ida,Crete

Spatial analysis in geoarchaeological applications can be improved by implementing a wider set of geoecological parameters, in order to provide more precise results. The aim of the paper is to show how geoscientific ground-truth and techniques can be adopted for detailed archaeological studies using a comprehensive set of environmental variables that might have influenced ancient settlement patterns. The project focuses on spatial patterns of archaeological sites as well as Bronze Age communication paths in Central Crete by applying a multi-method approach (surveying, remote sensing, DEM analysis, least-cost analysis, candidate site detection, predictive modelling, etc.). In contrast to conventional archaeological GIS applications this enhanced strategy offers promising prospects regarding landscape and settlement modelling.