Rice chaff in ceramics from the archaeological site of Sumhuram (Dhofar,Southern Oman)

The identification of the chaff used as temper in ancient ceramics represents a possible source of information about the area of origin of the pottery. This paper studies the occurrence of rice (Oryza sp.) chaff in potsherds from the archaeological site of Sumhuram (Dhofar, Sultanate of Oman). The information gathered at the site offers insight into commerce routes and networks to which the town belonged in the first centuries AD. The analysis of the plant material in the pottery and potsherds can also furnish interesting data on the ancient technologies of pottery production.     

The forest or the trees? Behavioral and methodological considerations for geochemical characterization of heavily-tempered ceramic pastes using NAA and LA-ICP-MS

In this paper, the utility of LA-ICP-MS for instrumentally separating clay and temper within pottery samples is examined through a well-known case study that has been previously characterized through NAA and petrography. Coarse Orange pottery is composed of kaolinitic clays heavily tempered within volcanic ash from the basalt-rich Tuxtla Mountains of southern Veracruz, Mexico. We attempt to address the following topics with analyses on this pottery: 1) can LA-ICP-MS replicate the same groups previously identified by NAA and petrography; 2) can instrumental isolation of the clay fraction within the pottery replicate known patterns in raw clay source geochemistry in the Tuxtla Mountains; 3) can data for both the clay and volcanic ash fractions of each pottery sherd be combined to simulate the bulk INAA data? The results demonstrate that the clay fraction of the pottery sherds can be isolated. Furthermore, the LA-ICP-MS data for the clay fractions display nearly identical chemistry to available NAA data for raw clay samples collected from geological contexts in the region. Instrumentally isolating the clay fraction in this case eliminates the homogenizing effects of adding a common temper and increases the chemical separation among groups making it easier to identify clay procurement strategies for each specimen. However, focusing only on the clay fraction ignores significant tempering variation. Attempts to simulate the bulk NAA by combining LA-ICP-MS data for clays and temper was reasonably successful in reestablishing the tempering variation lost by exclusive focus on clays, but such an approach could not replace the more precise data generated from NAA and petrography.     

‘ORGANIC TEMPER’ AND THE EARLY NEOLITHIC POTTERY PRODUCTION: INTERPRETATIONAL CHALLENGES

Well-preserved plant remains found in clay bodies of Early Neolithic pottery of Southeastern Europe have been largely understudied. The characteristics and provenance of this ‘organic temper’ remain mostly unknown, making interpretations obscure. Based on a range of research methods, this article explores the macro and micro plant remains within the pottery clays, considering such aspects as the use of domesticated versus wild plants and actual functional temper versus organic inclusions as background noise. This innovative approach is applied to explore three different Early Neolithic Balkan sites, demonstrating the importance in distinguishing between (a) deliberate addition of selected temper as a technological prerequisite; (b) sporadic occurrence of plant parts in (domestic) areas where pottery was made, (c) natural characteristics of the local clays containing organics and used as raw materials, and (d) plant use pointing towards more specific pottery-making techniques. Possible misinterpretations and pitfalls are discussed in using the applied integrated methodology, thus revealing crucial details on the variability of the technological approaches applied during the Early Neolithic of Southeastern Europe.     

Using hearths for temper: petrographic analysis of Middle Woodland charcoal-tempered pottery in Northeast Florida

Charcoal-tempered pottery is uncommon in North America, but was produced with notable frequency in Northeast Florida from ca. AD 300–600. Thirty-six thin sections of pottery were analyzed by petrographic analysis and compared to 10 clay samples in order to characterize the paste of charcoal-tempered wares in terms of charcoal and mineralogical composition and abundance, assess the number of clay sources used to make the pottery, identify the species of wood represented in charcoal inclusions, and infer techniques of ceramic production. This analysis identified four temper categories, three texture groups, and three distinct clay resources used to make charcoal-tempered pottery, all of which were likely local to Northeast Florida. Identified wood taxa include pine (Pinus sp.), cedar (cf. Juniperus sp.), cypress (cf. Taxodium sp.), and sassafras (Sassafras albidum), with pine suspected to be the most common. These genera of charred wood, which exhibit minimal shrinkage in the samples, along with the prevalence of bone and grog inclusions, indicate that hearth contents were processed as temper, sometimes in combination with quartz sand. Potential reasons for the use of hearth contents as temper are considered.     

Strength,Toughness and Thermal Shock Resistance of Ancient Ceramics,and Their Influence On Technological Choice

The basic underlying theory for the strength, toughness and thermal shock resistance of brittle multiphase clay ceramics, together with the measurement procedures to determine these parameters, are first outlined. Published experimental data obtained for test bars containing different types of temper and fired to a range of temperatures are then compared both with theoretical predictions and between themselves. The results confirm that to produce pottery with high strength requires high firing temperatures and low temper concentrations. Conversely, to produce pottery with high toughness and thermal shock resistance requires low firing temperatures and high temper concentrations, with platy or fibrous temper being most effective. There is no convincing published evidence that strength and toughness requirements were a significant factor in determining the technological choices (clay type, temper type and concentration, and firing temperature) in the production of pottery used as containers for transport and storage. In contrast, the routine use of high temper concentrations and low firing temperatures in the production of cooking pots suggests that the requirement for high thermal shock resistance was a factor that at least influenced technological choice in this case. In addition, there is some evidence that limestone and shell were, on occasions, deliberately chosen as temper in cooking pots. The need to take into account the crucial role that the full range of environmental, technological, economic, social, political and ideological factors have in influencing technological choice is also emphasized. This review highlights the fact that our current understanding of the factors determining strength, toughness and thermal shock resistance of clay ceramics is still far from complete. Further systematic measurements of these parameters, together with the establishment of a systematic database of the range of technological choices associated with the production of cooking pots, are therefore to be encouraged.     

CORRESPONDENCE AND DISCRIMINANT ANALYSES OF SAND AND SAND TEMPER COMPOSITIONS,TONTO BASIN,ARIZONA*

Geologists use petrographic modal analysis to relate fluvial sand composition to source rock composition, thus establishing provenance. Archaeologists seeking to establish provenance of sand temper in pottery can use similar petrographic methods, but their finer scale of investigation requires more precise statistical tools than those employed by geologists. A quantitative method for performing that task is presented. It utilizes correspondence analysis and discriminant analysis of logratio transformed point‐count data to define petrofacies, or sand temper resource procurement zones. The procedure is illustrated with sand and sand‐tempered sherd samples collected from the Tonto Basin, central Arizona; temporal trends in utilitarian ceramic production c. AD 100–1350 are reviewed.     

Ceramics Technology at Late Classic K’axob,Belize

Abstract

Excavation of a Late Classic Maya platform at K’axob, Belize, has revealed a suite of pit features and associated artifacts that are strongly suggestive of pottery production. Interpretation of the features as remnants of pit kilns used to fire pottery is bolstered by comparanda from the Andean region. Archaeometric and experimental replication studies also support the interpretation of this locale as one of pottery fabrication. Findings discussed include features identified as kilns, raw material suitable for temper, lumps of fired clay, ground stone, and expedient clay-working tools made of recycled pottery sherds. This research contributes to knowledge of the organization of Maya pottery production by providing the most comprehensive information presented to date on the technology of ancient Maya pottery fabrication and firing.     

Preliminary Characterization of Pottery by Cathodoluminescence and SEM–EDX Analyses: An Example from the Yeha Region (Ethiopia)

Yeha was a political and cultural centre of the Ethio‐Sabaean culture (D’MT) in northern Ethiopia and southern Eritrea. Part of the archaeological research deals with pottery of local, regional and imported origin. The research—investigations and examinations—tries to classify local pottery in two ways: first, by analysing the mineralogy of the temper using light microscopy and cathodoluminescence; and, second, by analysing the main element composition of the clay matrix using a scanning electron microscope with energy‐dispersive X‐ray detection (SEM–EDX). The cathodoluminescence shows that the temper material has differences in the colours of feldspars with a similar mineralogical composition. The results demonstrate that the pottery was produced by using local material that originates from various sources in the Yeha region and that the same raw materials were used in different types of pottery.     

Bipolar Reduction and Behavioral Variability During the Mid-Late Holocene at Eagle's Nest,Mount Sinai Harbor,New York

Recent syntheses for the Long Island Sound region argue for long-term cultural continuity amongst Holocene coastal hunter-gatherers. These notions derive primarily from studies of quartz lithic assemblages, which archaeologists argue show structural stasis over time. The remaining variability is explained with a ‘distance to source' model in which near-coastal sites tend to show a lack of quartz conservation while interior sites show quartz recycling. Under this model, technological strategies traditionally associated with raw material conservation (e.g., bipolar reduction) should not occur at near-coastal sites. We test the ‘distance to source’ model by reexamining a quartz lithic assemblage from Eagle's Nest-Long Island's richest Holocene coastal hunter-gatherer site. We find conclusive evidence for bipolar reduction in the site's “block/shatter” materials. Toolmakers used bipolar reduction to conserve raw material. Toolmakers also used anvils and bipolar reduction to open quartz cobbles, to stabilize freehand cores, to efficiently access cutting edges, and possibly to create crushed coarse quartz temper for pottery production. Our results point to previously unrecognized aspects of behavioral variability in the Eagle's Nest lithic assemblage and to possible revision of the ‘distance to source’ model. Similar variability may be present at other North American sites with quartz “block/shatter” material.     

Sponge Spicules in Pottery: New Data from Mali

Abstract

Until recently, the presence of sponge spicules in ancient ceramics has only been reported from South America. Current technological studies of Neolithic pottery from Sudan and Iron Age pottery from Mali provide evidence that sponge spicules are also a distinctive inclusion of some African ceramics. In this study, new data concerning the presence and quantitative variability of sponge spicules in West African Iron Age pottery from sites along the Niger River are discussed. Additionally, we discuss the potential archaeological insights offered by the study of sponge inclusions in pottery, and we consider methods for assessing whether or not these spicules were intentionally added as temper to vessels.     

Prehistoric Settlement,Mobility and Societal Structure in the Peak District National Park: New Evidence from Ceramic Compositional Analysis

Detailed compositional and technological analysis of a large assemblage of prehistoric ceramics from numerous sites situated within the Peak District National Park has been used to explore the settlement patterns, societal structure, mobility and interaction of the populations that inhabited this area during the Early Bronze Age to Early Iron Age. A surprising pattern emerges of the widespread dominance of a single, geographically restricted temper type, which appears to have been transported and mixed with locally procured clay and used to produce pottery at numerous different sites. The distribution of this and several other compositional groups are defined via thin‐section petrography and compared to raw material field samples. The resulting patterns are used to assess the validity of previous theories about prehistoric life in this region during the third to first millennia bc .     

Initial evidence of plant and animal-origin organic additives from the second-century bce earthen plaster of rock-cut caves of Karla,India*

Analytical investigations through phytochemical screening, scanning electron microscope (SEM) and light microscopic observation of the earthen plaster of Karla Caves of western India identified the presence of antifungal, antibacterial and insect repellent Careya arborea stem fibres as a vegetal additive. The scanning electron microscopy with energy-dispersive X-ray spectrometry (SEM-EDX) study also revealed the inclusion of rice (Oryza sativa) husk as a plant additive in the plaster. In the high rain-fed coastal regions of western India, the antimicrobial, antioxidant and termite-resistance properties of C. arborea helped the survival of the plaster in unfavourable climatic conditions. Besides, the C. arborea and rice husk together played a role in reducing cracks, decreasing the density, and imparting a plasticity and a durability to the plaster. The liquid Fourier-transform infrared spectrometer (FTIR) of organic extracts revealed carboxylic acid (fatty acids)-based additives in the earthen plaster. From the gas chromatography-mass spectrometry (GC-MS) analysis of the plaster, the presence of animal milk fat, animal and vegetable fat, and vegetable oil was identified, and probably used to strengthen the earthen plaster for their resistance to tensile stress. The analysis also diagnoses the inclusion of methyl commate B, a resinous material obtained from the Burseraceae plant family, which has antimicrobial properties, through GC-MS analysis.     

江苏泗洪韩井遗址水稻驯化的植硅体证据及相关问题

韩井遗址顺山集文化一期由洼地和水沟组成的水稻田,很可能是目前发现的最早与人类驯化水稻相关的遗迹,植硅体分析也在一定程度上对这一论断给予支持。从顺山集文化一期到二期,韩井遗址均以水稻双峰型植硅体居多,而且其百分比和浓度(均值)均呈现增多的态势;水稻扇型和横排哑铃型植硅体表现出相反的规律。与同时期顺山集遗址相比,韩井遗址的水稻扇型植硅体尺寸偏小。水稻扇型植硅体鱼鳞状纹饰个数和水稻双峰型植硅体形态测量用于水稻驯化程度的判定上,表现出非协同性。陶胎中掺入破碎稻壳是韩井遗址水稻栽培与驯化实践的又一反映。     

Tracing the clay source of Nasca polychrome pottery: results from a preliminary raw material survey

This paper describes the results of the first season of a survey in which clays suitable for the production of Nasca polychrome pottery were collected in an effort to (1) determine the geological variability of clay sources in the Nasca region and (2) match clays compositionally to paste groups from previous provenance analyses. Clays were collected, processed, fired, and analyzed using neutron activation. The results demonstrate that clays in the region were compositionally heterogeneous, and that the clay source for the majority of Nasca polychrome pottery sampled thus far can be traced to lower valleys in the region near the ancient ceremonial center Cahuachi. The results have implications for understanding the nature of polychrome pottery production in the Nasca region, and suggest centralized production near the ceremonial center of the majority of painted ceramics consumed in the Southern Nasca Region.     

Identical rock types with different chemistry: sourcing phyllite-tempered Hohokam pottery from the Phoenix basin,Arizona

The organization of ceramic production and distribution among the ancient Hohokam of the Phoenix basin, Arizona, has been documented in recent years with much detail. Based on diverse temper and clay compositions, the provenance of individual ceramics is routinely determined with considerable precision. One exception is phyllite-tempered pottery, which was made in one corner of the basin but also across a broad upland zone adjacent to the north. The phyllite-tempered pottery from different production sources cannot be distinguished on the basis of their temper type. As shown with assays with an electron microprobe, however, both the temper and clay fractions are chemically diverse and geographically distinct, allowing many of the phyllite-tempered wares to be sourced. Among the phyllite-tempered ceramics consumed in the Phoenix basin, some are shown to have been made locally, but, surprisingly, large numbers were imported from the northern uplands. Their numbers support the idea that the connection between the Phoenix basin and the northern uplands was a prominent component of the Hohokam regional economy despite the great difference between them in settlement size and density.     

A Late Roman ceramic production from Pompeii

The Via Lepanto site is one of the best examples showing how the Vesuvian region was partially reconstructed and earlier re-occupied after Vesuvius's eruption in the year 79 AD. The large amount of ceramic finds illustrates the typology in use in this area during the IV and V century AD. Analyses were focused on table and cooking ware productions. Archaeometric data were obtained using chemical and minero-petrographical methods (OM, XRD, XRF and SEM). Grain size measurements using Image Analyses on thin sections and a geochemical comparison with clayey deposits outcropping in the Campania region permitted the identification of the raw materials used for these pottery productions. XRD and SEM completed the data set, establishing the protocols used for pottery production in the Pompeii area during Late Roman period. The Via Lepanto site was part of an exchange network of markets with a periodic frequency, where locally produced and imported pottery was sold, indicating a flourishing network of exchanges spanning short, medium and long distances.     

Slave Communities and Pottery Variability in Western Brazil: The Plantations of Chapada dos Guimarães

In the region of Chapada dos Guimarães, Western Brazil, planters relied heavily on slave labor during the eighteenth and nineteenth centuries. In this article, we examine the locally produced pottery found on slaves contexts in five rural sites of this region. Based in data from probate inventories and the pottery decorative variability we suggest that slaves used decorated pottery to express cultural and social differences.     

THE ALPS—A BARRIER OR A PASSAGE FOR CERAMIC TRADE?*

The Alps as a barrier : ceramic remnants of the so‐called Laugen‐Melaun culture (c. 11th to c. sixth centuries bc ) can be found in the northern Italy (Trentino/Alto Adige)—eastern Switzerland—Liechtenstein and western Austria region. A petrographic study of 454 sherds from this area covering a time span of 500 years reveals the following. (1) The pottery from the Trentino/Alto Adige contains a predominantly volcanic temper, which can be linked to the volcanic rocks of the Bolzano area—in other words, to the core region of this culture. This material is therefore of a local/regional production. (2) These ceramics were imported from the Bolzano region to southeastern Switzerland (the Inn Valley) and the amount of imported pottery decreases markedly from the 11th century bc (approximately 70% imported) to the seventh to sixth centuries bc (approximately 10% imported). (3) No imported pottery can be detected north of the Alpine crest in Switzerland, Liechtenstein and Austria, and in this region serpentinite temper was preferred by ancient potters. These results demonstrate that long‐lasting contacts and ceramic trade existed between the populations of the Inn Valley and the Trentino/Alto Adige. Such contacts could have been motivated by intermarriages between the two populations and/or economic exchange. The potters north of the Alpine ridge adopted the Laugen‐Melaun style and produced such pottery locally. The use of serpentinite temper is puzzling and not related to any technological advantage. (Could it be recycled material? Or does it have any sociocultural specificity?) The Alps as a passage : 59 fragments of a black gloss ware, the so‐called Campana, unearthed at 11 Late Latene sites (second to first centuries bc ) in Switzerland and neighbouring Germany were analysed chemically by X‐ray fluorescence. The results revealed: (1) that all of them were produced either in Italy or Lyon and then exported to the north; (2) that two principal south–north exchange routes existed, (a) fluviatile, along the Rhône–Rhine corridor and (b) trans‐Alpine, using the Alpine passes, such as the Simplon and the Grand St Bernard.     

PETROGRAPHIC MODAL ANALYSIS - A NECESSARY COMPLEMENT TO CHEMICAL ANALYSIS OF CERAMIC COARSE WARE

Bulk chemical analysis is shown to be insufficient for the archaeometric interpretation of coarse ware pottery. Accompanied by quantitative petrographic analysis of the temper much more conclusive information can be obtained at little more expense. Three small groups of prehistoric pottery from Switzerland have been examined with both techniques, showing that expensive chemical bulk analyses may be obsolete or even misleading, and in any case need further confirmation and interpretation by petrographical means. Assuming a rigorous sampling strategy, the number of analyses necessary for valid statements can be substantially reduced relative to those necessary for the statistical interpretation of bulk analyses only.     

Characterization of Iron age pottery from eastern Turkey by laser- induced breakdown spectroscopy (LIBS)

Selected pottery sherds coming from the Ayanis, Dilkaya and Karagündüz excavations in eastern Turkey and dated from the Early to Middle Iron Age were examined as regards their composition by using laser-induced breakdown spectroscopy (LIBS). The objective of the study was first to investigate the potential of the LIBS technique in the compositional analysis of pottery and further to explore correlations in spectral data, by using chemometrics methods that would possibly enable discrimination among different sherds. This work is part of a broader study aiming to examine clay variability both before and during the Urartian State period and to explore possible relationships and differences among pottery objects from fortresses and settlements or settlements and cemeteries on the basis of the clay composition of sherds. Preliminary results demonstrate that by using the LIBS technique it is possible to analyse pottery sherds in qualitative and semi-quantitative ways, providing information on the clay and slip composition. Furthermore, encouraging results have been obtained by carrying out principal component analysis (PCA) on the LIBS spectra, which suggest that in certain cases, it is possible to directly correlate spectral information with the origin of pottery sherds.