Carbon isotope fractionation between diet,breath CO2, and bioapatite in different mammals

The carbon isotope fractionation between tooth enamel bioapatite, breath CO₂, and diet was measured for voles, rabbits, pigs, and cattle on controlled diets. The measured fractionation (expressed as isotope enrichment ɛ*) between enamel and diet was 11.5 ± 0.3‰, 12.8 ± 0.7‰, 13.3 ± 0.3‰, and 14.6 ± 0.3‰ for these respective species. There is a 1:1 correlation between ɛ*_{breath–diet} and ɛ*_{enamel–diet} (r² = 0.94, p < 0.01), whereas our data do not resolve significant inter-species differences in ɛ*_{enamel–breath}. These findings are consistent with the hypothesis that inter-species differences in ɛ*_{bioapatite–diet} are primarily a result of differences in digestive physiology, rather than differences in the magnitude of fractionation between mineral and body fluid.     

Analyzing the process of domestication: Hagoshrim as a case study

Recent excavations at the Neolithic site of Hagoshrim, northern Israel, have yielded a large assemblage of skeletal fragments, representing mostly caprines, cattle and pigs. The three layers of the site's occupation span approximately 2000 years of a crucial period in the domestication of these taxa in the southern Levant, including Pre-Pottery Neolithic C (Layer 6, 7562 ± 85 BP and 7735 ± 55 BP) and the Pottery Neolithic cultures, Jericho IX (Layer 5, 6725 ± 120 BP) and Wadi Raba (Layer 4, 6505 ± 120 BP). Therefore, this site provides an outstanding opportunity to study the process of domestication in a comparative manner, both across taxa and through time. We used kill-off patterns, size reduction and changes in body proportions, and introduced statistical methods to discern the different stages of the domestication process for each taxon. Pig remains reflect simultaneous changes at the end of the 7th millennium BP: kill-off patterns, size and proportions of cranial and post-cranial elements all change between Layer 5 and 4 with no significant changes between Layer 6 and 5. Gradual changes—both between Layer 6 and 5 and between Layer 5 and 4—were found only for cattle, while caprine remains exhibit no changes throughout the site's occupation. These results can be explained in light of the differences between the taxa in terms of their life history strategies, among other things, that can be viewed as pre-adaptations to domestication.     

Reconstructing northern Chinese Neolithic subsistence practices by isotopic analysis

Stable isotope signatures of both human and non-human animal bone samples indicate that Neolithic farmers of the Yellow and Wei River basins in China potentially cultivated millet for two reasons: as a staple for human consumption and as fodder for domesticated animals, specifically pigs, dogs, and perhaps chicken. Bone samples were analyzed from four Neolithic sites: Jiangzhai, Shijia, Xipo, and Kangjia, spanning the time period from 7000 to 4000 years ago. A combination of very high carbon isotope ratios (δ¹³C = −7.7 ± 0.4‰) and low nitrogen isotope ratios (δ¹⁵N = 7.5 ± 0.5‰) in samples of Xipo pig and dog bone suggests that these monogastric animals consumed substantial quantities of C₄ plants, almost certainly millets. In fact, the proportion of C₄ plants in animal diets appears to have been even greater than that in human diet. Stable isotope values (δ¹³C = −10.0 ± 0.8‰; δ¹⁵N = 8.3 ± 0.5‰) of human bone collagen recovered at Jiangzhai and Shijia indicate a staple role for millets, as well as the consumption of both wild and other non-C₄ domesticated plant foods. As millet agriculture and animal husbandry apparently depended on one another, a strong mutualism between them was likely established in northern China during the Neolithic. We propose that variable redistribution of agricultural products between humans and animals, depending on the availability of wild resources and annual fluctuations in agricultural output, helped ensure the stability of Neolithic human subsistence in the Yellow and Wei River basins.     

Assessment of material characteristics of ancient concretes,Grande Aula,Markets of Trajan,Rome

The Grande Aula, or Great Hall, of the Markets of Trajan (AD 96 to 115) is an intact example of the domed, concrete architecture of imperial Rome. Petrographic, x-ray diffraction, chemical, and SEM analyses demonstrate that wall mortars contain Pozzolane Rosse volcanic ash aggregate (harenae fossiciae) and strätlingite, a complex calcium aluminate cement hydrate (C₂ ASH₈) that gives modern cements good durability and compressive strength. Specific gravity tests and a new petrographic method for assessing bulk densities indicate unit weights of about 1750 kg/m³ for the wall mortars and 1430–1640 kg/m³ for the pumice bearing, vaulted ceiling mortars. Innovative point load source tests record the tensile strengths (f_t) of the aggregate and interfacial elements of the conglomeratic concrete fabric. These suggest f_t of about 2.7 MPa for brick, 1.2 MPa for Tufo Lionato tuff, and 0.9 MPa for Tufo Giallo della Via Tiberina tuff coarse aggregate (caementa), based on a tentative, approximate correlation with splitting (Brazilian) tests. The pozzolanic mortar and interfacial zones have lower f_t in the range of 0.8 MPa to 0.5 MPa. The relatively low mortar strength and its somewhat tenuous adhesion to the coarse aggregate suggests that the caementa may have arrested the propagation of tensile microcracks that formed in the mortar, thereby increasing the composite tensile strength of the concrete. Roman builders selected the complex aggregate mixes to optimize the performance of the wall and vault concretes.     

Selective hunting of pine marten,Martes martes,in Late Mesolithic Denmark

Pine marten, Martes martes, is the dominating fur prey at three contemporaneous Danish Late Atlantic sites, Agernæs (EMNI = 34), Ringkloster (EMNI = 41) and Tybrind Vig (EMNI = 26). All skeletal elements are represented and the only marks present on the skeleton are those consistent with skinning. Burned teeth in the three populations suggest either new hunting methods or a ritual act. Ringkloster is on the mainland, while Tybrind Vig and Agernæs are island localities. Morphometric data indicate that the subfossil population of larger individuals was maintained on the mainland due to free migration, while the animals in the subfossil island populations had decreased in size in the Late Atlantic.     

Colonization of Northern Eurasia by Modern Humans: Radiocarbon Chronology and Environment

The distribution of frequencies of radiocarbon-dated Palaeolithic sites in northern Eurasia shows three peaks of 40–30, 24–18 and 17–1 ka bp. We argue that these peaks reflect the waves in the colonization of that area by Anatomically Modern Humans stemming from Central and Eastern Europe and caused by environmental stress.     

From Lithics to Spatial and Social Organization: Interpreting the Lithic Distribution and Raw Material Composition at the Final Palaeolithic Site of Kettig (Central Rhineland,Germany)

During the Final Palaeolithic Federmessergruppen period, a wide range of siliceous raw materials was used in the Central Rhineland (Germany). Beside materials from the immediate region, exogenous resources such as flint from up to 100 km away in the Meuse drainage area and the moraines of the Saalian glaciation were exploited. At Kettig, the spatial distribution of different lithic raw materials and analysis of several categories of burnt finds allow the characterization of the settled area in space and time. While adequate, good-quality raw material was available in the Central Rhineland, the regular use of exogenous raw materials at Central Rhineland sites also demonstrates the necessity of maintaining regular social contacts with other groups in neighbouring regions.     

Sources of Archaeological Obsidian on Sakhalin Island (Russian Far East)

Instrumental neutron activation analysis was performed on 79 obsidian tools and flakes from 35 sites on Sakhalin Island dating from Upper Paleolithic (c. 19,000 bp ) to Early Iron Age (c. 2000–800 bp ). Due to the absence of volcanic glass on Sakhalin Island, raw materials from the nearest obsidian sources on Hokkaido Island, such as Oketo, Shirataki, Tokachi-Mitsumata, and Akaigawa, were also analysed. A strong correlation between the chemical compositions of obsidian artefacts from Sakhalin and volcanic glass sources from Hokkaido was discovered. In particular, the Oketo and Shirataki sources were used for tool manufacturing throughout all of Sakhalin Island's prehistory. The distances between sources and archaeological sites range from 200–1000 km. The intensive exchange of raw materials continued and even intensified after the appearance of the La Pérouse (Soya) Strait between Hokkaido and Sakhalin about 10,000–8000 bp. The Sakhalin Island populations were deeply involved in the obsidian exchange network centered on Hokkaido.     

The ‘Headless Romans’: multi-isotope investigations of an unusual burial ground from Roman Britain

Recent excavations at Driffield Terrace in York (Northern England) revealed an extremely unusual Romano-British cemetery of probably all-male composition, more than half of the individuals decapitated and with high incidence of other peri- and antemortem trauma. This paper presents the results of multi- (carbon, nitrogen, oxygen and strontium) isotopic analyses of bone and dentine collagen (n = 68) and tooth enamel (n = 18) which were conducted to obtain further information on the identity of these individuals and, more generally, in order to investigate the relationship between burial rite and geographical origin in a Roman provincial capital. The results show that the childhood origins of the “Headless Romans” were significantly more diverse than those of humans from other cemeteries in Roman York, but they demonstrate also that similar, unusual burial rites do not necessarily indicate a common geographical origin. Of particular interest were two individuals whose diet contained a significant proportion of C₄ plant (probably millet)-based protein. These are the first such isotope values observed in Britain from any archaeological time-period. Millet was not cultivated in the British Isles in antiquity and the results therefore demonstrate the value of palaeodietary data for assisting in isotopic mobility studies.     

Magnetite grain-size analysis and sourcing of Mediterranean obsidians

The potential of magnetic grain-size variations as an obsidian source characteristic is investigated using geological and archaeological obsidians from five islands of the Mediterranean Sea: Lipari, Sardinia, Palmarola, Pantelleria, Melos. Four parameters are used: magnetic (χ) and anhysteretic (χ_a) susceptibilities, saturation isothermal remanent magnetizations at room (SIRM₂₉₃) and liquid nitrogen (SIRM₇₇) temperature. The ratio S_T = SIRM₇₇/SIRM₂₉₃, which depends on the superparamagnetic grains relative abundance, varies little in each individual site, with the exception of Lipari which is characterized by large variations and the highest content of superparamagnetic grains. The χ_a vs. χ plot ( King et al., 1982) shows some within-site dispersion of the samples; but the ratio Q_a = χ_a/χ, which is strongly influenced by the single domain grains content, is characteristic for each site. The combined use of the King and Q_a vs. S_T plots discriminates the samples from most of the sites and suggests that the grain-size analysis is a promising approach in sourcing obsidian archaeological artefacts. Moreover, the measurements of the four parameters used are simple, quick and feasible with no or little damage to archaeological finds.     

Ancient long-distance trade in Western North America: new AMS radiocarbon dates from Southern California

Eleven Olivella biplicata spire-lopped shell beads from six sites located 250–365 km inland from the Pacific coast of southern California produced AMS dates between 11,200 and 7860 CAL BP. Olivella shell beads were well-documented items of prestige and media of exchange in Native California, and recovery of these examples from inland contexts indicates low-level exchange between resident populations of the coast and the southwestern Great Basin by at least 10,300–10,000 CAL years BP. These findings represent some of the earliest unequivocal evidence for long-distance trade in western North America and push the antiquity of this important form of inter-group interaction back several thousand years earlier than previously thought.     

Methods for inferring paleohabitats from the functional morphology of bovid phalanges

The functional morphology of postcranial remains can be used to infer habitat preference. This approach is typically considered an “ecomorphological” method, and has frequently been applied to bovid postcranial remains. Methods for predicting habitat preference from bovid postcrania currently exist for femora, metapodials, and astragali. Here we describe three methods for predicting paleohabitats using measurements of African bovid phalanges (proximal, intermediate, and distal). The proximal phalanx method correctly predicted the habitat preference for 130 of 183 modern bovid specimens (71.0%, 2.8 times better than chance, p < 0.0001). The intermediate phalanx method correctly predicted the habitat preference for 115 of 163 modern bovid specimens (70.6%, 2.8 times better than chance, p < 0.0001). The distal phalanx method correctly predicted the habitat preference for 87 of 122 modern bovid specimens (71.3%, 2.8 times better than chance, p < 0.0001). These accuracies compare well with those of existing such methods (1.8–3.4 times better than chance). Analysis of the probabilities associated with the habitat predictions allows confidence thresholds to be established that identify specific predictions which have <5% chance of being in error. This raises the effective accuracy of the methods to 95%. Extensive exploration and manipulation of the underlying data demonstrate that the habitat predictions are generally robust, and are relatively independent of body weight, taxonomy, and sample composition. These methods are broadly applicable, relatively accurate, and can be used to generate independent predictions of habitat from different elements, and thus constitute a useful approach to inferring past environments.     

Geo-Ethnoarchaeology of Pastoral Sites: The Identification of Livestock Enclosures in Abandoned Maasai Settlements

The earliest food producers in Africa were mobile pastoralists who left limited archaeological traces. As a result archaeologists studying the spread of food production in the region have difficulty distinguishing early pastoralists from hunter-gatherers with whom they interacted. This geo-ethnoarchaeological study contributes to the resolution of the problem through identification of sediments distinctive of livestock enclosures, and thus of pastoral settlements. Sediments were sampled in and around currently occupied and recently abandoned Maasai livestock enclosures ranging in age between one and 40 years. Twenty to thirty years after site abandonment, there is no visible difference between enclosure and regional sediments. Micromorphological, mineralogical, and phytolith analyses, of enclosure sediments, however, allow differentiation of enclosure from regional sediments. Our results show that a unique undulating microlaminated structure is distinctive of enclosure sediments. Enclosure sediments, especially small stock, also contain a rare mineral, monohydrocalcite (CaCO₃ . H₂O). In addition, large amounts of opal (SiO₂ . nH₂O), in the form of phytoliths, are found in enclosure relative to regional sediments. These differences are likely to be preserved in the archaeological record, and this approach will allow better understanding of the spread of pastoralism in Africa and elsewhere.     

Taphonomic implications of roosting behavior and trophic habits in two species of African owl

As some of the most common predators of micromammals, owls are implicated in the formation of many fossil assemblages. Actualistic research on owl-accumulated assemblages has tended to focus on owls roosting in caves. Comparatively few data are available on the roosting behavior, and prey preference of owls in open habitats. This paper presents observations on the roosting and prey habits of two sympatric species of owl in the Serengeti region of northern Tanzania, the Barn Owl, Tyto alba affinis, and the Spotted Eagle Owl, Bubo africanus. The Barn Owl and Spotted Eagle Owl are found to segregate by roosting habit, with Barn Owls occupying cavity roosts and Eagle Owls appearing on the ground or in tree crowns. Previous studies comparing these two species suggested a close similarity in trophic habits. A comparison of large samples (MNI = 1012) at cavity and exposed roosts shows identical taxonomic representation, though differences are found in the relative abundance of some taxa and significant differences in prey body mass.     

Cultural and trade practices in Sincu Bara (Senegal): a multi-proxy investigation

The Sincu Bara site in Senegal is one of the most famous archeological sites in Western Africa. Here we present the results of a multi-proxy study that combined microscopic analyses, carbon content, stable carbon isotope (δ¹³C) and radiocarbon (¹⁴C) measurements. This investigation exhibits a chronological framework in two phases: from 400 yr AD to 650 yr AD and 650 yr AD to 900 yr AD. Furthermore, it shows that besides basic potteries, some potsherds are notable for a temper exclusively made with human-harvested C4 plants. Finally, the ¹⁴C analysis performed on the organic slip strongly indicates the use of bitumen or bitumen-derived products for red slip preparation. This suggests the establishment of trade relationships with Nigerian and/or Trans-Saharan populations as early as 400 yr AD.     

Coal used for Fuel at Two Prehistoric Sites in Southern France: Les Canalettes (Mousterian) and Les Usclades (Mesolithic)

Charcoal analysis—the study of charcoal from archaeological contexts—is designed to reconstruct palaeoenvironment and human use of wood. At two prehistoric sites in the Causse du Larzac (France)—Les Canalettes (Mousterian) and Les Usclades (Mesolithic)—charcoal analysis has revealed specimens whose anatomical structure was abnormally compressed in transverse section. The authors conducted experiments to determine how the compression could have occurred. The result was the first evidence for lignite in Palaeolithic settlements. Lignite fragments in a hearth suggest local Palaeolithic people used it for fuel. The lignite could have come from major coal outcrops within 7 to 15 km of the sites. Coal use is otherwise unknown for Palaeolithic cultures in France, and its use at Les Canalettes during the last glacial is the oldest recorded instance. Coal may have been used for fuel primarily because wood became scarce during the last glacial.     

Infra-red Photoacoustic and Secondary Ion Mass Spectrometry Measurements of Obsidian Hydration Rims

A procedure has been developed for measuring obsidian hydration rim thicknesses on archaeological artefacts using infra-red photoacoustic spectroscopy (IR-PAS). Calibration of the IR-PAS values with depth was completed using secondary ion mass spectrometry (SIMS) and optical microscopy to relate the quantity of diffused water to the measured thickness of the hydration layer. By monitoring the absorbance intensity at 1630 cm⁻¹wavenumbers, hydration rims between approximately 1 μm and 12 μm may be accurately measured and used for chronometric age estimates. SIMS depth profiling has the ability to measure layers less than 1 μm thick, extending the age calibration to samples of less than 100 years in age.     

Methods for inferring paleohabitats from discrete traits of the bovid postcranial skeleton

Various “ecomorphological” methods exist for using the functional morphology of bovid postcranial remains to reconstruct paleohabitats. Most such methods use measurements, but both Gentry [The Bovidae (Mammalia) of the Fort Ternan fossil fauna, in: L.S.B. Leakey, R.J.G. Savage (Eds.), Fossil Vertebrates of Africa, vol. 2, Academic Press, London, 1970, pp. 243–323] and Köhler [Skeleton and Habitat of Recent and Fossil Ruminants, Münchner Geowissenschaftliche Abdhandlungen 25 (1993) 1–88] have identified numerous discrete (non-metric) traits of the bovid postcranial skeleton that are said to be indicative of habitat preference. However, these traits have not been systematically tested on a modern bovid sample. We report here such a test. Eighty-six non-metric characters were evaluated using a sample of modern African bovids (n = 197). Of the 86 characters, 48 were either insufficiently defined or exhibited too much intra-individual variation to be potentially indicative of habitat. Two characters were invariant in the sample. Of the remaining 36 characters, 11 were sufficiently correlated with habitat preference (Cramer's V > 0.5) to be of some potential use in reconstructing paleohabitats. These characters are primarily concentrated on the phalanges, and provide a means by which fragmentary phalanges can be used for habitat reconstruction, albeit at a broad level of resolution (open or closed habitat). The estimated accuracy of these methods is greater than 80%. Their use on fragmentary remains may lessen the bias introduced by basing habitat reconstructions on more complete fossils.