INVESTIGATION OF THE COLOURING MATERIALS OF FUSTAT CARPET FRAGMENTS

The Benaki Museum (Athens, Greece) possesses 50 fragments that, according to its archives, are recorded as having a provenance in the Fustat area. The objects are divided into three groups on the basis of the techniques employed. Most (eight) of the objects included in the present study belong to group A (8th–11th centuries). A few (five) fragments belong to groups B and C, which include objects dated up to the 18th century. The goal is to identify the colouring compounds contained in microsamples removed from the selected Fustat carpet fragments. Identifications are achieved using high‐performance liquid chromatography (HPLC) with photodiode array detection (PDA). The following compounds are identified repeatedly in many samples: laccaic acid A and other laccaic acids (components of Kerria lacca, Kerr), alizarin, purpurin and rubiadin (madder components), luteolin, apigenin and chrysoeriol (components of Reseda luteola L.), and indigotin and indirubin (components of indigoid dyes). In one sample, the type C compound (marker compound for the identification of soluble redwoods, Caesalpinia trees) is identified. The HPLC profiles collected for the samples in which madder components are detected suggest that most probably Rubia tinctorum L. (and not Rubia peregrina L.) was used during dyeing.     

THE ARCHAEOINTENSITY OF THE EARTH'S MAGNETIC FIELD RETRIEVED FROM PAMPEAN CERAMICS (SOUTH AMERICA)

Absolute intensity determinations using the Coe variant of the Thellier method have been carried out on some selected pottery fragments collected in the wetlands of the lower Paraná (Pampean region, Argentina) in order to construct the first archaeointensity master curve for South America. Associated radiometric ages range between 1640 ± 70 and 730 ± 70 bp . Twenty‐one samples (five fragments) out of 46 studied (eight fragments) provided successful absolute intensity determinations. The fragment‐mean archaeointensity values obtained in this study range from 21.9 ± 2.3 to 42.6 ± 5.4 μT, with corresponding virtual axial dipole moments (VADMs) ranging from 4.0 ± 0.5 to 8.1 ± 1.0 x 10²²Am². This corresponds to a mean VADM of (6.4 ± 1.8) × 10²² Am². The synthetic record retrieved from southern Argentina and Brazil consists of 17 mean archaeointensities distributed between approximately ad 700 and ad 1700. The data set shows several distinct periods of fluctuations of quite large intensity. However, most data are concentrated into a relatively narrow time period from ad 950 to ad 1300. Three general features may be detected: the time intervals from about ad 950 to 1130 and 1350 to 1480 are characterized by quite monotonic increases of geomagnetic intensity, while some decrease is observed from ad 1150 to 1280. These variations may be speculatively correlated to climate changes over multi‐decadal time scales. Important differences are observed between the data and the geomagnetic field predictions derived from recently reported global models, which reinforces the importance of regional reference curves for dating purposes.     

Micromorphological Study of Concotto Surfaces Protected by the Avellino Eruption in 3945 ± 10 cal. BP at the Early Bronze Age of Afragola Village in Southern Italy

ABSTRACT

The term Concotto refers to fragments or patches of hard heated clay that derive from living surfaces, walls, and ovens. Concotto fragments are found throughout the Italian peninsula and date from the Neolithic to the Iron Age. Current studies express contradictory opinions about whether or not the Concottos on living surfaces represent intentionally constructed surfaces or the secondary products of the contact between hot embers and sediments. This study uses micromorphological analysis to investigate the function and composition of Concotto surfaces from several domestic structures at the Early Bronze Age village of Afragola in southern Italy. Afragola is an exceptionally preserved agricultural village that was covered by almost 1?m of volcanic ash during the Vesuvius eruption in 3945?±?10 cal. BP. The Concottos at Afragola are hard, red surfaces that are typically associated with burned materials. Micromorphological analysis reveals that the Concottos were intentionally made by laying down patches of clay and then heating them to create a hard, flat surface. This study explores the potential uses of the Concotto as cooking surfaces during the Early Bronze Age of southern Italy.     

Thelodont fish and conodonts from the Early Devonian of Reefton,New Zealand

Thelodont scales and associated fragments of conodont elements identified as Turinia sp. cf. Turinia australiensis and Ozarkodina sp. cf. Ozarkodina buchanensis respectively are described for the first time from the Early Devonian Murray Creek Formation of Reefton, New Zealand. The conodont and thelodont components of the fauna suggest a late Pragian to early Emsian age for the assemblage.     

Umkomasia (megasporophyll): part 1 of a reassessment of Gondwana Triassic plant genera and a reclassification of some previously attributed

The genus Umkomasia, a megasporophyll, belonging to the pteridosperms (seed ferns) in the family Umkomasiaceae (Corystospermaceae), is reassessed comprehensively worldwide. All previous records are analysed. Certain fertile structures previously attributed are reclassified. Umkomasia is shown to be restricted to the Triassic of Gondwana where it is associated with the genus Pteruchus, a microsporophyll, and the genus Dicroidium, a vegetative leaf. It is well represented from Argentina, Australia and southern Africa where the Molteno Formation is by far the most comprehensively sampled with eight species described. Two specimens from the upper Permian of India attributed to Umkomasia are reclassified as cf. Arberiopsis sp. A whorled fertile structure from Antarctica, previously assigned to Umkomasia, is reclassified in a new genus as Axsmithia uniramia. Another compression fossil and the permineralized Umkomasia resinosa remain as valid records from Antarctica. The material described as Umkomasia from the Triassic of China is reclassified as Stenorachis asiatica. The Lower Jurassic record from Germany is placed in a new genus as Kirchmuellia franconica. The records of Umkomasia sp. from the Rhaetic of Germany are reclassified as cf. Kirchmuellia sp. and the single specimen from the Jurassic of Libya as genus et sp. indet. The Lower Cretaceous record from Mongolia has been reclassified by other researchers as Doylea mongolica. A pictorial key to Umkomasia species is provided, geographic and stratigraphic distributions are tabulated.     

A STUDY ON LATE MEDIEVAL TRANSPARENT‐GLAZED POTTERY AND ARCHAIC MAJOLICA FROM ORVIETO (CENTRAL ITALY)*

Nineteen samples of medieval transparent‐glazed pottery and archaic majolica from Orvieto (central Italy) were studied. They were classified by archaeological criterion as follows: five transparent‐glazed fragments with green and brown decorations (first half of the 13th century), eight green transparent‐glazed fragments (13th century) and six tin‐glazed fragments with green and brown decorations (second half of the 13th century). SEM–EDX, XRD (the Rietveld method) and XRF were used to characterize the chemical and mineralogical compositions both of the bodies and the coatings. In all of the samples, the paste is Ca‐rich with CaO contents as high as 13–20 wt%. The mineralogical composition is compatible with a firing temperature of about 950°C, which is the typical temperature reached in a wood kiln. No difference was observed between the bodies of transparent‐ and tin‐glazed pottery. In the case of transparent glazes, the burial conditions lead to heavy weathering of the samples. However, on the basis of the analyses carried out in non‐weathered areas, the typical composition is PbO 55–65 wt%, SiO₂31–35 wt%. In tin glazes, the tin is scattered on the mass of the glaze as SnO₂crystals with a concentration of 7–14 wt%. Concerning the decorations, it is established that the green colour is due to the presence of copper, while manganese is responsible for the brown colour. These pigments, which represent the typical colours of ‘archaic majolica’, are spread through the glaze homogeneously, apart from one case in which there is clear evidence of manganese oxide crystals.     

A guide for the distinction of species, sex and body side in bones of sheep and goat

Morphological criteria are described that were found to be the most successful for distinguishing between skeletal fragments of adult sheep (Ovis) and goats (Capra) in the Western European, early medieval sites of Haithabu and Oldenburg in Holstein. It is emphasized that a sufficiently large sample should be observed. In addition, methods are given for distinguishing sex in the pelvis, and body side in distal metacarpus and metatarsus ends.     

Last meals inferred from the possible gut contents of a mummy: A case study from Astana Cemetery,Xinjiang, China*

The gut contents of ancient humans have been proven to be the most direct evidence for palaeodietary study. In the Xinjiang region of north-west China, large numbers of mummies are well preserved owing to the extremely dry environment to be found there. Fourier-transform infrared spectroscopy (FTIR) combined with multi-archaeobotanical methods, including macrofossil examination, starch grain analysis, phytolith analysis and bran fragments analysis, were applied to investigate the possible gut contents (c.1300 bp by ¹⁴C dating) of a person unearthed at tomb 75TAM601 in Astana Cemetery, which were the public graveyards of the ancient Gaochang people (residents of Turpan, dating from about the third to the ninth centuries ce ), in Turpan, Xinjiang. The result of the FTIR analysis showed that the matrix of the possible gut contents consisted of protein and starch and was characterized as undigested food residue. The white mineral fragments of this sample were from the decomposition products of the skeleton. The microfossil analysis demonstrated that Setaria italica, Panicum miliaceum and Triticum aestivum were the main cereal resources for the last meals eaten by the deceased. Moreover, direct macrofossil evidence also advocates for the importance of the three aforementioned cereal crops and fruits of Cucumis melo and Vitis vinifera in the person's diet.     

Chemical composition and colouring agents of Roman mosaic and millefiori glass, studied by electron microprobe analysis and Raman microspectroscopy

About 100 fragments of Roman mosaic and millefiori glass were stylistically attributed to a Hellenistic type, a Ptolemaic and Romano-Egyptian period type and an early imperial period type. Twelve representative fragments were studied by electron microprobe analysis and Raman microspectroscopy. Eleven of them display a Na-pronounced recipe with low K, Mg and P contents, typical for the Roman period. Minor differences in composition are unsystematic, not reflecting the stylistic classification. Ionic colouring agents are Mn³⁺ for violet, Cu²⁺ for light blue, Co²⁺ for deep blue and Fe³⁺ for brown translucent colours. Calcium antimonates, lead antimonate and cuprite are the colourants responsible for white, yellow and red colours, respectively, and additionally serve as opacifiers. Mixing of ionic colouring agents and opacifying colourants led to a more differentiated palette of colours. Pb was used as yellow colouring agent, as a flux material and as a stabiliser for the colourant crystals. The remaining fragment consisting of a K-pronounced but still Na-bearing glass matrix was most likely produced during the Middle Ages or later.     

ROMAN AND MEDIEVAL GLASS FROM THE ITALIAN AREA: BULK CHARACTERIZATION AND RELATIONSHIPS WITH PRODUCTION TECHNOLOGIES*

Compositional investigations were performed on 81 Roman and medieval glass fragments (first to 14th centuries ad ) from four Italian archaeological sites. The samples were soda–lime–silica in composition, with natron as flux for the Roman and early medieval glass samples, and with plant ash as flux for the late medieval ones. The varying colours are due to the differing FeO, Fe ₂ O ₃ , MnO and Sb ₂ O ₃ contents. Hierarchical cluster analysis identified six compositional groups related to age, which were compared with those found in the literature. In this way, technological continuity from the Roman to the early medieval period and the appearance of plant ash technology in the ninth century, 200 years in advance of the period previously believed, are demonstrated.     

Reims,Bibliothèque Carnegie, 806: a little‐known manuscript of Benedict of Aniane's Concordia regularum

Benedict of Aniane is usually portrayed as the major instigator of a series of monastic reforms undertaken by Louis the Pious in the early years of his reign, which attempted to impose the Rule of Benedict of Nursia as the sole monastic standard across Francia. Based on information provided by Ardo, Benedict of Aniane's biographer, the Concordia regularum has been seen as Benedict's main instrument in his attempt to convince or compel others to accept the Rule as a superior norm. The Concordia itself is a sort of commentary on the Rule, where almost the whole of St Benedict's Rule is explained by texts drawn from other monastic rules. However, a number of fragments from a copy of the Concordia, apparently written a decade or more before the accession of Louis, contests Ardo's chronology, and challenges our traditional understanding of both Benedict of Aniane's role in monastic reform and of the Aachen reform councils. An edition of these fragments is included in an Appendix.     

TECHNOLOGICAL STUDY OF PTOLEMAIC – EARLY ROMAN FAIENCE FROM MEMPHIS,EGYPT*

Fourteen fragments of faience vessels from the Ptolemaic/Roman period found at the Egyptian site of Memphis, near Cairo, were analysed by SEM. The fragments included high‐relief polychrome vessels, which are first produced in numbers in this period. Analysis allowed the composition and microstructure of the vessels to be assessed and conclusions drawn as to the raw materials of manufacture. Combining this information with archaeological evidence from excavation of the kilns and associated finds, it was possible to reconstruct the production technology of the vessels.     

CHEMICAL ANALYSIS OF COPPER ALLOY TRADE METAL FROM A POST-CONTACT HURON SITE IN ONTARIO,CANADA

Fifty-three copper-based metal fragments, recovered from the Robitaille site in southcentral Ontario, were analysed by neutron activation to establish their chemical make-up and to sort them by their trace elemental chemistries. Three different European copper samples, one brassy copper and 48 brass samples with five different chemistries were found. As few as eight trading actions may account for all of the recovered European metal fragments.     

Shah Isma‘il’s Poetry in the Silsilat al-Nasab-i Safawiyya

This article examines the four poems attributed to Shah Isma‘il Safavi that are included in the seventeenth-century genealogy of the Safavid dynasty, the Silsilat al-Nasab-i Safawiyya. The article includes translations and commentary on the four poems, offering insight into the religiosity and concerns both of Shah Isma‘il and the Silsilat's author, Husayn ibn Shaykh Abdal-i Zahidi.     

THE RED INK OF THE DEAD SEA SCROLLS

The red ink on four fragments of the Dead Sea Scrolls was analysed by X-ray fluorescence and X-ray diffraction. The red pigment was identified as mercury sulfide (HgS), cinnabar. The significant archaeological and historical aspects of this finding are discussed.     

Plant macroremains from the Roman harbour of Pisa (Italy)

Abstract

Results relating to the identification of macroscopic plant remains (leaves, fruits, seeds) discovered during the archaeological excavation of the Roman harbour of Pisa, in Tuscany, Italy are reported. The plant samples include the cultivated species Prunus spp., Corylus, Olea, Vicia, Juglans and the nemoral wild species Salix spp., Quercus spp., Fagus, Ulmus, Alnus. The remains of cultivated plants — fragments of fruits and seeds — were perhaps part of the boats' cargo or stores for the crew's meals. In the case of the wild taxa, the simultaneous presence of fruit and leaves, suggests that the remains recovered came from the forest vegetation bordering the area of excavation and the adjacent higher grounds, thus delineating a new vegetation landscape for the ager pisanus.