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1.
    
Samples of mortars and stone of Portal de ses Taules from the Renaissance city walls of Eivissa (16th century) were characterized using thermal analysis— thermogravimetry and derivative thermogravimetry (DTG)—x-ray diffractometry, and scanning electron microscopy. The granulometric fraction of particle size <63 μm was selected as representative of the binder, while the fraction 0.5–1 mm was taken as representative of the aggregate in order to characterize mortar samples. The results show that local materials were used. Lime was the main component of most of the samples tested. Thermal analysis revealed the hydraulic nature of the lime mortars. High amounts of sodium chloride were found in the samples analysed.  相似文献   

2.
Scanning electron microscopy has been applied to experimentally cut bone samples and an ethnographical example of trephination on a human skull in order to produce diagnostic criteria for the identification of mollusc shells as cutting implements used in trephination. Shell scrapes are identifiable by parallel striations in the direction of cut, crossed at 90° by chatter marks caused by uneven movement of the fragile shell-edge across the bone surface.  相似文献   

3.
    
The original fineness of coins is very important information that can help us to understand the commercial situation in a wide historical context. This paper deals with a comparison of analytical methods suitable for the evaluation of the actual and original fineness of coins based on a detailed case study of a medieval coin sample. Both non‐destructive (i.e., scanning electron microscopy/energy‐dispersive X‐ray spectroscopy, X‐ray fluorescence, atomic force microscopy and hydrostatic weighing) and destructive (i.e., inductively coupled plasma – mass spectrometry and the Volhard titration method) techniques were used. The original fineness can be also deduced from knowledge of the internal structure of the coin (limited miscibility of copper and silver). A new analytical method based on a combination of a micrograph of the metallographic cross‐section with consequent image analysis was developed for determination of the original fineness. The proposed approach is relatively simple and provides reliable values. Sample heterogeneity and its impact on the determination of fineness are also discussed.  相似文献   

4.
The skeletal remains of a child aged 13–15 years, recovered from Wharram Percy, England, and dating from AD 960–1700, were examined using gross observation, radiography and scanning electron microscopy. Lesions suggestive of renal osteodystrophy were found. Palaeopathological recognition of renal disease has hitherto relied upon the identification of soft tissue lesions or the presence of urinary calculi. This appears to be the first palaeopathological identification of renal insufficiency on the basis of skeletal changes alone. Copyright © 2007 John Wiley & Sons, Ltd.  相似文献   

5.
By means of scanning electron microscopy, four out of a series of twelve inhumations from the Hellenistic Period were examined for traces of the decay process. The changes represented the result of erosion and biological decomposition of human bones on a small island in the northern part of the Persian Gulf over a period of ca. 2200 years. Special emphasis was given to bone preservation and blood cell survival, and to bone changes due to physicochemical erosion and fungus, bacterium, insect and plant-root activity. Related soil and climatic conditions were taken into consideration. The observations should be evaluated to understand the unusual state of preservation of the bones and to avoid possible misinterpretation of pseudo-pathological bone changes as ante-mortem pathology.  相似文献   

6.
Ultrastructural features of deep, intermediate and superficial enamel were quantitatively assessed for the mandibular first permanent molars of 10 specimens each of the domestic sheep (Ovis aries) and goat (Capra hircus). The means of a number of variables differed interspecifically at high levels of statistical significance, especially with regard to the enamel of intermediate depth. A canonical discriminant function analysis employing nine variables at all three enamel depths resulted in the correct taxonomic assignment of 95% of the specimens comprising the present sample. These results, coupled with the simple preparative and analytical methods presented here, may enable archaeozoologists to utilize enamel ultrastructure in order to discriminate between fragmentary dental remains of these caprine species.  相似文献   

7.
医用螺钉在手术中得到大量的使用的同时,因其质量事故频发,患者对质量鉴定要求越来越迫切。我们借助光学显微分析、电子显微分析技术、X射线荧光能谱分析等微量物证分析技术。从微观角度对螺钉断裂原因进行了质量鉴定.  相似文献   

8.
    
In this article, we present the results of application of petrographic and neutron activation analyses to a group of pottery fragments dating to the 12th century BCE deriving from ancient Eleon (Boeotia, Greece) as a means of investigating regional and interregional networks in which the site participated. Production centres in Boeotia and central Euboea provided, as could be expected, the majority of sampled pottery across various shapes. A number of more distant areas, however, such as eastern Attica, the Cyclades, Macedonia, and western Crete, are also documented in the present study, suggesting their products were available to local consumers at ancient Eleon. These results are discussed with reference to consumer preferences and exchange networks operating at that time. Finally, some of the identified petrographic and chemical groups can be securely identified at the macroscopic level, allowing us to arrive at conclusions pertinent to a substantial part of the entire pottery assemblage.  相似文献   

9.
    
This paper presents the results of analyses carried out on the paintings on the rock‐hewn walls of the Forty Martyrs church at ?ahinefendi in Cappadocia (a UNESCO World Heritage Site), a central region of Turkey, performed during conservation work from 2007 to 2012. The micro‐samples were investigated by spectroscopic, micro‐stratigraphic and scanning electron microscopy analysis in order to study the painting technique, the materials and the degradation products. The micro‐stratigraphic analysis showed a white, sometimes pinkish, plaster. Micro‐Raman analysis, performed on cross‐sections of the mortars, enabled the detection of calcite, gypsum, anhydrite and calcium oxalate. Scanning electron microscopy and energy‐dispersive spectroscopy revealed a similar composition among all investigated phases, aside from minor differences such as the presence of diatoms in the second and third phases and of biotite, lime lumps and plants fragments in the fourth one. Apart from traditional pigments of medieval wall paintings, micro‐Raman analysis revealed the presence of lead‐based compounds and jarosite.  相似文献   

10.
This paper presents the results of the scanning electron microscopy of a series of experimental tools designed to investigate the role of abrasive agents and humidity in microwear polish formation. The tools—35 end scrapers—were divided into four groups and used to work dry hide. It was found that both humidity and abrasive agents are two basic variables in the development of the microwear polish.  相似文献   

11.
The prevailing archaeological consensus on Paleoindian origins and colonization of the Americas has been shaken by recent wide acknowledgment of pre-Clovis occupation at Monte Verde, Chile, and by claims that ostensibly non-Mongoloid skeletal remains might represent a precursor population. Recent mitochondrial DNA studies have been interpreted by some as indicating an earlier and more complex peopling of the continent. This paper reviews the current archaeological and biological evidence, in America and northern Asia, for the origins of Native Americans, assesses models of the colonization process in the light of new data and a revised chronology, and suggests avenues for future research.  相似文献   

12.
    
Roman plasters sampled from different houses at the archaeological site of Herculaneum, Italy, (2010–12) were studied by means of petrography, thermal analysis and X‐ray fluorescence. Herculaneum plasters are composed by preparatory layers (arriccio) with a thickness of several centimetres and are based on a calcitic binder and volcanic scoriae as aggregates, covered by a thin final layer characterized by a low granulometry. Most of the sampled plasters can be placed into two groups based on the aggregate composition and classified as marmorino or intonachino. However, a similar aggregate composition did not induce superimposable thermal behaviour, thus suggesting that the samples underwent different ageing/weathering processes, with a consequent change of the ratio among the components.  相似文献   

13.
    
ABSTRACT

The microstructures of building materials from the archaeological complex of Huaca de la Luna on the northern coast of Peru is assessed for the first time by a multiscale approach. The multiscale microstructural characterization used laboratory techniques including optical microscopy, scanning electron microscopy, X-ray microtomography, and both gas and powder pycnometry. Optical microscopy revealed the presence of organic matter and shell fragments and X-ray microtomography showed differences in the sizes and connectivity of pores. The BET (N2 gas adsorption) specific surface areas showed greater presence of clayey matrix in the mortars. No significant differences among mortars and brick fragments mineralogy were detected by X-ray diffraction, so the larger amount of fine binding matrix in the mortars suggests that they were produced blending raw material with different grain sizes. The aim of this study is to provide data that can be used for a better understanding of the Moche culture, its construction techniques, and to support conservation strategies of the archaeological heritage.  相似文献   

14.
    
ABSTRACT

This paper aims to evaluate mineralogical, elemental, and thermal differences among original Roman joint mortars and those used in twentieth-century restoration campaigns taken from different areas at the Herculaneum archaeological site. The purpose is to improve the compatibility of restoration mortars. Roman and modern mortars were studied with petrography, thermal analysis and x-ray fluorescence investigations. The results indicate significant differences between the Roman and modern mortars which could facilitate the degradation process. Roman mortars, in particular, were composed of a coarser aggregate which was present in a lower ratio with binder in comparison with modern mortars.  相似文献   

15.
    
ABSTRACT

Since a radiocarbon chronology of the Dalton culture in the Southeast was first proposed, several new sites have been dated. I propose a new chronology based on radiocarbon dates from sites in the Dalton Heartland and its eastern periphery using Bayesian statistical models in OxCal and an analysis of the associated diagnostic projectile points. The analyses indicate that the Dalton culture probably evolved from the Clovis or Gainey phenomena about 12,680?cal?BP (ca. 10,700?BP) and lasted at least until ca. 10,400?cal?BP (ca. 9,200?BP), if not several centuries later. I propose early and late Dalton phases that follow changes in how Dalton points were made and resharpened. It appears that the people living to the east of the Heartland followed a different trajectory of projectile point evolution. There, notched points appear about 11,500?cal?BP, while in the Heartland, true notched points do not appear in large numbers until the Graham Cave point over 2,000 years later. The chronologies demonstrate that early, coeval, region-wide cultural changes may not have been the norm. They also raise interesting questions about how people in the Heartland and its eastern periphery interacted.  相似文献   

16.
ABSTRACT

Weeden Island mortuary ceremonialism united distinct cultures across the Late Woodland social landscape. The Weeden Island pottery series is central to recognizing regional ceremonial parity, with prestige (elite) and sacred (cult) wares showing strong similarities among distant sites. Finely made vessels and their ostensibly shamanistic themes led archaeologists to consider the liturgical and political roles of ritual specialists, whose tasks might have included vessel manufacture in centralized locations. This research evaluates the prospect of craft specialization and centralized production of sacred and prestige wares through comparisons of the provenance of vessels from three Florida localities: Palmetto Mound (8LV2), the mounds at Melton (8AL5, 8AL7), and McKeithen (8CO17). Results of Neutron Activation Analysis and petrographic analysis show that the majority of the sampled vessels were made far from the mounds in which they were deposited, from a variety of locations but especially within the area between Kolomoki and the Tallahassee Hills. We argue that production was not centralized but may have been specialized to the extent that an integrated ritual network was necessary to coordinate rules of manufacture and use that were evidently observed by all participants.  相似文献   

17.
A recently described case of putative early tertiary syphilis in a young adult male from 6th century Anglo‐Saxon England exhibits a distinctive endocranial pathology. A case–control study using both clinical and archaeological materials was performed to investigate a possible association of the pathology with syphilis. Scanning electron microscopy and microcomputed tomography were used to image the syphilitic case and normal cranial material. Although the pathology does seem to have an association with syphilis (OR = 13.14), the sample size is small, and the authors caution against overinterpretation of the results. The study confirms observations by other authors suggesting the lesion has some association with a range of pathological conditions. Any association with syphilis seems to be restricted to the early tertiary stages and is possibly absent in the later stages of the disease. The morphological differences present in the samples observed by scanning electron microscopy and microcomputed tomography illustrate the abnormal nature of the vascularity within the syphilitic cranium. The widespread presence of similar lesions within other tubular bones leads the authors to propose hypothesis that unresolved angiogenesis is the underlying mechanism behind the skeletal changes in tertiary syphilis. This angiogenic model accounts for several diverse characteristics in the progression of skeletal disease resulting from infection by spirochetes of the Treponema pallidum family. Copyright © 2012 John Wiley & Sons, Ltd.  相似文献   

18.
Aspects of Roman pottery production at the workshops of Kontich, Tienen, Rumst, Grobbendonk and Clavier-Vervoz in the Civitas Tungrorum of central Belgium are explored. A total of 150 wasters from five sites were studied macroscopically, as well as via a combination of thin-section petrography, geochemistry and scanning electron microscopy, in order to gain insights into ceramic technology and aspects of the organization of production. Particular emphasis was given to the individual technological sequences and shared strategies of raw material selection, paste preparation and firing employed at the five adjacent sites. The integration of petrographic and geochemical data permitted the establishment of compositional reference groups for the Roman kiln sites of Civitas Tungrorum, which can be used to track their products within the surrounding landscape.  相似文献   

19.
    
M. Wojcieszak  L. Wadley 《Archaeometry》2018,60(5):1062-1076
Micro‐residue analysis of stone tools is generally performed with optical light microscopy and the visual observations are then compared with experimental, replicated pieces. This paper complements such archaeological research by providing physico‐chemical evidence. Raman spectroscopy and scanning electron microscopy have been used to confirm the presence of hematite on red‐stained medial and proximal parts of 71 000‐year‐old Still Bay bifacial tools from Sibudu Cave. Our results confirm the conclusion from optical light microscopy that the tools were hafted with an ochre‐loaded adhesive. However, we point to some instances when hematite residues are incidental or may be inclusions in the rock used to make the stone tools.  相似文献   

20.
A methodology is described for the analysis of Holocene charcoals excavated from a rock shelter in the Lubombo Mountains of northeast Swaziland. Scanning electron microscopy was used to compare these with modern reference woods. Of the ancient material 96·6% could be identified, in some cases at specific level. It is in such a subtropical area, where the woody flora is so rich, that assemblages of local taxa can be used in palaeoclimatic reconstructions. The changing taxa indicated by the charcoal fragments from the rock shelter clearly reflect minor shifts in Holocene climate, from moist to dry and back to moist in recent times. This is of relevance to the fluctuations in Stone Age populations in southern Africa. The wider use of such evidence to complement other palaeoenvironmental and archaeological data is advocated.  相似文献   

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