NON‐DESTRUCTIVE ANALYTIC METHOD USING XRF FOR DETERMINATION OF PROVENANCE OF ARCHAEOLOGICAL OBSIDIANS FROM THE MEDITERRANEAN AREA: A COMPARISON WITH TRADITIONAL XRF METHODS*

A non‐destructive analytical method using wavelength‐dispersive X‐ray fluorescence (WDXRF) that allows the establishment of the provenance of archaeological obsidians was developed and a comparison with the classical XRF method on powders is discussed. Representative obsidian samples of all the geological outcrops of archaeological interest of the Mediterranean area (Lipari, Pantelleria, Sardinia, Palmarola and the Greek islands of Melos and Gyali), were analysed with the normal procedures used in rock analysis by XRF (crushing, powdering and pelletizing). The non‐destructive XRF analysis was instead conducted on splinters taken from the original geological pieces, with the shape deliberately worked to be similar to the refuse usually found at archaeological sites. Since the analysis was conducted on the raw geological fragment, intensity ratios of the suitably selected chemical elements were used, instead of their absolute concentrations, to avoid surface effects due to the irregular shape. The comparison between concentration ratios (obtained by traditional XRF methods) and the intensity ratios of the selected trace elements (obtained from the non‐destructive methodology) show that the different domains of the chemical composition, corresponding to the geological obsidians of the source areas, are perfectly equivalent. In the same way, together with the geological splinters, complete archaeological obsidians, from Neolithic sites, may be analysed and their provenance may be determined. The proposed non‐destructive method uses the XRF method. Due to its sensitivity, low cost and high speed, it is surely an extremely valid instrument for the attribution of the provenance of the archaeological obsidian from Neolithic sites.     

Mapping Submerged Landscapes Using Multibeam Bathymetric Data: a case study from the north coast of Ireland

This paper outlines work currently being undertaken to reconstruct submerged archaeological landscapes off the north coast of Ireland. This research uses the recently‐completed Joint Irish Bathymetric Survey (JIBS), which has provided full‐coverage high‐resolution multibeam bathymetric data for the sea‐bed off the north coast. This data has been examined for evidence of past sea‐level change and been used to produce palaeo‐geographic reconstructions of the past landscape, which in turn have facilitated the identification of ten areas of high archaeological potential. The results presented here will form the basis of a future programme of archaeological survey and prospection. © 2010 The Authors     

Between rocks and a hard place: prehistoric funerary practices at Wādī Ḍebayʿān,northern Qatar

Archaeological survey by the Qatar National Historic Environment Record Project (QNHER) in 2009, led to the discovery of a Neolithic flint scatter, a settlement and an ancient, raised shoreline associated with higher, mid‐Holocene sea levels at Wādī ?ebay?ān, north‐western Qatar (Al‐Naimi et al. 2010, 2011; Cuttler, Tetlow & Al‐Naimi 2011). The QNHER project is a collaboration between Qatar Museums and the University of Birmingham, which over the past five years has developed a national geospatial database for the recording of archaeological sites and historic monuments in Qatar. A significant aspect of the project involved archaeological survey and excavation in advance of major construction projects. Between 2012 and 2014 excavations at Wādī ?ebay?ān revealed a burial of a typology previously unknown in Qatar, the unmarked graves (Cuttler, Al‐Naimi & Tetlow 2013).     

A Multi‐disciplinary Approach to the Archaeological Investigation of a Bedrock‐Dominated Shallow‐Marine Landscape: an example from the Bay of Firth,Orkney, UK

Investigation of shallow‐marine environments for submerged prehistoric archaeology can be hampered in many localities by extensive bedrock exposure and thus limited preservation potential. Using the concept of ‘seamless archaeology’ where land‐based archaeology is integrated across the intertidal zone through to the offshore, a multi‐disciplinary approach is essential. This approach taken in the Bay of Firth, Orkney uses geophysics, historical archive and ethno‐archaeology, coastal geomorphology, palaeo‐environmental analyses and sea‐level science, and allows a clearer understanding of the landscape in which prehistoric settlers lived. While acknowledging the limitations of the preserved environment, we are successful in identifying areas of archaeological potential on the sea‐bed for both upstanding structural elements as well as sediment preservation that contains evidence for human occupation. This has wider implications beyond Orkney's World Heritage sites to provide a blueprint for similar studies elsewhere in the coastal zone. © 2012 The Authors     

The Palaeo‐Environmental Contexts of Three Possible Phoenician Anchorages in Portugal

The 2002 Joint Expedition of the Institute of Nautical Archaeology and the Centro Nacional de Arqueologia Náutica e Subaquática examined Phoenician maritime involvement in Portugal, combining archaeological, geological and geophysical surveys of former coastal sites—Santa Olaia, Abul and Castro Marim—where previous excavations have uncovered Phoenician remains. Significant geomorphic evolution of bay‐head delta and estuarine settings masks the fact that Phoenician sites were situated at the head of marine embayments or on estuary margins, had easy access to the sea, and immediate access to at least one natural anchorage. All sites exhibited topographical criteria familiar from Phoenician trading‐stations and merchant outposts in the Mediterranean. © 2009 The Authors     

BAYESIAN ANALYSIS OF PLEISTOCENE CHRONOMETRIC METHODS*

Bayesian analysis of radiocarbon dates on Holocene archaeological sites has become well established. Application to Pleistocene sites dated by multiple techniques would be advantageous. This paper develops the necessary mathematical apparatus in the form of likelihoods for luminescence dating, and uranium‐series dating, and considers the possibility for amino‐acid racemization dating. Application of the new methods is illustrated using the stratigraphic sequences of dates from the sites of Saint‐Césaire and La Chaise‐de‐Vouthon. For application to amino‐acid racemization dating, fuller publication of data is found to be required.     

Estimating age by tooth wear of prehistoric human remains in Brazilian archaeological sites

The occlusal surfaces of 298 permanent maxillary and mandibular molar teeth of prehistoric shellfish‐gatherer subjects from the Piaçaguera and Tenorio sites (4930 to 1875 BP), near the central‐northern coastline of São Paulo, Brazil, were examined for classification of macro‐wear stages. Molar tooth wear is an indication of masticatory activity and can be used in the estimation of age at death. The examination of visual and schematic aspects of occlusal macro‐wear used a visual chart proposed by Brothwell, which includes the three superior and inferior, left and right, permanent molars. Three examiners performed the macroscopic observations twice under the same conditions. The resulting age estimates were compared with previous information of age estimated by skeletal examination. A reduced intra‐ and inter‐observer variation was observed; all re‐examinations indicated discrepancies of less than two years for the upper and lower limit of the age range estimates. The procedure was also considered consistent with the skeletal method used for age estimation of human remains excavated in Brazilian archaeological shell mounds, with a discrepancy of less than 8.22 years between the upper and lower limits of estimates by both methods. Age classification by the occlusal molar wear may be a useful tool for the classification of archaeological findings, mainly when only fragmentary skeletal remains are excavated. The current results indicate that the application of the Brothwell chart for Brazilian archaeological series presented satisfactory results of consistency, and its expanded use may represent a relevant adjunct for research. Copyright © 2006 John Wiley & Sons, Ltd.     

High‐Resolution 3D Marine Seismic Investigation of Hedeby Harbour,Germany

Offshore 3D‐seismic acquisition has been a standard for high‐precision structural imaging in the oil and gas industry for many years. Recently this technique has been adapted by only a few teams to the resolution required for archaeological marine investigation. In contrast to sonar techniques, the 3D‐seismic method produces images below the sea‐floor. We investigate the harbour of the Viking age proto‐town of Hedeby in Northern Germany with the SEAMAP‐3D system. SEAMAP‐3D allows for rapid acquisition and employs an automated data processing sequence. We observe a wealth of archaeologically relevant detail and compare our results with previous work.     

Turquoise Mine and Artefact Correlation for Some Bronze Age Archaeological Sites in Hubei Province,China

In China, there are places that are rich in gem‐quality turquoise resources, including north‐west Hubei Province and the nearby Baihe County in Shaanxi Province, and many ancient mining sites, although the mining history remains a mystery. Based on the compositional data from reference samples of known deposits, a comparison of the major and trace element contents of archaeological turquoise may help with determination of artefact provenance. This paper discusses new evidence of provenance‐tracking of turquoise in this area, obtained from geochemical analyses using REE and other trace elements of 22 turquoises and their surrounding rock samples from six ancient mines and three archaeological sites. The results indicate that the three archaeological turquoises from the tomb of the Middle Spring and Autumn Period (580–560 bc ) and the Warring States Period (476–221 bc ) in Hubei Province were made of raw material from north‐west Hubei Province and the nearby Baihe County in Shaanxi Province. [Correction added on 29 October 2014, after first online publication: In the preceding sentence, the correct dates for the Middle Spring and Autumn Period, and the Warring States Period have been added]     

Image‐Based Modelling from Unmanned Aerial Vehicle (UAV) Photogrammetry: An Effective,Low‐Cost Tool for Archaeological Applications

The recording and 3D modelling of complex archaeological sites is usually associated with high capital and logistical costs, because the data acquisition must be performed by specialists using expensive surveying sensors (i.e., terrestrial laser scanners, robotic total stations and/or ground‐penetrating radar). This paper presents a novel, low‐cost, user‐friendly photogrammetric tool for generating high‐resolution and scaled 3D models of complex sites. The results obtained with unmanned aerial vehicle (UAV) photogrammetry of an archaeological site indicate that this approach is semi‐automatic, inexpensive and effective, and that it guarantees quality.     

Provenance analysis of Olivella biplicata shell beads from the California and Oregon Coast by stable isotope fingerprinting

While Olivella beads are a common component of archaeological sites in California, and were widely traded in prehistory, no method has been developed to trace individual beads to a point of origin. This study examines the potential of stable carbon and oxygen isotopes to source Olivella beads from the Pacific coast. The study shows that 1) the oxygen isotopic composition of modern Olivella biplicata shells faithfully varies with ambient sea surface temperature and local upwelling, lending themselves to sourcing studies; 2) oxygen isotope ratios in modern shells can be used to identify shells that grow north versus south of Point Conception, California; and 3) shell carbon isotope ratios may further subdivide these two regions into more spatially restricted source zones. Analyses on a small sample of 10 beads found at various archaeological sites within the interior of California suggest that all were made in southern California.     

IDENTIFICATION OF POST‐DEPOSITIONAL CHEMICAL ALTERATION OF CERAMICS FROM THE NORTH COAST OF PAPUA NEW GUINEA (SANDUAN PROVINCE) BY TIME‐OF‐FLIGHT–LASER ABLATION–INDUCTIVELY COUPLED PLASMA–MASS SPECTROMETRY (TOF–LA–ICP–MS)*

The measured chemical composition of archaeological ceramics can result from a variety of geological, cultural and taphonomic factors. In the present study, we evaluate the likelihood that elevated barium concentrations in ceramics from the archaeological site of Wom/Aiser, located on the northern coast of Papua New Guinea, result from post‐depositional enrichment. Using time‐of‐flight–laser ablation–inductively coupled plasma–mass spectrometry, we mapped chemical compositional profiles across cut sections of ceramic sherds from four archaeological sites, all previously chemically characterized. We identify the formation of pronounced concentration gradients in samples from Wom/Aiser relative to sherds with low barium concentrations, consistent with post‐burial uptake.     

CHARACTERIZATION OF ARCHAEOLOGICAL AND IN SITU SCOTTISH WINDOW GLASS

Scottish window glass from both archaeological sites and historic buildings was examined using portable X‐ray fluorescence (pXRF) and scanning electron microscopy – energy‐dispersive X‐ray micro‐analysis (SEM–EDX). The elemental composition of the glass provides information regarding the materials used and, subsequently, an approximate range of dates of manufacture. pXRF is shown to be more vulnerable than SEM–EDX to the effects of surface corrosion and matrix effects in archaeological samples. The study showed that the production of window glass in Scotland from the 17th century onwards appears to closely parallel that in England. It also demonstrated the potential of pXRF for in situ studies of window glass in historic buildings. pXRF was used to assess two Scottish buildings; one in state care and one in private ownership. The building in state care, the Abbot's House at Arbroath Abbey, showed a uniform glass type, suggesting that the building was re‐glazed completely at some point during the late 19th or early 20th century. The building in private ownership, Traquair House, had a range of glass types and ages, demonstrating a different maintenance and repair regime. This type of data can be useful in understanding historic buildings in the future, particularly if re‐glazing is being considered.     

Using Sector‐Scan Sonar for the Survey and Management of Submerged Archaeological Sites

This article reports the results of using a sector‐scan sonar to record diverse submerged archaeological sites in shallow and deep water. The Kongsberg MS1000 sector‐scan sonar was developed for commercial applications, typically underwater inspections of bridges, dams, ports and harbours. The ability of the device to rapidly generate high‐quality, geometrically accurate scans of submerged features, coupled with its ease of use and deployment make it a potentially important, yet largely overlooked, tool for survey and management of underwater archaeological sites. As one of several technologies available, the paper examines its advantages and limitations, and considers, through case studies, under which conditions it is most effectively deployed.     

Technological Choices in Hand‐Made Indigenous Pottery from Western Mallorca (Balearic Islands,Spain) (C.1200–75 bc): An Archaeometric Approach

This paper addresses the technological choices observed in Mallorca (Spain) for the production of hand‐made pottery during the Late Bronze and Iron Age. We have conducted a diachronic analysis of the ceramic assemblages recovered from two archaeological sites placed in the same territory by means of X‐ray fluorescence and optical microscopy by thin‐section analysis. The archaeometric characterization of the hand‐made vessels allows us to establish several compositional groups related to the use of different raw materials and certain paste recipes associated with the archaeological sites and periods considered. Thus, this study evidences different productive strategies in each site and across time in the same geographical area.     

Archaeological survey,paleogeography, and the search for Late Pleistocene Paleocoastal peoples of Santa Rosa Island,California

Abstract

The northern Pacific Coast is an important area for understanding human colonization of the Americas, but Late Pleistocene coastal sites are rare and interglacial sea level rise has inundated the continental shelf and the primary areas where Paleocoastal archaeological sites are likely to occur. Here we outline a terrestrial archaeological survey project designed to identify Paleocoastal sites on Santa Rosa Island, California. Using reconstructions of ancient shorelines and paleogeography, we predicted that sites might be found where lithic resources, freshwater springs, caves or rockshelters, and strategic vistas drew Paleocoastal peoples into the island interior. We identified nine new Paleocoastal sites, including four radiocarbon dated to >11,000 cal b.p. that are among the oldest sites on North America’s Pacific coast. Our targeted survey demonstrates an important technique for investigating island and coastal settings where sea level rise remains a significant challenge for locating early sites.     

Documenting Archaeological Mortuary Features using High Dynamic Range (HDR) Imaging

This technical note presents a refined technique for photo‐documenting archaeological mortuary features using High Dynamic Range (HDR) imaging. Mortuary features in archaeological context can be complex and delicate given the wide variability in grave constructions and preservation of human skeletal remains. It is therefore critical to obtain the greatest detail possible when photo‐documenting these features. HDR techniques represent more contrast in photographs and provide greater detail across the DR of illumination within mortuary features—where complex arrangements of human remains can obscure or darken other elements or associated funerary objects, making them difficult to identify in traditional photographs. HDR can be employed with most standard digital single lens reflex cameras used for archaeological field projects, is easy to learn and employ (as described here), can be processed and produced with commonly used photo editing programs, and is ideal for use in unpredictable conditions that are often encountered with archaeological mortuary features and in field conditions. Copyright © 2013 John Wiley & Sons, Ltd.     

THE DISCOVERY OF ANOMALOUSLY HIGH SILVER ABUNDANCES IN POTTERY FROM EARLY ROMAN EXCAVATION CONTEXTS IN JERUSALEM*

This is the first study on the differential distribution and concentrations of silver in ceramics recovered from archaeological excavations. The chemical compositions of 1174 pottery vessels from 38 Roman‐period sites in Israel have been determined. Unusually high and variable abundances of silver were discovered in pottery samples of all vessel types and chemical compositions from four distinct archaeological contexts dating to late first century bce to 70 ce Jerusalem. The large majority of the Jerusalem vessels could be distinguished by their silver abundances from all analysed pottery pieces recovered at rural sites outside Jerusalem, even when the pottery types and chemical compositions, except for silver, of pottery found within and outside Jerusalem were indistinguishable. The evidence is suggestive of a human origin for the high and variable silver abundances, and dispersion of the silver by aqueous transport. The differential silver concentrations found in excavated pottery from Jerusalem and other urban and rural sites suggest that attention to the distribution of silver in pottery from excavated contexts may be helpful for evaluating the nature and function of archaeological remains and patterns of urban contamination.     

Reconstructing age distribution,season of capture and growth rate of fish from archaeological sites based on otoliths and vertebrae

The growth increments of otoliths and vertebrae of plaice (Pleuronectes platessa) derived from a 15th century single depositional event at Raversijde (Belgium) are analysed with the aim of reconstructing (a) the age distribution of the population, (b) the season of capture, and (c) the growth rate. Otoliths and vertebrae give slightly different age distributions but it is possible to arrive at similar seasonality estimations in both structures when information from the literature and our own data from monthly captures of plaice from the North Sea are taken into account. These modern data show that the timing of annulus formation in otoliths and vertebrae is more or less similar. Back‐calculations on vertebrae and otoliths yield similar growth curves. The age distribution, the edge condition of both vertebrae and otoliths, and the growth rate obtained on the material from Raversijde all show that the plaice from the studied assemblage were captured during spring in the southern part of the North Sea. Vertebrae are commonly preserved in archaeological sites whereas otoliths rarely survive. Although they are more difficult to read than otoliths, vertebrae of plaice can be used for growth increment analyses, and the growth rates obtained from vertebrae from archaeological sites can, therefore, be compared in the future to growth data from modern otoliths studied in sea fisheries research. Archaeozoological material predating industrialized fishing since the 19th century can hence serve as a reference in the study of the compensatory response of commercially important species to heavy exploitation. Copyright © 1999 John Wiley & Sons, Ltd.