DATING OF THE HOMINID (HOMO NEANDERTHALENSIS) REMAINS ACCUMULATION FROM EL SIDRÓN CAVE (PILOÑA,ASTURIAS, NORTH SPAIN): AN EXAMPLE OF A MULTI‐METHODOLOGICAL APPROACH TO THE DATING OF UPPER PLEISTOCENE SITES

The age of Neanderthal remains and associated sediments from El Sidrón cave has been obtained through different dating methods (¹⁴CAMS, U/TH, OSL, ESR and AAR) and samples (charcoal debris, bone, tooth dentine, stalagmitic flowstone, carbonate‐rich sediments, sedimentary quartz grains, tooth enamel and land snail shells). Detrital Th contamination rendered Th/U dating analyses of flowstone unreliable. Recent ¹⁴C contamination produced spurious age‐values from charcoal samples as well as from inadequately pretreated tooth samples. Most consistent ¹⁴C dates are grouped into two series: one between 35 and 40 ka and the other between 48 and 49 ka. Most ESR and AAR samples yielded concordant ages, ranging between 39 and 45 ka; OSL dating results permitted adequate bracketing of the sedimentary layer that contained the human remains. Our results emphasize the value of multi‐dating approaches for the establishment of reliable chronologies of human remains.     

The Holocene fluvial history of the Tremithos river (south central Cyprus) and its linkage to archaeological records

This study aims to reconstruct the Holocene fluvial history of the Tremithos river, south central Cyprus and examine linkages to regional and local archaeological records. Three stratigraphic profiles (Sp1, Sp2 and Sp3) located in the lower valley have been investigated using sedimentology and magnetic parameters. The ¹⁴C dating of 10 samples reveals mid-Holocene ages for Sp1 and Sp2, while the upper most part of Sp3 can be attributed to the early to mid-Holocene. Two main phases of vertical accretion have been recognised: the first, recorded in the lower most part of Sp3, could not be dated but might relate to the late Glacial period. It is not associated with any archaeological artefacts. The second, recorded in all profiles, dating from ca. 5000 to ca. cal 2800 BC, spans the Late Neolithic Sotira (cal 4800/4000 BC) and Late Chalcolithic (cal 2900–2500 BC) cultures. The sediments of Sp1 and Sp2 are up to 8–10 m thick and mainly composed of fine material. However, an intercalated phase of coarse sediment has been identified at the beginning of the third millennium BC, indicating a sudden change in river dynamics, potentially associated with the 5.2 ka rapid climate change regional event. Typical mid-Chalcolithic (ca. cal 3300–3050 BC) ceramics found in a palaeosol in Sp2 indicate for the first time human occupation of the Tremithos river terraces. Two other palaeosols have also been recognised in Sp3 and radiocarbon dated to ca. cal 5600–4100 BC and ca. cal 2900–2600 BC, respectively. These results make it possible to propose a palaeogeographic reconstruction of the Holocene evolution in the Tremithos valley and to make a preliminary assessment of the relative roles of tectonics, climate and anthropogenic forcing.     

Growth of the Lichen Buellia albula and its Potential for Lichenometric Dating in South‐eastern Australia

Lichenometric dating is a cheap, relatively rapid means of dating rock surfaces, which has generally been overlooked in Australia. While lichenometry finds its greatest application in arctic and alpine geomorphological studies, there has been limited application to archaeological studies. This project set out to test the technique in south‐eastern Australia, and assess its usefulness for dating post‐settlement artefacts. The diameters of Buellia albula lichens growing on well‐dated memorials in the Bendigo cemetery were measured, and the relationship between age and lichen diameter established. The results indicate that B. albula can be used to determine the age of exposed cement surfaces from the 1890s to the present. The positive results suggest the technique should be investigated in other applications and environments in Australia, particularly where alternative dating techniques cannot be used.     

Human Palaeoecological Interactions and Owl Roosting at Tron Bon Lei,Alor Island,Eastern Indonesia

We report on tetrapod (Reptilia, Amphibia, Mammalia, Aves) vertebrates recovered during excavations at Tron Bon Lei rockshelter on the south coast of Alor Island, eastern Indonesia. These include both archaeological specimens recovered from a 1 m² test pit dating from ～21 kya cal BP to the late Holocene, and a modern eastern barn owl deposit recovered nearby. To discern between the depositional processes that accumulated the small numbers of micro- and macrovertebrate remains from the archaeological deposits, the taphonomic signature of the natural assemblage was quantified and compared to the archaeological record. The taphonomic data indicates that the tetrapod archaeofaunal remains are a combination of barn owl predation of microfauna and human predation of larger fauna. This approach provides new information on human-tetrapod interactions on Alor in Wallacea during the late Quaternary, including an apparent increase in cave site use and hunting intensity during the Pleistocene-Holocene transition, sea turtle butchery and probable transport, and extinctions of previously unknown giant to large rat species.     

A Late Holocene Tsunami at Basta Voe,Yell, Shetland Isles

A distinctive sand layer enclosed within Holocene peat is described from Basta Voe, Isle of Yell, Shetland Isles. The sand layer, that can be traced considerable distances inland and up to a maximum altitude of c. + 9 m OD, is here interpreted as having been deposited by a former tsunami. AMS dating appears to indicate that the tsunami occurred between 1300 – 1570 cal years BP. At present, the tsunami has no known source mechanism although the most likely mechanism is thought to have been an offshore slump or slide. The available information would presently seem to indicate that this tsunami was restricted to the eastern coastline of Shetland. The relatively young age of this inferred tsunami is of considerable importance to planners and engineers concerned with estimating coastal flood frequency and magnitude.     

Trilobites from the Middle Ordovician Stairway Sandstone,Amadeus Basin,central Australia

Abstract

During the Middle Ordovician (Darriwilian) sandstones and siltstones were deposited in the epicontinental Larapintine Sea, which covered large parts of central Australia. The Darriwilian Stairway Sandstone has, for the first time, been sampled stratigraphically for macrofossils to track marine benthic biodiversity in this clastic-dominated shallow-water palaeoenvironment situated along the margin of northeastern Gondwana. The faunas from the Stairway Sandstone are generally of low diversity and dominated by bivalves but include several animal groups, with trilobites representing 25% of the entire shelly fauna. Thirteen trilobite taxa are described from the Stairway Sandstone; the fauna displays a high degree of endemism. One new species, Basilicus (Parabasilicus) brumbyensis sp. nov. is described.     

OPTICAL DATING OF SINGLE AND MULTIPLE GRAINS OF QUARTZ FROM JINMIUM ROCK SHELTER,NORTHERN AUSTRALIA: PART I,EXPERIMENTAL DESIGN AND STATISTICAL MODELS*

Jinmium rock shelter is famous for the claims made by Fullagar et al. (1996) for the early human colonization and ancient rock art of northern Australia. These claims were based on thermo-luminescence ages obtained for the artefact-bearing quartz sediments that form the floor deposit at the site. In this paper, we outline the background to the optical dating programme at Jinmium, and describe the experimental design and statistical methods used to obtain optical ages from single grains of quartz sand. The results, interpretations, and implications of this dating programme are reported in a companion paper (Roberts et al. 7999, this volume).     

PINE RESINS AND POTTERY SEALING: ANALYSIS OF ABSORBED AND VISIBLE POTTERY RESIDUES FROM CENTRAL NEW YORK STATE*

Analysis was performed on absorbed and visible residues from 21 New York State prehistoric pottery sherds dating from 2905 ± 35 bp (Intcal04) (1256–998 cal bc ) to 425 ± 40 bp (Intcal04) (1417–1626 cal ad ). The use of pine resin was detected in 10 of 12 absorbed residue samples and 11 of 17 sherds subjected to visible residue analysis. It seems likely that the pots were resin‐sealed to make them more impermeable, constituting the first chemical evidence of extensive resin‐sealing in North America. A comparison of the results of absorbed and visible residues from eight of the sherds indicates that the two kinds of residue provide complementary evidence of vessel use.     

Red abalone collecting and marine water temperature during the Middle Holocene occupation of Santa Cruz Island,California

Oxygen isotope values derived from prehistoric mussel (Mytilus californianus) shell calcite are used to determine whether sea-surface temperatures in the vicinity of the Punta Arena site (CA-SCRI-109) on Santa Cruz Island, California, were cooler than present between 6300 and 5300 cal BP. This site and others in the western sector of the island dating to this period are distinctive because of the presence of large red abalone (Haliotis rufescens) shells, a species that historically has been subtidal around Santa Cruz and the other northern Channel Islands. Comparison of temperature values derived from archaeological shells with those from modern mussel shells, along with water temperatures derived from satellites, indicates that waters were cooler during the 6300 to 5300 cal BP period. These results are consistent with a previous study and support the interpretation that collection of red abalone during the 6300–5300 cal BP period was partly the result of cooler water temperatures that made this large mollusk more available to foragers in the intertidal or shallow subtidal zone.     

Modern and early-middle Holocene shells of the freshwater mollusc Unio, from Çatalhöyük in the Konya Basin, Turkey: preliminary palaeoclimatic implications from molluscan isotope data

Carbon and oxygen isotope ratios in the shells of the freshwater Unio mollusc yield information on the isotopic composition of the water in which the shell was formed, which in turn relates to climatic conditions prevailing during the bivalves’ life span. Here we analysed shells from one modern Unio, from a modern lake shore in Anatolia, and 4 subfossil Unio shells from Çatalhöyük (dated between 7200 BC and 5000 BC, Neolithic and Chalcolithic periods). Sequential carbon and oxygen isotope analysis along the surface of the shells provides information on seasonal or shorter-term variability of lake waters during the lifetime of the organisms. δ¹⁸O values of the modern shell are consistent with it being collected from a dammed portion of the Seyhan River that does not undergo intensive summer evaporation. This is in contrast to many of the surface water bodies in Anatolia which suffer extensive evaporation in the arid summers. δ¹⁸O values of the subfossil shells from the Çatalhöyük middens indicate that the bivalves came from lakes which evaporated extensively during the summer months but were replenished by high winter rainfall, suggesting that the subfossil shells lived in relatively small lakes or ponds. Stable isotope analysis along the growth of freshwater bivalves is one of the few methods for investigating seasonal water fluctuations in the past. These results may alter current interpretations on the environment of Çatalhöyük during the Neolithic, although more work is needed to confirm these initial findings.     

Geoarchaeological tsunami deposits at Palaikastro (Crete) and the Late Minoan IA eruption of Santorini

The explosive eruption at Santorini in the Aegean Sea during the second millennium BCE was the largest Holocene volcanic upheaval in the Eastern Mediterranean region. The eruption was disastrous for the Minoan settlements at Santorini, but the effect on human society in the neighbouring islands and regions is still clouded in uncertainty. Tsunami generation was suggested, but comparatively little evidence was found. The lack of firm tsunami traces is particularly puzzling in Crete with its coastal settlements of the Late Minoan IA period, during which the Santorini eruption occurred. Here, we report the discovery of extensive geoarchaeological tsunami deposits at Palaikastro in north-eastern Crete. These deposits are characterized by a mixture of geological materials, including volcanic Santorini ash, and archaeological settlement debris. Various tsunami signatures were identified: (1) erosional contact with the underlying strata, (2) volcanic ash intraclasts in the lower part of the deposit, (3) reworked building stone material in the lower part of the deposit, (4) individual marine shells, (5) marine micro-fauna, (6) imbrication of rounded beach pebbles, settlement debris, ceramic sherds and even bones, (7) multi-modal chaotic composition. Late Minoan human settlement activities at Palaikastro provided architectural and stratigraphic frameworks in space and time that recorded and preserved tsunami evidence as geoarchaeological deposits. Such stratigraphic resolution and preservation may not occur in the natural landscape. Volcanic ash transported by wind from Santorini south-east to Crete preceded the tsunami. Geological, archaeological and radiocarbon dating criteria all converge, indicating that the tsunami deposits are coeval with the Minoan Santorini eruption. Field evidence suggests that tsunami waves at Palaikastro were at least 9 m high. Inverse tsunami modeling was attempted, based on these newly discovered tsunamigenic deposits. The initial wave in the generation region at Santorini that best fits the stratigraphic data is a wave with +35 to −15 m initial amplitude and a crest length of about 15 km.     

Holocene Elevated Sea Levels on the North Coast of Vietnam

We present evidence of elevated Holocene sea levels on the north coast of Vietnam, comprising radiocarbon dating of raised coastal geomorphological and palaeobiological features at localities on the margins of the Bac Bo (Red River) Plain. This evidence indicates that by ca. 5500 cal yr B.P. mid‐tide lay approximately 5.4 m above national datum, that is 3.25 m above present local mid‐tide. By c. 3500 cal yr B.P., sea level was lowering and, by ca. 2000 cal yr B.P., mid‐tide lay at or above 1.5 m above present local mid‐tide. It is not yet possible to infer patterns of sea‐level fluctuation other than an overall lowering of elevation, although the separation of the raised and modern erosion notches does suggest two dominant mid to late Holocene periods of erosion — probably periods of sea‐level still‐stand or relatively slow sea‐level change. The intervening period of relatively rapid sea‐level change and associated reduced erosion probably dates to after ca. 2000 cal yr B.P..     

ON THE AGE AND CONTENT OF JAR‐35—A SEALED AND INTACT STORAGE JAR FOUND ON THE SOUTHERN PLATEAU OF QUMRAN*

An intact and sealed storage jar known as Jar‐35 was found in 2004, south of the Qumran settlement. A previous study identified tartrate in the deposit of the jar, indicating the possible past presence of wine ( Buti et al. 2006 ). However, we cannot confirm this finding. Using liquid and gas chromatography with mass spectrometric detection, no trace of tartaric acid or salts thereof could be detected in our samples. We show that the major component of the deposit is gypsum. No other organic compounds were identified with the methods that we have applied. Both radiocarbon dating of charcoal in the deposit and thermoluminescence dating of the ceramic jar show that it dates to the main period of habitation at Qumran (c. 100 bc to ad 70).     

Two radiocarbon dates for freshwater shells from hierakonpolis: Archaeological and geological interpretations

Shells of two species of freshwater bivalve (Unio willcocksi Bullen Newton and Etheria elliptica Lamarck) from the predynastic Gerzean (Nagada II) Decorated Tomb at Hierakonpolis, Egypt have given dates of 5000±90 bp for the tomb, and 12,900±120 bp for an episode of Nile terrace accumulation (correlated here with the Sahaba-Darau aggradation event). The archaeological and geological significance of these results is discussed, together with an outline of problems associated with radiocarbon dating of shell. Comparisons are made with the few other radiocarbon dates available for the Predynastic period in Egypt and possible reasons for the presence of shells in the tomb are considered.     

Microchemical and crystallographic analysis of human bones from Nasca,Peru. A possible method of direct dating of archaeological skeletal material

This paper provides two archaeometric equations obtained by crystal–chemical parameters for dating human bone samples from the archaeological site of Nasca, Peru. Based on radiocarbon dating, the burials span from 500 BC to AD 1000. Crystal–chemical modifications in bone hydroxylapatite over time were compared with a twentieth century skeleton from Italy. Chemical analysis was carried out by means of electron microprobe along a profile from the periosteal to the endosteal border of the midshaft of four human femurs. The results indicate that the Ca/P ratio is linearly correlated with time according to the equation t=7880.68Ca/P−12805.90 (r=0.97; r²=0.95). Bone apatite X-ray powder diffraction analysis showed a systematic increase in the (002) reflection intensity with time, according to the equation t=250.49h/a−1961.86 (r=0.98; r²=0.97). The two independent archaeometric equations permit good accuracy in dating osteoarchaeological remains from the south coast area of Peru. © 1998 John Wiley & Sons, Ltd.     

DIET AND ENVIRONMENT IN SOUTH‐EASTERN IBERIA DURING THE BRONZE AGE,BASED ON ISOTOPE ANALYSIS OF HUMAN REMAINS

A large sample of human bones from a series of archaeological sites in the south‐eastern Iberian Peninsula was selected for δ¹³C and δ¹⁵N stable isotope analysis. Except for some contrast samples, the remains date from the first half of the second millennium cal BC and are ascribed to the Argar Culture, which developed during the Bronze Age in south‐eastern Iberia. Most authors have considered that this region reached a high degree of social hierarchical organization at this time, as demonstrated by the funerary record, both with regard to the grave goods and to the evidence of physical effort and diseases on the human remains. Results of the isotope analysis revealed the existence of differences among the settlements studied, as well as differences over time within every settlement and among the various individuals tested. Some variances can be assigned to social classes/status and others are linked to chronological factors. In particular, changes in δ¹³C can be explained by the increasing aridity of the first half of the second millennium cal BC, although other causes can be put forward too.     

Palaeogeographical reconstructions of Lake Maliq (Korça Basin,Albania) between 14,000 BP and 2000 BP

Since the early 1990s, excavations of a protohistoric lakeside settlement in the Korça basin carried out by a French–Albanian archaeological team have induced geomorphological and palynological studies about the sedimentary records of Lake Maliq. These studies allow us to distinguish a series of centennial-scale high and low lake level events between 4200 and 4000 cal BP (2899–2637 BC/2843–2416 BC) and 2600 cal BP (822–671 BC), probably due to large-scale climate changes (in the Mediterranean basin). In addition, the sediment sequence also gives evidence of a millennial-scale trend of lake level rise. It appears to be an interplay between lake level rises and falls against tectonic subsidence of the basin allowing accommodation space for sediment deposition.The variations of the lake's level and the lake's surface area influenced the development and the abandonment of the nearby lakeside settlements (like the tell of Sovjan). In order to prepare an archaeological survey around the now dried up lake, we made a 3D model of the Holocene deposit from the lake including these lake level results, geomorphological mapping, excavation data, numerous core logs, AMS ¹⁴C dating and SRTM DEM data. The GIS model allowed us to propose four palaeogeographical reconstructions of the extension of Lake Maliq: around 14,000 BP, during the Mesolithic (around 9000 BP – 8781–8542 BC), the Early/Middle Bronze Age transition (around 3800 BP – 2310–2042 BC) and the Iron Age (2600 BP – 822–671 BC). A map of the thickness of the sediments above potential archaeological layers is also proposed.     

The Evolution of a Holocene Estuarine Barrier on the Coromandel Coast,New Zealand

Whitianga Harbour on the Coromandel Peninsula, North Island, New Zealand is fronted by a broad sandy barrier composed of linear beach ridges. The barrier developed through a process of rollover as sea level rose in the early Holocene with shelly sandy sediment washed inland over estuarine muds. These overwash deposits are present to 3 m below sea level in the back barrier area. Once sea level stabilised and barrier rollover had ceased the barrier continued to prograde in a series of beach ridges. The back barrier area is characterised by estuarine muds, overlain by splay and overwash deposits that are reworked by fluvial and tidal channels. The initial flooding of the estuary occurred at around 7350–7225 years cal BP, reaching modern levels by 6894–6729 years cal BP at the earliest. Infill was rapid as evidenced by estuarine species (crustaceans and bivalves) preserved in life position. From ～6000 years BP to present, the estuary is characterised by tidal and fluvial reworking, suggesting that modern sediment inputs are bypassing the estuary.     

Variability in the marine radiocarbon reservoir effect in Muscat (Sultanate of Oman) during the 4th millennium BC: reflection of taphonomy or environment?

Radiocarbon (¹⁴C) dating of archaeological coastal sites in arid areas is challenging because of the relative rarity of datable terrestrial artefacts. Marine artefacts provide an abundant source of carbon, which is technically easy to date but radiocarbon dates need to be corrected for local variations from the global average marine ¹⁴C reservoir age (ΔR). In archaeological sites, this is usually done by the comparison of the ¹⁴C age measured between coeval pairs of terrestrial and marine samples that have no inbuilt age. Here, we present the results of a study that aims to determine the local ¹⁴C marine reservoir effect (MRE) along the Eastern coast of the Arabic Peninsula during the 4th millennium BC, a period of important cultural, demographic and social changes in this region. Previous estimates of the MRE based on associated shells and charcoal vary by about 400 ¹⁴C yr and this is a serious limitation to the establishment of a precise chronology in the area based on marine material. In order to maximize the chances to obtain contemporaneous terrestrial–marine pairs for a new assessment of the MRE in this region we dated charcoal, shells, fish and turtle bones as well as human bones found in three recently and carefully excavated graves from Ra’s al-Hamra RH5. A large variability was found between charcoals (up to 240 ¹⁴C yr) and marine specimens (up to 785 ¹⁴C yr) present in the same grave. This variability was attributed to inbuilt ages, diagenesis and possibly environmental factors although taphonomic processes cannot be excluded. We discarded the oldest charcoals and used the ¹⁴C ages obtained on human apatite as a cut-off value to remove the marine outliers. Two out of the three graves provided terrestrial and marine assemblages which did not differ statistically and were used to calculate an average MRE of 645 ± 40 ¹⁴C yr (ΔR = 255 ± 55 ¹⁴C yr). This value is consistent with previous estimates based on the ¹⁴C dating of marine sediments off Pakistan and suggests stability of the MRE in the Arabian Sea since the 4^th millennium BC.     

Geological setting, nature of ore fluids and sulphur isotope geochemistry of the Fu Ning Carlin-type gold deposits, Yunnan Province, China

Carlin‐type gold deposits in southern China are present in Palaeozoic to Mesozoic siliciclastic and carbonate rocks. The border region of Yunnan, Guizhou and Guangxi Provinces contains gold deposits on the south‐western margin of the Pre‐Cambrian South China Craton in south‐eastern Yunnan Province. The Fu Ning gold deposits host epigenetic, micron‐sized disseminated gold in: (i) Middle Devonian (D₁p) black carbonaceous mudstone at the Kuzhubao gold deposit and (ii) fault breccia zones at the contact between Triassic gabbro (β ) and the Devonian mudstone (D₁p) at the Bashishan gold deposit. The deposits are associated with zones of intense deformation with enhanced permeability and porosity that focused hydrothermal fluid flow, especially where low‐angle N‐S striking thrust faults are cut by NW striking strike‐slip and/or NE striking normal faults. Major sulphide ore minerals in the Fu Ning gold deposits are pyrite, arsenopyrite, arsenic‐rich pyrite, stibnite and minor iron‐poor sphalerite. Gangue minerals are quartz, sericite, calcite, ankerite and chlorite. Hypogene ore grades range from 1 to 7 g t^?1 Au and up to 18 g t^?1 Au at the Kuzhubao gold deposit and are generally less than 3 g t^?1 Au at the Bashishan gold deposit. Sub‐microscopic gold mineralization is associated with finely disseminated arsenic‐rich pyrite in the Stage III mineral assemblage. Two types of primary fluid inclusions have been recorded: Type I liquid–vapour inclusions with moderate‐to‐high liquid/vapour ratios, and Type II inclusions containing moderate liquid/vapour ratios with CO₂ as determined from laser Raman analysis. Temperature of homogenization (T_h) data collected from these primary fluid inclusions in gold‐ore Stage III quartz ranged from 180 to 275°C at the Kuzhubao gold deposit and 210 to 330°C at the Bashishan gold deposit. Salinity results indicate that there were possibly two fluids present during gold deposition, including: (i) an early fluid with 0.8–6.5 wt.% NaCl equivalent, similar to salinity in shear‐zone‐hosted gold deposits with metamorphic derived fluids; and (ii) a late fluid with 11.8–13.4 wt.% NaCl equivalent, indicating possible derivation from connate waters and/or brine sources. CO₂ and trace CH₄ were only detected by laser Raman spectrometry in gold‐ore‐stage primary fluid inclusions. Results of sulphur isotope studies showed that δ³⁴S values for pyrite and arsenopyrite associated with gold‐ore mineralization during Stage III at the Kuzhubao and Bashishan gold deposits are isotopically similar and moderately heavy with a range from +9 to +15 per mil, and also fall into the range of δ³⁴S values reported for Carlin‐type gold deposits. Sulphur isotopes suggest that the Fu Ning gold deposits were formed from connate waters and/or basinal brines. Fluid geochemistry data from the Fu Ning gold deposits suggest a Carlin‐type genetic model, involving fluid mixing between: (i) deep CO₂‐rich metamorphic fluids, (ii) moderately saline, reduced connate waters and/or basinal brines; and (iii) evolved meteoric waters.