THE SUBTRACTION TECHNIQUE OF THERMOLUMINESCENT DATING

Combination of the routine approaches of thermoluminescence dating, the fine-grain and inclusion methods, allows an age to be determined that is independent of knowledge of the environmental dose-rate. This socalled subtraction technique is exampled by several terracottas of museum origin and some pottery collected from archaeological contexts without associated burial media. Age determination is estimated to have an accuracy of around ± 12%, in favourable conditions.     

THE ASSESSMENT OF ERROR LIMITS IN THERMOLUMINESCENT DATING

This paper discusses known sources of error, both random and systematic; suggests quantitative limits; and proposes a consistent method for compounding them to yield an overall error in age, both for individual sherds and for the weighted average of a number of sherds from the same context. It is proposed that two error limits should be quoted for the date of a context: first, the standard error of the mean value as calculated from the experimentally observed root-mean-square deviation of the individual samples, and secondly, the expected overall error from the sources discussed in the paper. The former can be considered as a lower limit and relevant when comparing contexts on the same or similar sites whereas the latter is more realistic when comparing TL dates with radiocarbon or archaeologic chronology.     

THERMOLUMINESCENT DATING: ASSESSMENT OF ALPHA PARTICLE CONTRIBUTION

A new system for specifying alpha source strength, in terms of track length per unit volume of sample, is proposed. It is based on the experimental observation that the TL induced per unit length of track is essentially independent of alpha particle energy. The new system avoids the need to make assumptions about sampple stopping power and it is shown to be consonant with the old system as long as up-to-date evaluation of alpha ranges is used. A revised table of dose-rate data is given.     

THERMOLUMINESCENT DATING OF COLOMBIAN POTTERY IN THE YOTOCO STYLE

Two contexts from the Colombian sites, Yotoco Ferry and Moralba, had been linked by archaeological similarities in pottery style, and dated by association with ware from other sites at circaa.d. 1000. However, radiocarbon dating of those contexts set Moralba at circa 800 b.c. , some 2000 yr older than Yotoco Ferry. Thermoluminescent dating of pottery from Yotoco Ferry dated it at circaa.d. 900, and pottery from Moralba was dated at circaa.d. 870. In addition a metal-smelting pottery crucible, thought to be prehispanic, was studied by thermoluminescence and dated, on the contrary, at less than 120 yr old.     

THERMOLUMINESCENT DATING OF BAKED CLAY BALLS OF THE POVERTY POINT CULTURE

Seven sites in Mississippi, Louisiana and Arkansas have been dated. For six sites (Terral Lewis, Poverty Point, Jaketown, Teoc Creek, Shoe Bayou, and Claiborne) the results are not inconsistent with contemporaneity; excluding Claiborne the average date is 1000 b.c. , with an error limit in absolute terms of ± 200 years. The seventh site (Loggy Bayou), in which sherds and balls were found in association, gave a date some fifteen hundred years more recent.     

THERMOLUMINESCENT AUTHENTICITY STUDY AND DATING OF RENAISSANCE TERRACOTTAS

A comparative study is made of the thermoluminescence (TL) of terracottas of the Renaissance era and some known limitations of such ware dating to the middle of the last century. The data shows that conclusions on authenticity of an unknown work can be reliably obtained using this scientific method. Also examples are presented of accurate dating of genuine terracottas despite a lack of knowledge about the environmental circumstances of each piece's archaeological past.     

RADIOCARBON DATING BY THERMOLUMINESCENT DOSIMETRY

Work is presented that tests the possibility of performing radiocarbon dating measurements by using the thermoluminescence induced in sensitive phosphors, using existing thermoluminescence equipment. It is concluded that, for such a technique to be viable, a more specifically designed, and more elaborate, system will be necessary. Some comparative results on certain TLD phosphors are also given.     

THE EFFECT OF HF ACID ETCHING ON THE MORPHOLOGY OF QUARTZ INCLUSIONS FOR THERMOLUMINESCENCE DATING

The assumption of isotropic etching in hydrofluoric acid of quartz grains prepared for thermoluminescence dating has been tested by optical and scanning electron microscopy. We have found that the rate of etch is very irregular over the surface of many grains and that some grains are attacked much more severely than others. The uncertainty introduced into TL dating by this effect is discussed.     

THERMOLUMINESCENT DATING OF EGYPTIAN PREDYNASTIC POTTERY FROM HEMAMIEH AND QURNA-TARIF

Eight sherds from Hemamieh and two from Qurna-Tarif, both Predynastic settlement sites in the Nile valley, have been dated by the thermoluminescence method (quartz inclusion technique). The results put the Badarian phase at Hemamieh in the sixth and fifth millenium b.c. , and the Gerzean phase in the first half of the fourth millenium b.c. The dates for the village of Qurna-Tarif fall around 4000 b.c.     

THERMOLUMINESCENCE DATING: RADIOACTIVITY IN QUARTZ

Alpha activities measured for four quartz extracts indicate that, in some samples, the alpha dose-rate to the quartz due to radioactivity within the quartz can be significant. Uranium mapping of the quartz by neutroninduced fission tracks shows that the radioactivity is not homogeneously distributed.     

THERMOLUMINESCENT DATING OF FIRED ROCK-CRYSTAL FROM BELLAN BANDI PALASSA,CEYLON

Fired rock-crystal was found within the matrix of a Balangodese (pre-Vedda) burial in a Mesolithic midden in Ceylon; thermoluminescent measurements indicated a date of about 7000 years before present.     

THERMOLUMINESCENCE DATING OF BURNT FLINT AND QUARTZ: COMPARATIVE RESULTS

Thermoluminescence dates obtained from burnt flints and quartz recovered from the same sites are compared. For the Upper Perigordian level at la Vigne Brun (Loire, France), four quartz specimens and three flints yielded average ages of 27 400 ± 2300 and 26 900 ± 2200 years respectively, which are 15% greater than the radiocarbon age obtained for the same site (Evin 1982). For the neolithic site of la Vallée aux Fleurs (Loir et Cher, France), the respective averages of three flints and three ceramic sherds were 6830 ± 560 and 6570 ± 520 years.