THE FIRST ARCHAEOMETRIC CHARACTERIZATION OF ROMAN MILLSTONES FOUND IN THE AQUILEIA ARCHAEOLOGICAL SITE (UDINE,ITALY)*

An archaeometric study of all the Roman millstones preserved today in the National Archaeological Museum of Aquileia, the ancient capital of the X Regio Augustea –‘Venetia et Histria’ located on the Friuli plain (northeastern Italy), has been recently envisaged to define their geological–geographical provenance. We present here the results of the first step of the research, which is aimed at characterizing all of the definitely allochthonous lithologies. In order to carry out petrography on thin‐section and geochemical analyses, 10 small samples were picked out directly from Pompeian‐style millstones (catilli and/or metae) and rotary querns. Five different lithologies originating in various Italian regions were recognized: eight samples consist of pale‐ and dark‐grey lavas from the Venetian Volcanic Province, Vulsini Volcanic District (Latium), Etna Volcano and Pantelleria island (Sicily), whereas two samples were shown to be made of green garnet‐bearing schists (pietra ollare) from the Western Italian Alps. The presence of Alpine pietra ollare in northeastern Italy, used to produce pots and food containers, was established for numerous classical findings at Roman and Middle Age sites, but the analysed items represent the first evidence for the utilization of this kind of stone to produce mills during the Roman epoch.     

PROVENANCING AND ARCHAEOLOGY OF ROMAN MILLSTONES FROM SARDINIA (ITALY)

Summary. Sardinia was an important Roman settlement and trade centre between 238 BC–500 AD and is an ideal site for study of Roman trade. Study of Roman millstones in Sardinia shows that the commonest type is the Pompeian (hour-glass) mill (forty-eight stones studied), with smaller numbers of cylindrical hand querns (sixteen stones studied). Most of these millstones are composed of igneous rocks which include grey vesicular lavas of basic/intermediate composition and a distinctive reddish rhyolitic ignimbrite. There is historical and archaeological evidence for millstone manufacture at six localities in Sardinia. Visual and petrographic study and X-ray fluorescence analysis for major and trace elements of seventeen millstone samples, and fifty rock samples from potential source areas have been used to provenance the igneous rock millstones. The grey vesicular lava millstones have varied sources within the Tertiary-Recent volcanic rocks of Sardinia, while the millstones composed of rhyolitic ignimbrite are from a single source of Tertiary ignimbrite at Mulargia (central west Sardinia). A single hand mill from the north of Sardinia was imported probably from Agde in southern France, and is the only sample composed of non-local rock. Mulargia millstones were widely traded within the western Mediterranean and show a rapid decrease in frequency of occurrence with increasing distance from the source. Sardinia was therefore an important centre of Roman millstone production and a source of millstone trade during the period of Roman settlement.     

Roman Millstones from Orvieto (Italy): Petrographic and Geochemical Data for A New Archaeometric Contribution

The probable site of extraction and production of Pompeian‐style leucite‐bearing millstones, singled out by Peacock (1980, 1986) in the vicinity of Orvieto, and the outcropping of the ‘Leucitophyre’ lava have been systematically studied employing standard petrographic and geochemical methods (optical microscopy and ICP–AES/MS spectrometry). The combination of petrochemical data, previously very poor, allowed us definitively to exclude the possible ‘overlap’ of phonolitic and tephri‐phonolitic lavas from other Quaternary Volcanic Districts of Latium, and provides a helpful tool for future work on leucitite millstones. Consequently, the databank obtained has been used to attribute the origin of five Roman millstones discovered in three archaeological sites in central Italy (Latium and Marche). It has also been useful to verify the geological provenance of some Sicilian and French leucitite millstones analysed by previous workers. The results point to a provenance from the Orvieto area, with the exception of the millstones from Sicily, for which a different origin was hypothesized.     

Geochemical provenance analyses of Roman lava millstones north of the Alps: a study of their distribution and implications for the beginning of Roman lava quarrying in the Eifel region (Germany)

In Roman times, rotary querns and different types of millstones, driven either by horse-capstan or water power, were produced in the lava quarries of the quaternary volcanic Eifel region and exported to many parts of the Empire. The geographic distribution of Roman lava millstones from the Eifel region provides important information about trade patterns and, in cases of well dated millstones, also allows an estimate as to when the Roman lava quarrying in the Eifel region began. Sixty-two millstones from Germany, France and Austria were sampled and analyzed for major and trace elements by X-ray fluorescence. To determine their provenance, the millstone data was evaluated by a combination of geochemical discrimination and cluster and discriminant analyses using an extensive and detailed database of all Roman lava quarries in the Eifel region. An Eifel provenance could be confirmed for forty-four artefacts and, furthermore, determined down to the exact lava flow. The affiliation of the other artefacts to other possible regions where millstones of comparable lava were extracted was carried out on the basis of geochemical data from the literature. However, because of insufficient data, only assumptions about the regional provenance can be made. The origins of the other finds are assumed to be the Vogelsberg region, the Massif Central, Orvieto, and, possibly, the Pannonian Basin. A preliminary map of the distribution of Eifel millstones in Roman times based on these data is presented; the beginning of Roman lava quarrying can be constrained to 8–7 BC.     

Geoarchaeological insights from a Roman age incineration feature (ustrinum) at Enconsta de Sant'Ana (Lisbon,Portugal)

Ustrina are incineration funerary structures that are relatively common in Roman age cemeteries. Salvage excavations at Encosta de Sant'Ana (Lisbon, Portugal) in 2002 brought to light a part of the necropolis of the Roman town of Olisipo, including some ustrina. One of them, designated Burial 1 during fieldwork, is analyzed here from a geoarchaeological viewpoint to understand the formation processes of such an archaeological feature, namely its construction technique, use and function. The study of site context and subsurface pedofeatures, and the application of archaeological soil micromorphology, revealed that the ustrinum was constructed digging a hollow in bedrock and building a mud-brick ridge around it, with raw material taken from the local bedrock. The structure was used at various times and remodelled at least once, and its base was not always thoroughly cleaned – according to the custom called “pars pro toto” by Roman authors – and probably left open when not in use.     

Cartography of the archaeological surveys taken from an Ikonos stereo-pair: a case study of the territory of Hierapolis in Phrygia (Turkey)

The paper analyses methods and issues connected with the elaboration of Ikonos stereo high-resolution satellite images to create a large-scale cartography for archaeological research. This methodology has been used on an area of the ancient territory of Hierapolis in Phrygia (Turkey), where archaeological surveys, developed by the Italian Archaeological Mission, are in progress. In particular, the study area is situated between the modern villages of Yeniköy and Küçükdereköy, for which neither cartographies suitable for ground surveys nor aerophotogrammetrical covers were available. In this area there are a lot of archaeological remains; in particular, a large Hellenistic and Roman settlement and its necropolises, and also an old Turkish settlement, now destroyed. An Ikonos image was ortho-rectified to obtain a space-map of the entire area. It was used to extract vectorial thematic elements (modern topography, hydrology, archaeological remains and traces, etc.) for the production of maps for archaeological research in the tolerances of a 1:10,000 scale.     

Sourcing Volcanic Millstones from Greco-Roman Sites in Albania

Abstract

Provenience studies provide insights concerning trade in various goods, such as millstones. This is the first attempt to source millstones from Albania. Thirty-one vesicular volcanic millstones, predominately from the Greek and Roman periods, were obtained from two sites, 21 from Apollonia and ten from Butrint. The purpose of this study was to determine the provenience of these millstones using textural, mineralogical, and chemical data. The compositions of the samples were compared to those of vesicular volcanic sources in the central and eastern Mediterranean. Eight viable sources were initially identified based on major element chemistry; these were ultimately reduced to three based on trace element provenience studies. All of the Apollonia and five of the Butrint millstones have chemical signatures similar to those of Sicilian sources (the Iblean Fields and Mt. Etna). The remaining five Butrint millstones are chemically similar to stones from quarries other on the Cycladic island of Melos other than Rema (another Melian quarry), suggesting that Melian sources were exploited earlier than previously thought. The results of this preliminary study indicate there was no preference for a given source region at a particular time in the past. They also provide a baseline for future provenience studies of millstone trade patterns in Albania.     

THE USE OF TRACE ELEMENT ANALYSIS OF ENTRAPPED SLAG INCLUSIONS TO ESTABLISH ORE – BAR IRON LINKS: EXAMPLES FROM TWO GALLO‐ROMAN IRON‐MAKING SITES IN FRANCE (LES MARTYS,MONTAGNE NOIRE,AND LES FERRYS,LOIRET)*

Knowledge of the iron trade in ancient times rests on determining the source of the objects recovered during archaeological excavations. Unfortunately, attributing the origin is not always possible using archaeological tools alone. Trace element data of the ore and the archaeological material (reduction and reheating slags, entrapped slag inclusions from the bloom, bar iron and iron blades) from two Gallo‐Roman iron‐making centres, Les Martys (Montagne Noire) and Les Ferrys (Loiret), were determined using ICP–AES/MS and LA–ICP–MS. The results highlight a continuity of composition that makes it possible to establish a link between the initial ore and the semi‐finished iron products.     

Identification of psychoactive alkaloids in ancient Andean human hair by gas chromatography/mass spectrometry

Various ethnographic sources have demonstrated the symbolic and ritualistic importance of psychoactive plants in Native American societies. The social milieu of these mind- altering plants appears to be ancient. Archaeological evidence during the Tiwanaku empire expansion along the Atacama Desert of Chile, circa 500–1000 A.D., shows the presence of highly decorated snuffing tablets and tubes as grave goods. The preservation of mummified human bodies in the Azapa Valley, northern Chile, provided an opportunity to test the exact nature of the psychoactive plants used in this region. Using gas chromatography/mass spectrometry (GC–MS), here we show that ancient Andean populations from northern Chile consumed Banisteriopsis, a vine that contains harmine. This is the first direct archaeological evidence of hallucinogenic and medicinal ethnographic practices. Interestingly enough, this rainforest plant does not grow along the Atacama coast, thus our findings suggest extensive plant trade networks in antiquity as far as the Amazon.     

Publications

Abstract

This paper presents the results of a fabric study of the late Roman coarse wares (3rd century–6th century A.D.) from the Roman coastal town of Potentia (Porto Recanati) Marche, Italy). The petrographic analysis established the presence of several imported coarse ware classes, originating from the eastern Mediterranean to northern Africa. Of particular interest are the Adriatic common wares, which allow us to examine and define the extent, scale, and configuration of ancient trade within Adriatic Italy. While it is difficult to trace trade routes, items transported as a secondary commodity, like regional coarse wares, can help in reconstructing ancient economic interaction. The burnished coarse ware discussed here documents the ancient N-S trade routes from the Po region to the central Adriatic. Moreover, the identification of a northern Italian ware in central Adriatic Italy shows that this burnished coarse pottery had economic value and was part of a wider distribution network within the Adriatic.     

Archaeometric analysis of Late Roman amphorae from <Emphasis Type="Italic">Africa</Emphasis> in the ancient city of <Emphasis Type="Italic">Iluro</Emphasis> (Mataró, Catalonia,Spain)

In this paper, the results of the archaeometric study of an assemblage of Late Roman amphorae, found in several contexts from the ancient city of Iluro (Mataró, Catalonia, Spain) and with a presumable origin in Roman Africa, is presented. A total of 57 samples have been analysed, by means of optical microscopy (thin-section analysis), X-ray fluorescence and X-ray diffraction, in order to obtain an integrated petrographic, chemical and mineralogical characterisation and, from this data, to shed light on their provenance. The results indicate the presence of a large number of fabrics, most of them with a Tunisian provenance; a fabric probably from Algeria was also found, as well as a few chemical-petrographic loners that should be related to a provenance out of Africa. Concerning the Tunisian fabrics, the comparison with data from production centres allows for a more precise provenance hypothesis for many of them. These results are useful for the study of the trade networks of Iluro in Late Antiquity, since they provide new evidence on the diversity of transport amphorae that were arriving to this urban centre in Hispania Tarraconensis, showing a more complex reality than initially suggested by the archaeological evidence.     

Finding millet in the Roman world

Examining the evidence for millet in the Roman empire, during the period, circa 753 bc–610 ad, presents a number of challenges: a handful of scant mentions in the ancient surviving agrarian texts, only a few fortuitous preserved archaeological finds and limited archaeobotanical and isotopic evidence. Ancient agrarian texts note millet’s ecological preferences and multiple uses. Recent archaeobotanical and isotopic evidence has shown that millet was being used throughout the Roman period. The compiled data suggests that millet consumption was a more complex issue than the ancient sources alone would lead one to believe. Using the recent archaeobotanical study of Insula VI.I from the city of Pompeii, as a case study, the status and role of millet in the Roman world is examined and placed within its economic, cultural and social background across time and space in the Roman world.     

DNA analysis of archaeological sheep remains from China

Recent research has thrown considerable light on the history of the domestic sheep, but has not extended to ancient sheep specimens. In the present study, ancient DNA analysis was carried out on eight archaeological sheep remains recovered from Erlitou archaeological site in Henan Province (ca. 2100–1800 B.C.) to explore the genetic structure of ancient sheep and the phylogenetic relationship between ancient and modern sheep. We analyzed the control region sequences and coding regions of mitochondrial DNA from the remains by direct sequencing and restriction fragment length polymorphism analysis, respectively. Our results reveal that all ancient sheep belong to lineage A defined by modern sheep sequences. Phylogenetic analysis shows that neither argali (Ovis ammon) nor urial (Ovis vignei) mtDNA is closely related to Erlitou ancient sheep. In addition, our results suggest that ancient DNA analysis can serve as a powerful tool in tracing prehistoric population movement.     

Evidence of early medieval trade and migration between Wales and the Mediterranean Sea region

Imported Mediterranean pottery recovered from 5th–7th century settlement sites along the south Wales coast indicates that trade and contact between Wales and Byzantium continued following the collapse of the Roman Empire in the early-5th century. It is hypothesised that people as well as pottery continued to travel to Wales from Byzantium, some of whom subsequently settled amongst the local communities. Strontium and oxygen isotope analysis was undertaken on human remains (n = 33 individuals) from four early medieval cemeteries from south Wales. The study identified individuals who may not have been local to the British Isles, thus demonstrating that the isotopic analysis of human remains from Wales can further our understanding of migration to Britain during the early medieval period.     

Livestock Trade during the Early Roman Period: First Clues from the Trading Post of Empúries (Catalonia)

Written sources show that livestock were traded during the Roman period. However, there is scarce information available to characterise this trade because of its invisibility in the archaeological record. In our paper, we shed light on this issue by applying both osteometric and genetic analyses on cattle remains from the Roman trading post of Empúries (Catalonia) to determine how livestock contributed to Roman trade and, thus, to the economy of the Empire. Analysis of 26 cattle metacarpals from Empúries has allowed us to document the presence of different cattle morphotypes in this city during its Early Roman occupation. The morphological and genetic differences seen in Empúries cattle can be explained through trade of different cattle varieties, more appropriate for milk production and/or traction than the local stock. Once arrived at the port of Empúries, these imported cattle would have then been distributed to surrounding villas. Copyright © 2016 John Wiley & Sons, Ltd.     

Stable hydrogen isotopes of bone collagen in palaeodietary and palaeoenvironmental reconstruction

The stable hydrogen isotope ratios (δD) of bone collagen in archaeological human and animal samples demonstrate a trophic level effect, with increasing δD from herbivores to omnivores to humans, in steps of 10–30‰. In addition the archaeological sites studied (Yarnton, Eton Rowing Lake, Danebury Environs–Suddern Farm, and Windmill Hill in the UK, Balatonszárszó in Hungary, and Huari in Peru) demonstrate geographical variation in δD. The detection of manuring in prehistory by comparison of δ¹⁵N to δD values in humans and a local herbivore (cattle) is also considered. This work is the first to measure δD in a large number and range of archaeological samples, with several animal species and humans. It demonstrates unequivocally that δD is different between species in ancient material, increasing from herbivores to omnivores to carnivores.     

Plant remains and amphorae from the Roman harbour under Flacius Street in Pula (Istria,Croatia)

The aim of this archaeobotanical and archaeological research is to expand knowledge about Roman diet and plant cultivation in Istria and to compare it with similar localities on the Eastern Adriatic coast. We have also tried to find some new information about maritime trade routes in the Mediterranean area in ancient times. Out of 27 samples collected from an excavated Roman port in Flacius Street in Pula, in total, 9809 plant macrofossils were recovered, identified and analysed. The results of the analysis show that most of the plant remains belong to the group of fruit trees and nuts. The most abundant are the remains of Ficus carica, Pinus pinea, Vitis vinifera subsp. vinifera, Rubus fruticosus agg. and Olea europaea subsp. europaea. These are all species that are widespread in the Mediterranean area and have likely always been consumed by the local population. The number of ruderal and weed species found is relatively high (31) in comparison with other plant categories (fruit trees and nuts; fruit collected from the wild; cereals; condiments; oil crops; vegetables and tubers; plants of fresh water environments; elements of maquis), but as they came to the site accidentally and not by targeted human activity, there are far fewer macrofossils of such plants than those of cultivated species. There were a few elements of evergreen forest vegetation and plants of aquatic habitats at the site (2 + 1), which suggests the existence of this type of vegetation in the area of the site in Roman times. Archaeobotanical comparisons of the site in Flacius Street with similar coastal Roman sites—Verige Bay on Veli Brijuni (first-fifth century ad), the port of Zaton near Nin (first-third century ad) and Caska Bay on the island of Pag (first and second century ad)—reveal considerable similarities, confirming the uniformity in nutrition and plant growth in the wider coastal area. Together with the two Roman ships, during the archaeological excavations of the Roman harbour and its layers, we collected over 2000 different archaeological artefacts out of which a large number was almost perfectly preserved. Some of the mentioned artefacts include ceramic amphorae, ceramic table- and kitchenware, ceramic lamps, different usable objects made of glass, wooden use objects, parts of ship’s equipment and other wooden tools, architecture elements from the nearby port as well as residential structures and remains of stone monuments. Because of the large amount of artefacts found at the site, the analysis of the artefacts and data processing are still in progress. As a contribution for recognizing organic remains, we isolated the amphorae whose purpose was the storage and maritime transportation of different food products and ingredients.     

Cereal grinding technology in ancient Mesopotamia: evidence from dental microwear

Dental microwear features in a sample of 10 human teeth from Tell Ashara and Tell Masaikh, two archaeological sites in the Middle Euphrates valley, Syria, were compared for possible evidence of a shift in grinding technology in Mesopotamia—parallel to the well-documented introduction of large rotary querns and watermills in the Graeco-Roman world. Two chronological subsets (Bronze Age, n = 4 and Late Roman/Islamic period, n = 6) differred substantially and features related to a more abrasive diet (broad lines, pits and punctures visible on SE micrographs) were significantly less frequent in the later subsample which may indicate that the shift in cereal grinding technology occured in Mesopotamia before the Late Roman period.     

Recovery of DNA from archaeological insect remains: first results,problems and potential

We report the recovery of short fragments of PCR amplifiable ancient DNA from exoskeletal fragments of the grain weevil Sitophilus granarius (L.) extracted from Roman and medieval deposits in Northern England. If DNA preservation in archaeological insect remains is widespread then many applications in the spheres of evolutionary studies and archaeology can be conceived, some of which are outlined.     

Chemical characterisation of anthro-technosols from Bronze to Middle Age in Bologna (Italy)

The aim of this research was the understanding of a peculiarly expanded soil sequence in Bologna (i.e., Roman Bononia, Etruscan Felsina), one of the most important archaeological poles for Etruscan colonisation and settlement in northern Italy. The uppermost part of the chronological sequence dating from the Bronze Age up to medieval and modern times was analysed for the first time from geochemical and pedological viewpoints. The integration of archaeological, stratigraphical and pedological data supported by soil chemical analysis, a fundamental key for reconstructing a correct evolutionary sequence, made it possible to recognise seventeen buried Soil Units (ancient Technosols, Anthrosols and Cambisols) characterised by different kinds and degrees of intensity of anthropogenic influence. In some cases, the results show a relatively severe element concentration (Cu, Sn) mainly characterising the Iron Age (Etruscan and Villanovan) stratigraphic units, representing an ancient industrial pollution linked to local dispersal of melting activity dump products generated in near-site surrounding areas. Therefore, a comparison was possible between natural blank and anthropogenically polluted geochemical values for some local soils.