Plants as material culture in the Near Eastern Neolithic: Perspectives from the silica skeleton artifactual remains at Çatalhöyük

Investigating plants used for building and craft activities is important for understanding how environments surrounding archaeological settlements were exploited, as well as for considering the social practices involved in the creation and use of plant objects. Evidence for such plant uses has been observed at many Near Eastern Neolithic sites but not widely discussed. Survival may occur in a number of ways, including as impressions in clay, and as charred or desiccated macroremains. Another, less well-known, way in which plant artifacts can be found is as silica skeletons (phytoliths). Formed by the in situ decay of plants, their analysis may tell us about taxa exploited, and locations in which plant artifacts were used or discarded. At Çatalhöyük, an abundance of silicified traces of plants used in building materials and for craft activities survive, and are found in domestic and burial contexts. Their analysis demonstrates the routine use of wild plants, especially from wetland areas, for basketry (mats, baskets and cordage) and construction, as well as the secondary use of cereal husk chaff in certain types of building materials. The numerous finds suggest that plant-based containers played an important role as an artifactual class, even after the adoption of early pottery.     

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Abstract

Plant macroremains were recovered during the renewed excavation at Grap?eva ?pilja, a cave on the island of Hvar in Croatia. This is the first archaeoboatnical investigation on an eastern Adriatic island to use flotation samples. Samples were taken from layers dating from the Early Neolithic to the Middle Bronze Age (ca. 6000–1500 B.C.). Sixteen radiocarbon dates obtained from wood charcoal date the samples precisely. Detailed archaeobotanical analyses of plant macroremains reveal plant use during the occupation of the cave, with the highest density of plant remains in the Neolithic. Oak acorns were the most abundant plant remains. Finds of two types of juniper berry cones, various parts of gymnosperm cones, and cypress seeds and leaves indicate that the Mediterranean evergreen woodland was exploited. Remains of cultivated plants are rare. A small number of cereal grains, including emmer, einkorn, and possibly bread wheat were recovered from the Neolithic layers, as well as a few wheat grains from later horizons. Remains of typical wild Mediterranean fruits included almond nutshell fragments, a grape pip, and a fig seed. These finds indicate that the occupants of Grap?eva utilized processed crops but also gathered plants from the wild for food, fuel, and perhaps ritual. Fourier Transform Infrared Spectroscopy (FTIR) analysis was performed in order to assess charred versus mineralized preservation. Macroplant remains from Grap?eva were compared to the few available plant analyses from the eastern Adriatic. This comparison provides evidence that caves had different functions both from each other and from open-air sites. The plant remains are discussed in the context of the spread of farming on both sides of the Adriatic.     

Shepherds and plants in the Alps: multi-proxy archaeobotanical analysis of neolithic dung from “La Grande Rivoire” (Isère,France)

The analysis of phytoliths, pollen, charcoal and other macroremains was carried out in the neolithic shelter of “La Grande Rivoire”, Vercors massif (French Alps). The results show the predominance of tree species, in the form of phytoliths, clustered pollen, stomata, small branches charcoal, needles, bark, buds… The practice of leaf fodder is already known in the alpine and circum-alpine area from archaeological and historical sources. The analyses of the neolithic dung levels of “La Grande Rivoire” illustrate the use of leafy and flowering tree branches as fodder. The results also suggest that some species were used for special purpose in relation with the tending of livestock (litter, dietary supplement, veterinary practices).     

Selective woodland exploitation for charcoal production. A detailed analysis of charcoal kiln remains (ca. 1300–1900 AD) from Zoersel (northern Belgium)

A detailed study of charcoal burning activities has been made for the Zoersel forest (Northern Belgium) based on an inventory of charcoal kiln remains, the analyses of wood charcoal and other charred botanical macroremains and radiocarbon dating of 10 of these kilns. Age determination of the youngest kilns was refined by dendrochronological analysis of trees growing on top of these kiln sites. The results show that, although many kilns were found, charcoal was produced in Zoersel only at certain moments during late and post-medieval times suggesting that charcoal burning was not a part of the regular management practice of these forests. The wood used for the production of charcoal mainly consists of taxa of alluvial (alder) forests while the kilns are situated on sites that currently are rather dry, with an oak dominated vegetation. For the older kilns, this contrast could be explained by an important change in local soil conditions. The younger kilns may be related to the conversion of alder woodland to grassland in the lower parts of the domain, with the kilns being constructed in the nearby dryer woodland areas.     

How an integrated diagnostic approach can help in a correct evaluation of the state of preservation of waterlogged archaeological wooden artefacts

Artefacts made of wood coming from archaeological excavations provide insights into human cultural behaviour of the past. They show how man utilised natural resources and how the development of woodworking techniques and artistic endeavour were developed. Within archaeological contexts, waterlogged anaerobic conditions generally preserve the appearance of artefacts, although wood is subject to severe decay processes. The said conditions can transform the original material into a new one, thus demonstrating specific differences from those of the “fresh” wood of the same species. In order to assess these new properties correctly, an integrated diagnostic approach is needed, one which includes a multidisciplinary (micromorphological, physical and chemical) evaluation of the state of preservation.     

A new approach to study the fuel used in hearths by hunter-gatherers at the Upper Palaeolithic site of Abri Pataud (Dordogne,France)

The fuel used in hearths in the Upper Palaeolithic period and the management of this fuel have long given rise to questions on intentional or opportunistic human comportment. To understand how fuel was managed during the Aurignacian and Gravettian cultures, hearth samples from the French site of Abri Pataud (ca. 34–20 kyr BP) were collected. An image analysis method for the automated quantification of burnt particles from macroscopic-to-microscopic sediment fractions was developed, and the results obtained using this method were compared with the palaeoenvironmental data available close to the site. At Abri Pataud, the use of bones was dominant during the Pleniglacial, suggesting an intentional practice. However, environmental pressures could have influenced the fuel management practices of the hunter-gatherers, even if the dualistic relationship between the availability of firewood and the use of bone in hearths must be considered. Thus, burnt particle quantification provides more than just an observation of burnt macroremains in hearths: it relates to fundamental information on human behavior.     

Archaeological applications of testate amoebae analyses: a case study from Derryville,Co. Tipperary,Ireland

The value of testate amoebae in the reconstruction of changes in surface wetness from ombrotrophic mires is well known, but the potential value of such records in specifically archaeological investigations has not yet been investigated. This note describes the analysis of testate amoebae for a sediment sequence from the multi-period wetland archaeological site of Derryville, Co. Tipperary, Ireland. The reconstructed watertable is presented and plotted against the range of dates from excavated archaeological features in the wetland area. The data demonstrate a clear association between periods of low watertable and increased anthropogenic activity as reflected by site construction. The value of testate amoebae in future integrated archaeological investigations of wetland systems is discussed.     

A new approach to recording and monitoring wet-preserved archaeological wood using three-dimensional laser scanning

The analysis and preservation of organic materials preserved within wetland environments represents one of the most costly parts of any post-excavation strategy. This paper outlines the application of high-resolution terrestrial laser scanning to one class of preserved material, worked archaeological wood. Scanning allowed the recording of the artefacts in three dimensions and the identification of features such as toolmarks. Features can be measured and volumetrically modelled within the digital environment, which may not always be possible for these often fragile materials using conventional techniques. Repeat scanning of the artefacts provided an opportunity to use comparative analysis software to investigate changes in the morphology of artefacts under contrasting conditions of short-term storage. The results suggest that immersion in water results in the least deterioration, whereas both freezing and air-drying caused distortion and degradation. This paper demonstrates that laser scanning provides a viable alternative post-excavation method for the recording, analysis and long-term ‘virtual archiving’ of organic archaeological materials, which may be more cost-effective in some instances than other methods of preservation.     

The Environment and Subsistence of the Early Neolithic Settlement Area at Těšetice-Kyjovice,Czech Republic

This paper presents a reconstruction of environmental conditions and subsistence strategies in the Early Neolithic (6th Millenium BC) settlement area at Tě?etice-Kyjovice (Czech Republic). Our detailed reconstruction of the environment contributes to the unravelling of the genesis and spread of steppes and the formation of secondary anthropogenic forest-free areas in the Holocene in eastern-Central Europe. Mollusc shells, charcoals and plant macroremains were used as on-site evidence of a settlement environment. A relatively warm and dry anthropogenic forest-free area is reconstructed for the immediate vicinity of the Early Neolithic settlement. Communities of mixed deciduous forests are recorded in the surroundings of the settlement. Plant macroremains reflect the characteristic Neolithic range of cultivated plants (e.g. Triticum monococcum, Triticum dicoccon, Lens culinaris and Pisum sativum). Papaver somniferum seeds were also found, possibly constituting the oldest evidence of its presence and cultivation in the territory of the Czech Republic.     

Changes in the Physico-Chemical and Microbial Nature of Wetlands from the Leaching of Chromated Copper Arsenate (CCA)-Treated Wood

Abstract

Microbial activities are responsible for reducing the harmful effects of pollutants in different burial environments. Within wetlands in particular, microorganisms play an important role in the transformation of heavy metals and metalloids via direct or indirect oxidation/reduction. In turn, these microbial transformations can lead to the detoxification of pollutant elements such as copper, chromium and arsenic that comprise CCA-treated wood.

CCA was the most commonly used wood preservative in the UK (up until its partial ban in 2004). CCA prolongs the service life of wood by making it resistant to microbiological attack. As such, it has been regularly used in the construction of platforms and boardwalks in wetlands. However, recent concerns over the impact of the chemical constituents of this treatment on both the environment and human health have prompted the introduction of legislation in order to ensure that this type of treated wood is disposed of in accordance with the relevant health and safety guidelines.

In light of this information, it is important to assess changes in the physico-chemical and microbial nature of wetlands associated with the leaching of CCA from wooden structures. The results will not only provide a greater scope for understanding the implications associated with the in situ preservation of the archaeological resource contained within these environments, but also highlight the potential ramifications for wetland ecosystem dynamics.     

Dendrochronological and radiocarbon dating of the medieval stronghold in Ujście (Poland)

In 2008, the archaeological museum in Piła carried out excavations in the site No. 5 in Ujście upon the river Noteć (Poland), at the Rybacka Street and in the Old Market Square. In 12 archaeological excavations and 4 surveys abundant wooden structures were discovered, from which about 800 samples were taken, mainly of pine (Pinus sylvestris L.) and oakwood (Quercus sp.). The studies were aimed at absolute dating of wood with the dendrochronological method, the wiggle matching fitting curves method, as well as anatomical determination of wood. Absolute dating of the oakwood from the Rybacka Street allowed to distinguish the oldest fortifications of the stronghold from the ninth century, and also intensive introduction of wood in the years 980–1080 AD, whereas analysis of wood from the Old Market (survey IV) allowed to distinguish eight structural levels, from the 1530s until the 970s. On the basis of the pine wood 227-year-long local chronology 2U_02A was produced, dated with the wiggle-matching method for the period 860–1080 (±10) cal. AD. Most of the pine samples proved to represent wood introduced in the 990s and 1040s (±10) cal. AD, and also some repairs in the years 1000–1030 and 1050–1070 (±10) cal. AD.     

New trials in the consolidation of waterlogged archaeological wood with different acetone-carried products

Some acetone-carried consolidants for waterlogged archaeological wood were tested in order to evaluate treatments able to save time and energy. In details, colophony (rosin), two esterified colophonies (Rosin 100^® and Rosin 459^®), a mixture of colophony with PEG 3400 and a vinyl acetate - vinyl versate copolymer (Vinavil 8020S^®) were tested. The treatments were carried out at temperatures of 20 and 35 °C on waterlogged maritime pine, elm, oak and beech. The materials came from the archaeological site of the ancient ships of Pisa (Tuscany, Italy) and were dated back to VII cent. BC – II cent. AD. To evaluate the processes, equilibrium moisture content and dimensional stability of treated wood samples at different relative humidity, and retention of impregnating products were measured; moreover macroscopic and microscopic examination were also run to respectively assess the shape and appearance of treated wood and the way of deposition of consolidants. The results highlighted that natural and modified colophony treatments gave the most satisfactory results both in the maintenance of shape and dimensions of samples and in the stabilization with respect to RH variations. Moreover, the equilibrium moisture contents of samples treated with R100 and R459 were much reduced in comparison to the other consolidants and to untreated archaeological wood. This fact was related to the high retention values of those products that occluded most of the porosity including the microporosity of cell walls. Therefore, in terms of higroscopicity treated wood was more similar to impregnating substances rather than to decayed wood. This fact was considered helpful in contrasting the moisture-related negative effects in cases of eventual faults in the climate control during e.g. exhibition and in protecting treated wood from the risks of new fungal attacks.     

Lipid residue analyses of Early Neolithic funnel-beaker pottery from Skogsmossen,eastern Central Sweden,and the earliest evidence of dairying in Sweden

This study address the question of the use and function of Early Neolithic (4000–3000 cal. BC) funnel-beaker pots from Mälardalen in eastern Central Sweden. The material studied is pottery from a wetland offering at the site Skogsmossen in the province of Västmanland. While deposited under ritual circumstances in a fen, the pots were likely used in a domestic domain on the settlement adjacent to the offering fen, prior to final deposition. The lipid analysis indicate a varied vessel use, there are traces of aquatic resources, plants, terrestrial animals and milk. The identification of milk residue is the oldest so far from Sweden.     

Settlement and environmental history of a multilayered settlement mound in Niederröblingen (central Germany) – a multi-proxy approach

A multi-disciplinary palaeoecological approach on a sequence of dated archaeosediments was accomplished. The sediments derive from a multilayered prehistoric settlement mound in central Germany, representing the remnants of a prehistoric village. Based on the analysis of biological remains and geochemical/physical analysis of the settlement layers its environment was reconstructed. There is a trend to increasing anthropogenic activities and impact on the environment represented through a rise of indicators for productive surplus from the Early Neolithic (5300–4900 BC) until the Roman Times (400 AD). During the Early Neolithic, shifting flat settlements were situated in a locally opened landscape. The immediate surrounding of the floodplain was used by the settlers for their economic requirements (e.g. wood from the riparian forest). After a hiatus of ca. 1900 years, a multilayered settlement mount rose from Late Neolithic Times (3000 BC) to Roman Times. Since the Middle Bronze Age (approximately 1500 BC) the riparian forest was obviously replaced by agricultural fields and meadows and henceforward the hinterland used by the settlers probably grew in size. The continuing demand of wood was maintained by the acquisition of more distant sources. The onset of house constructions substituting wood by loam (wattle and daub) might be a possible societal response to this shortfall. This is reflected in the growing thickness and composition of the settlement layers, as well as in the archaeological record (e.g. tumbled wattle and daub house walls). The rising of the groundwater table and the start of severe floods of the adjacent river Helme during pre-Roman Iron Age (approx. 800–100 BC) might reflect a geomorphological response to the increased land use intensity at a regional scale.     

Branch age and diameter: useful criteria for recognising woodland management in the present and past?

When prehistoric archaeological sites yield non-carbonised wood, one of the ways to test for management practices consisting of pollarding and coppicing is analysis of branch diameter and age. However, the interpretation of such data is often based on assumptions. To test whether it is in fact possible to identify past woodland management on the basis of age/diameter analysis in archaeological wood assemblages, this paper presents models that predict the expected age and diameter distribution of branches from unmanaged and managed trees. The models have been tested using data on modern-day Alnus glutinosa, Fraxinus excelsior and species of the genus Salix. Branches of modern-day unmanaged and managed trees with a diameter up to approx. 2 cm (not an absolute limit) have a comparable age. Branches with a diameter of approx. 2–6 cm from unmanaged trees are older than similar branches from managed trees. The age distribution in the latter also ends abruptly. The age/diameter data from the modern-day trees indicate that the models can be used to discern management in the past, if branches up to approx. 2 cm in diameter are avoided and if, critically, taxon, sample size, growing conditions, natural disturbance/opportunistic wood collection and the possibility of diameter selection are taken into account. Archaeological datasets mainly from prehistoric sites are then reinterpreted by means of comparison with the models. Indications of management in prehistory as demonstrated by age/diameter are scarce but available. There is thus a clear need for further research in this field. Practical suggestions are provided for improving the quality of future research on woodland management practices by means of branch age/diameter analysis.     

Reburial of shipwrecks in marine sediments: a long-term study on wood degradation

Historical shipwrecks in marine environments are continuously decomposed by wood-degrading organisms, adapted to this specific environment. To protect the wrecks from degradation and to preserve the unique remains for future generations, reburial of wrecks using various covering materials has been suggested as a long-term preservation method. The following experiment was carried out to study the bio-protective effect of sediment. Sound oak, pine, and birch samples were buried above and within marine sediment in Marstrand harbour, and retrieved for analysis after 6, 12, 24, and 36 months. Macroscopic as well as light-microscopic examinations were carried out on each occasion. Marine borers (shipworm, Limnoria), soft rot and tunnelling bacteria were wood degraders immediately above the seabed; soft rot, tunnelling bacteria, and erosion bacteria were active 10 cm below the seabed; erosion bacteria were the only degraders at a depth of 43 cm below the seabed. The wood species had different durability towards the decay agents. After 3 years, wood samples above the seabed were totally decomposed, whereas wood was highly protected at 43 cm depth in sediment. In the sediment, decay decreased significantly with depth of burial. The results suggest that reburial of shipwrecks in marine sediment can be recommended as a simple and efficient method for long-term preservation of the wooden cultural heritage.     

Investigating crop processing using phytolith analysis: the example of rice and millets

The application of crop processing models to macro-botanical assemblages has traditionally been used to interpret past husbandry practices and organisation of labour involved in crop-processing. Phytoliths offer an alternative method of analysis because they are durable in most environments, regardless of whether plant parts are charred, and the identification of plant types and plant parts allows them to be used in much the same way as macro-botanical remains. Indeed macro-remains and phytoliths are complementary datasets for examining the input of plant parts, such as crop-processing waste, into archaeological deposits. We outline crop-processing models in relation to macro-remains and then develop the framework for their application to archaeological phytolith assemblages. Rice and millet processing models are explored in relation to patterns expected in both macro-remains and phytoliths. The utility of these models is demonstrated with archaeological evidence from the site of Mahagara, an early farming site in North-Central India. The results indicate a way to employ phytoliths in archaeology which complements the fragmentary evidence available from plant macroremains.     

Tikal timbers and temples: ancient Maya agroforestry and the end of time

Tikal, a major lowland Maya civic-ceremonial center in the heart of the Petén region of Central America, relied heavily on the adjacent lowland rainforest as a resource base for fuel and construction materials. In this study, we analyzed 135 wood samples from timbers used in the construction of all six of the city's major temples as well as two major palaces to determine which tree species were being exploited and to better understand ancient Maya agroforestry practices during the Late Classic period. We found evidence for a change in preference from the large-growing, upland forest species, Manilkara zapota, to a seasonal wetland species Haematoxylon campechianum in A.D. 741 as well as a decrease in lintel beam widths over time. Though M. zapota later returned as the wood species of choice in A.D. 810, beam widths were found to be significantly smaller. These findings concur with models that hypothesize widespread deforestation during the Late Classic period and indicate a declining forest resource base by the 9th century A.D. Because of the many large timbers available for temple construction in the 8th century, some system of forest conservation is indicated for the ancient Maya prior to the Late Classic period.     

Roman landscape and agriculture on the Ligurian coast through macro and microremains from a Vada Sabatia well (Vado Ligure,Italy)

Abstract

The results of an analysis on plant remains (fruit, seeds, pollen and wood) found in sediments in a Roman well in Vada Sabatia (Vado Ligure, Liguria, Italy), dated between the first and fourth centuries AD are presented. The remains are well preserved and constitute an exceptional record of the Ligurian area. Five layers have been recognised: three corresponding to the well when in use and two to the well when it was no longer in use. The vegetational cover of the area has been found to be similar to that observed in the coastal plain near Albingaunum (Albenga) pertaining to the same period. Moreover, the two superficial layers have cumulated a large amount of macroremains related to the period in which the well was no longer in use. The principal tree and vegetable crops and cereals of the coastal plain were present, due to the influence of maritime and mercantile trade, as were the prevailing ruderal and weed species and the tree cover. The presence of carpological remains of Castanea sativa, Secale cereale, Beta vulgaris and Cucumis sativus is reported for the first time in the Roman Age in Liguria. The influence of the arrival of the Romans can be seen from new crops, such as Prunus persica, and the introduction of exotic fruit like Phoenix dactylifera and Ziziphus jujuba. Several wooden artefacts, for example, a rack for drying lucerne and a tool handle, made of Cornus or Viburnum and Viburnum cf. lantana respectively, have been found. The well has proved to be an ideal location for the preservation of plant remains compared with other studied archaeological situations in Liguria and in Southern France, as it presents a higher variety of cultivated fruits, vegetables and cereals.     

A preliminary study on using enzymes in cleaning archaeological wood

The main goal of this study was to study and evaluate the effect of hydrolyzing enzymes on the anatomical structure and chemical composition of archaeological wood samples. Pine and beech wood samples, which were taken from anonymous mashrabia, have been cleaned with three types of enzymes then a scanning electron microscopy (SEM) and infrared spectroscopy (FTIR) study were undertaken, to see if any significant structural or chemical differences could be detected between “untreated” and “treated” wood. No dramatic changes in functional groups on the wood surface, as monitored by infrared spectroscopy, occurred in the samples before and after enzymatic cleaning. SEM data, however, show that protease and lipase enzymes may give good results in cleaning wood surface, but the enzyme residues remaining on the cell walls of archaeological wood are another point to consider.