Age determination of Petra's engineered landscape – optically stimulated luminescence (OSL) and radiocarbon ages of runoff terrace systems in the Eastern Highlands of Jordan

The unfavourable mountainous environment of the Petra region in southern Jordan was modified by ancient engineers to supply the Nabataean/Roman city of Petra with food and water. The area was reclaimed by installing extended runoff terrace systems and hydraulic structures. The agricultural terrace systems have so far been dated based on surface pottery, and the chronology of the systems is under debate. In this study, optically stimulated luminescence (OSL) and radiocarbon dating techniques were successfully applied to date these terrace systems. Samples were taken from the fills of agricultural terraces and underneath their walls to determine the chronology of the construction, use and abandonment of the agricultural terraces. The results suggest that runoff farming in the Petra region started around the beginning of the Common Era, and construction, use and maintenance lasted at least until 800 AD.     

Radiocarbon dating of prehistoric hearths in alpine northern Sweden: problems and possibilities

The chronology of prehistoric Sami settlement sites has previously been established by conventional radiocarbon dating of bulk charcoal samples associated with hearths from sunken hut floors (stállo-foundations). Here we present results of a comprehensive dating exercise of stállo-foundations in the alpine area of northern Scandinavia using Accelerator Mass Spectrometry (AMS) radiocarbon dating of charcoal. Over a 3 km² study area, AMS calibrated ages of hearth charcoal from 22 stállo-foundations across 12 sites securely date these features to between cal. AD 640 and AD 1180. Only small variations in age were found between charcoal samples from different areas of a given hearth. Statistical analysis of all the charcoal AMS radiocarbon dates obtained reveals that 12 stállo-foundations across nine sites are contemporaneous and date to the Viking Period (AD 800–AD 1050). The tightly constrained AMS-based chronology of stállo-foundations contrasts with the existing chronology based on conventional radiocarbon analysis, which places these features within a significantly greater time-frame of between AD 600 and AD 1900, with most dates ranging between AD 800 and AD 1350.This discrepancy is likely to result from the necessity of collecting composite hearth charcoal particles, which may originate from different phases of occupation, in order to achieve the required final carbon content for conventional radiocarbon analysis. We argue that the new AMS-based radiocarbon chronology of stállo-foundations presented here supersedes the existing chronology based on conventional (Gas Proportional counting) radiocarbon analysis and we advocate the use of AMS radiocarbon dating in future hearth investigations.     

Agricultural slope management and soil erosion at La Laguna,Tlaxcala, Mexico

Several superimposed systems of agricultural terracing are preserved at the archaeological site of La Laguna in central Mexico. Excavations uncovered complex stratigraphic sequences of terrace fills and colluvial deposits. Their chronology was established by radiocarbon, optically stimulated luminescence (OSL), and the presence of diagnostic features and artifacts. The Formative occupations of the site (ca. 600–400 BC and 100 BC–AD 100) resulted in severe erosion and exposure of indurated subsoil horizons. In the Middle to Late Postclassic (AD 1150–1520) stone-walled terraces were built to recover the degraded slopes for cultivation. Renewed reclamation works have been undertaken since the Colonial period, eventually taking the form of sloping-field terraces with berms planted in maguey. The reconstructed sequence of local land use underscores the risks of dating agricultural features by association with sherd scatters, as well as the complexity of the relationships between demographic variables, agricultural intensity and terracing.     

The 13th century polynesian colonization of Hawai’i Island

We assess 926 radiocarbon dates from Hawai’i Island, the largest assemblage of dates compiled from a single island in Oceania. Based on a classificatory approach that arranges the dates based on their reliability, accuracy, and precision, our results indicate that the most reliable estimate for the initial Polynesian colonization of Hawai’i Island is AD 1220–1261, ∼250 to 450 years later than the current consensus. This conclusion is strikingly convergent with recent estimates for the colonization of remote East Polynesia. Our analysis highlights the need for wood charcoal identification to insure selection of short-lived plants/plant parts for radiocarbon dating, and that a reliance on dating unidentified wood charcoal is a waste of resources that only serves to retard progress in refining the settlement chronology of Hawai’i Island and other locations.     

四川广汉三星堆遗址四号祭祀坑的碳十四年代研究

2020年,广汉三星堆遗址新发现祭祀坑的田野考古发掘工作正式启动,为解决祭祀坑的年代问题,四川省文物考古研究院委托国家文物局考古研究中心与北京大学考古文博学院考古年代学联合实验室对四号祭祀坑开展了碳十四年代研究,得到6个碳十四年代数据,经过贝叶斯统计树轮校正计算得到其埋藏年代有95.4%的概率落在距今3148—2966年的时间范围之内,属商代晚期。     

Radiocarbon Dating of Architectural Mortar: A Case Study in the Maya Region,Quintana Roo,Mexico

Abstract

The use of radiocarbon dating to analyze mortar and charcoal inclusions within mortar or plaster is a useful way to date the construction of architecture, particularly when options for other chronometric methods are limited. In the Yalahau region of northern Quintana Roo, Mexico, members of the Yalahau Regional Human Ecology Project have faced challenges in dating buildings made of large blocks of stone in the Megalithic architectural style. The Megalithic style poses serious problems for any analysis, as excavating into structures with stones weighing several tons can be dangerous, expensive, and time consuming. Additionally, there are no associated sculptures, texts with dates, or other traditionally accessible chronological markers. These factors have resulted in a reliance on a ceramic chronology despite the uncertainty of the dating of many ceramic types in this region, as well as the questionable contextual associations between recovered ceramics and architectural construction phases. Megalithic-style structures at the ancient Maya site of El Naranjal have residual mortar with charcoal inclusions left behind during the mortar-making processes that can be extracted and dated with AMS ¹⁴C methods. Several samples of mortar and charcoal were obtained from structures 1 and 10 from exposed exterior walls and an interior vault. The resulting dates confirm the date for the construction based on ceramics excavated from the same site.     

Investigating the likelihood of a reservoir offset in the radiocarbon record for ancient Egypt

Some radiocarbon dates for ancient Egypt have been significantly offset from the established historical chronology (see Bonani et al., 2001). In this paper, short-lived plant species collected in Egypt between 1700 and 1900 AD were used to investigate the possibility that the radiocarbon record had been influenced by reservoir effects. AMS radiocarbon measurements were made on 66 known-age samples, resulting in an average offset from expected values of 19 years. The implications of this minor discrepancy on the likelihood of a reservoir process are discussed, and the agreement of the data with recent models of radiocarbon seasonality is also considered.     

The Short History of the Ifugao Rice Terraces: A Local Response to the Spanish Conquest

Establishing the construction sequence of agricultural terraces is extremely complicated due to the nature of their technological foundation and use. A number of methodological approaches have been developed to address this difficulty, such as bulk soil ¹⁴C dating, Optically-Stimulated Luminescence (OSL), sediment grain size, or a combination of these, but a fundamental problem of stratigraphic disturbance still exists. In this article, we utilize multiple datasets, including radiocarbon determinations, faunal isotopic signatures, human osteological remains, archaeobotanical data sets, energetics assessments, and spatial data to establish the origins of Philippine Cordillera rice terraces. Dominant historical narratives in the region suggest a 2000–3000 b.p. inception of the terrace systems, but previous Bayesian modeling and current archaeobotanical, ethnohistorical, and ethnographic data indicate that the shift to wet-rice cultivation is a recent phenomenon and a response to the intrusion of the Spanish Empire in the northern highland Philippines.     

Implications of a freshwater radiocarbon reservoir correction for the timing of late Holocene settlement of the Elk Hills,Kern County,California

Uncertainties regarding the magnitude of freshwater radiocarbon reservoir effects can introduce random errors into dates on archaeological freshwater carbonates. As a result, many archaeologists avoid dating freshwater shells unless no other datable materials are available. The chronology of prehistoric occupation of the former Naval Petroleum Reserve No. 1 (NPR-1) at Elk Hills, Kern County, has been established with 50 radiocarbon dates on freshwater mussels (Gonidea and Anodonta sp.). Characterization of any freshwater radiocarbon reservoir effect is crucial for the accurate interpretation of inferred settlement and subsistence changes on the Elk Hills. Paired charcoal and freshwater mussels sampled from closely associated contexts were dated to identify a freshwater reservoir effect. Paired Anodonta and Gonidea sp. shells were dated to investigate interspecific differences in fractionation. Results indicate that a 340 ± 20 ¹⁴C yr correction should be applied to conventional ¹⁴C dates on freshwater carbonates in the Buena Vista Basin before calendar calibration. Evidence of interspecific differences is inconclusive. Dates recalibrated with the reservoir correction indicate that widespread occupation of the Elk Hills is correlated with increasing precipitation towards the end of the Medieval Climatic Anomaly and during the Little Ice Age, suggesting that slough resource exploitation may have been driven by regional population pressure rather than drought-related declines in aquatic productivity.     

Debates over Palaeolithic chronology – the reliability of C is confirmed

The debate about the complex issues of human development during the Middle to Upper Palaeolithic transition period (45–35 ka BP) has been hampered by concerns about the reliability of the radiocarbon dating method. Large ¹⁴C anomalies were postulated and radiocarbon dating was considered flawed. We show here that these issues are no longer relevant, because the large anomalies are artefacts beyond plausible physical limits for their magnitude. Previous inconsistencies between ¹⁴C radiocarbon datasets have been resolved, and a new radiocarbon calibration curve, IntCal09 (Reimer et al., 2009), was created. Improved procedures for bone collagen extraction and charcoal pre-treatment generally result in older ages, consistent with independently dated time markers.     

Geoarchaeological studies on Roman time harbour sediments in Cologne — comparison of different OSL dating techniques

Due to the construction of a new North-South subway in Cologne, Roman time harbour sediments were exposed and were sampled for luminescence dating. A very good independent age control was given by the precise knowledge of the chronology of Roman activity and by radiocarbon ages of charcoal samples. Hence, different methodological approaches within luminescence dating were applied for Holocene heterogeneously bleached fluvial samples and were compared to the known ages. For one sample, optically stimulated luminescence (OSL) dating was applied to coarse-grained quartz using a single aliquot regenerative-dose (SAR) protocol. After D_e-measurements, different statistical approaches were tested (i.e. arithmetic mean, median, minimum age model, finite mixture model, leading edge method and the Fuchs and Lang approach). It is demonstrated that the Fuchs and Lang approach along with the leading edge method yielded the best matching OSL ages with respect to the known ages.     

Chronostratigraphy of an Eroding Complex Atlantic Round House,Baile Sear,Scotland

A high-resolution chronostratigraphy has been established for an eroding Atlantic round house at Sloc Sàbhaidh (North Uist, Scotland), combining detailed OSL profiling and dating of sediments encompassing the main bracketing events associated with the monument, radiocarbon AMS dates on bone recovered from excavated features and fills within it, and TL dates on pottery and burnt clay. Concordant OSL and radiocarbon evidence place construction of the wheelhouse in the first to second centuries AD, contemporary with dates from the primary occupation. Beneath the wheelhouse, clay deposits containing burnt material, attest to cultural activity in vicinity to the monument in the preceding second to first centuries BC. At a later date, the southern wall collapsed, was rebuilt, and the interior spaces to the monument re-structured. The chronology for the later horizons identified from the sediment luminescence dates extends to the second half of the first millennium AD, which goes beyond the range of the radiocarbon dates obtained. The data from ceramics encompass both periods. The juxtaposition of the dating evidence is discussed relative to short and longer chronologies for this Iron Age monument. Corollaries of this research are the implications that based on the long chronology, some of the ecofacts (bone) appear to be residual, and that the temporal duration of Hebridean Coarse Ware may extend into the second half of the first millennium AD.     

Chronology during the Bronze Age in the archaeological site Tell Qubr Abu al-‘Atiq, Syria

Archaeosediments are deposits with a direct or indirect anthropogenic component. They provide useful information about past human activities and interaction with the environment. When other materials, such as pottery, are present in archaeosediment layers, the combination of TL ages from pottery and OSL ages from sediments can provide complete data about the occupation and evolution of an archaeological setting. In Mesopotamia, tells are mounds formed by the debris of human occupation and the accumulation of muddy sediments mainly due to the decomposition of mud bricks in ancient towns. Many other materials such as pottery fragments, bones and charcoal can be found in the sediment layers. The combination of OSL, TL and radiocarbon ages can be very useful in the case of the Bronze Age Period in Syria, allowing the occupation sequence of such archaeological sites to be reconstructed. Tell Qubr Abu al-’Atiq, is located on the left bank of the Middle Euphrates River (Syria). The archaeological artefacts found in the sediment layers (pottery) collected during excavations in two areas of the site, indicated the occupation of the tell during the Early and Late Bronze Age by typological pottery classification. The radiocarbon ages of charcoal indicate that human occupation fits the archaeological hypothesis, providing an older and maximum occupation period between 2800 and 2300 BC and a younger period between 1400 and 900 BC. OSL dating of sediments shows ages younger than charcoal, while TL ages of pottery are generally older than sediment and charcoal ages. This can be explained as the different materials correspond to different events. The charcoal and pottery correspond to occupation periods, while sediments correspond to the further destruction of the site.     

Potential geoarchaeological sites for luminescence dating in the Ganga Bhagirathi-Hugli delta,west Bengal,India

Archaeological studies in the upper and lower part of the Ganga-Bhaghrathi-Hugli delta were taken up to understand the nature of site formation and human adaptation in a dynamic fluvial zone. This aspect has been neglected in Indian archaeology. However archaeological dating using typological information, has an error margin of a couple of centuries and hence, is of limited use. We suggest that high resolution chronology using Optically Stimulated Luminescence (OSL) and radiocarbon dating can be quite effective in the study of archaeology and human environment relationship in the Ganga-Brahmaputra Delta (GBD).     

Evaluating the Reliability of Fluoride Dating at Two Prehistoric Mound Sites in Mississippi

Abstract

Ion-selective electrode fluoride dating is used to address chronological problems at two mound sites located in Mississippi. At the Mississippian period (A.D. 900–1520) Lyon's Bluff site, 220K520, the fluoride content of deer and human bone is compared with radiocarbon dates and stratigraphic levels to evaluate the reliability of the fluoride dating method for understanding relative burial chronology. At a second site, Pocahontas Mound A (22HI500), fluoride content of deer bone is used to corroborate radiocarbon dates and to establish the proper chronology of levels associated with two distinct occupations (Archaic and Coles Creek/Plaquemine) identified in a large midden area. Fluoride analysis also is used to date a second midden area at this site. For Lyon's Bluff; fluoride dates did not correspond with accelerator mass spectrometry (AMS)-dated burials and midden strata. In contrast, fluoride dating proved very useful in determining chronological placement of midden levels and dating other areas at Pocahontas Mound A. Sample age, site location, soil, and bone preservation are considered as possible causes for the negative results at Lyon's Bluff.     

The earliest evidence of domesticated wheat in the Crimea at Chalcolithic Ardych-Burun

Abstract

This paper reports the discovery of the earliest evidence of domesticated wheat in the Crimean peninsula from the Ardych-Burun shell midden site, Ukraine. The Ardych-Burun site dates to middle of the 4th millennium cal b.c. For the first time, the chronology of a Ukrainian Chalcolithic period site has been established through direct radiocarbon dating of cereal grains retrieved from it. This discovery allows for a wider discussion of the chronology and geographical origins of domesticated plant species in Ukraine and the role the Caucasian corridor may have played in the spread of agriculture into eastern Europe. The presence of cereal crops in the southern Crimea enriches our understanding of the subsistence strategies of the coastal population, which was previously linked only with pastoralism, hunting, and the exploitation of marine resources.     

Technology,chronology and the role of crucible steel as inferred from iron objects of the ancient site at Junnar,India

Ordinary iron objects from an ancient habitation site at Junnar in India, dating to the 2nd BC to AD 2nd century, were examined for their microstructure, chemical composition and age. The objects were mostly made of high carbon steel with a homogeneous microstructure consisting of fine spherical particles of carbide in the ferrite background, free of non-metallic inclusions. Their carbon concentration ranged from 0.7% to over 1.6% with one exception at 0.2%. Some of them contained trace amounts of silicon, manganese and sulfur while one object retained cavities due to volume contraction during solidification reactions. These features indicate that the objects examined constitute an early example of Indian steel making in crucibles. Evidence was found that basic techniques needed for the success of crucible steel technology were mostly available at Junnar at the time. The radiocarbon measurement on carbon samples extracted from one of the iron objects placed its date between 176 BC and AD 20, in agreement with the radiocarbon dates of three charcoal samples from the same site. The forgoing results support that crucible steel was produced in India at a much earlier date than previously supposed, to serve as a material for specific needs arising in daily life.     

U-series dating of soda straw stalactites from excavated deposits: method development and application to Blanche Cave, Naracoorte, South Australia

This study aimed to further test the method, reported by St Pierre et al. (2009), to develop robust chronologies of deposits in limestone caves through U/Th (Uranium/Thorium or U-Series) dating of soda straw stalactites. The chronology of fossil bearing deposits at Blanche Cave was further constrained with thermal ionisation mass spectrometry (TIMS) U/Th dating of 17 additional soda straw stalactite samples, and results were compared to recalibrated ¹⁴C ages of charcoal. The results support the assertion that soda straw stalactites can provide ages close to the time of sediment deposition and may be used as reliable chronological markers, particularly for periods reaching or beyond the radiocarbon dating limit. The application of an enhanced cleaning technique facilitated the reduction of detrital Th in samples, significantly increasing age accuracy and precision. Additionally U/Th age accuracy and precision was increased through the application of site-specific measured U/Th ratios to correct for the detrital ²³⁰Th component in samples.     

THE RADIOCARBON CHRONOLOGY OF KOPIA,AN EARLY GLASS MANUFACTURING CENTRE IN INDIA

Right from the time of the Painted Grey Ware (PGW) culture, dating to c. 1200–600 bce , more than 210 archaeological sites in India have provided evidence of glass, but there has been no attempt to date the glass‐yielding layers by radiometric techniques. This has hampered the establishment of a chronology for the beginning and evolution of glass‐making in India. The site of Kopia was excavated by the first author for three seasons from 2004 to 2006 to understand the history, development and technology of glass production in India. The excavation produced evidence of a long period of occupation, covering the Fine Grey Ware (FGW), Northern Black Polished Ware (NBP), Sunga–Kushana and Gupta periods. Twenty accelerator mass spectrometry (AMS) and radiocarbon dates, all derived from charcoal samples and processed independently by three laboratories, are available from the site. The dates range in their calibrated form on average from the ninth to the second century bce in locality I and from the second century bce to the second century ad in locality II.