A NEW THERMOLUMINESCENCE DATING TECHNIQUE FOR HEATED FLINT*

A new thermoluminescence (TL) technique for determining the age of heated flint artefacts from archaeological sites is presented. It is a variant of the SAR protocol, which is usually used for OSL dating of sediment, but it is not based on a presumed model for fitting the dose–response curve. Dose recovery tests as well as comparisons with standard protocols show the accuracy of the new technique. It is found that the sensitivity of the thermoluminescence (TL) signal of flint in the orange–red waveband does not show severe changes due to the heating process while measuring the TL. This allows the application of a short SAR procedure, which requires only two dose points. The technique does not require as much instrument time as other SAR techniques, and thus is advantageous for dating very old samples. The major advantage of this new technique is the small amount of sample material required, which allows the dating of samples that are too small for standard TL dating techniques.     

THE SUBTRACTION TECHNIQUE OF THERMOLUMINESCENT DATING

Combination of the routine approaches of thermoluminescence dating, the fine-grain and inclusion methods, allows an age to be determined that is independent of knowledge of the environmental dose-rate. This socalled subtraction technique is exampled by several terracottas of museum origin and some pottery collected from archaeological contexts without associated burial media. Age determination is estimated to have an accuracy of around ± 12%, in favourable conditions.     

THE BILZINGSLEBEN ARCHAEOLOGICAL SITE: NEW DATING EVIDENCE

New absolute dates have been obtained for the Bilzingsleben (D.D.R.) archaeological site, using uranium-series analyses of travertine, and electron spin resonance (ESR) analyses of travertine and tooth enamel of rhinoceros. The results indicate that the site was apparently occupied during interglacial isotope stages 9 or 11. The surrounding terrain has been subsequently dissected by at least three discrete stages of fluvial erosion during succeeding glacial stages. Bilzingsleben is thus shown to be significantly older than the Lower Travertine at the nearby site of Ehringsdorf, assigned to isotope stage 7 by uranium-series dating. The latter assignment is confirmed by new ESR data presented here.     

SIMS‐SS,A NEW OBSIDIAN HYDRATION DATING METHOD: ANALYSIS AND THEORETICAL PRINCIPLES*

The water diffusion mechanism in obsidian has been revisited with the advent of a new dating approach employing secondary ion mass spectrometry (SIMS). The water diffusion SIMS(+) profile and the concept of a surface saturation (SS) layer in obsidians both provide a sound basis for the new diffusion age equation (SIMS‐SS) and are supported by dated world examples ( Liritzis et al. 2004 ). Here, we present the basic physical–chemical analysis of the mass transport phenomenon on which the new dating method is based. The crucial age parameter of the SIMS‐SS dating approach for archaeological obsidians—that is, the surface saturation (SS) layer—is supported by both theoretical and experimental data.     

OBSIDIAN HYDRATION DATING: AN IMPROVED OPTICAL TECHNIQUE FOR MEASURING THE WIDTH OF THE HYDRATION RIM

A simple optical method is described that will enhance the color contrast between the outer birefringent hydration rind and the inner unhydrated core on obsidian thin sections used for hydration dating. The technique utilizes a gypsum nccessory plate. The gypsum plate rotates all incoming light by 550nm causing the black isotropic core of the nhsidian to become transparent first-order pink and interacting with the transmitted light from the birefringent rind, by either addition or subtraction. to produce a second-order blue or a first-order yellow color.     

SOIL PHOSPHATE ANALYSIS: A NEW TECHNIQUE FOR MEASUREMENT IN THE FIELD USING A TEST STRIP*

A new method for soil phosphate analysis has been developed for field measurement which will increase the applicability of phosphate mapping in archaeological prospection.     

NEW CHRONOLOGICAL EVIDENCE FOR THE MIDDLE TO UPPER PALAEOLITHIC TRANSITION IN THE CZECH REPUBLIC AND SLOVAKIA: NEW OPTICALLY STIMULATED LUMINESCENCE DATING RESULTS

We report new optically stimulated luminescence (OSL) dates from the Central European sites of K?lna, Stránská skála, Bohunice, Vedrovice V, Vedrovice Ia, Moravský Krumlov IV and Dzeravá skala, which date to the Middle–Upper Palaeolithic transition period. There are important unresolved questions surrounding the timing of archaeological events during this crucial period in European prehistory. Archaeological layers from this time period are at the limits of the ¹⁴C method and most of these sites lack good chronology. The results of this dating project suggest that some parts of the current chronological framework may need to be revised. Although in many cases our OSL results are broadly consistent with previous dates obtained by ¹⁴C, in other cases they reveal unexpected surprises. One OSL result from K?lna opens up the possibility that Neanderthals may have survived in this part of Europe past the 30 ka bp mark as has been argued for several Neanderthal sites in southern Europe. The large Szeletian assemblage recovered from Vedrovice V may be significantly older than previously thought, which undermines the idea that the Szeletian culture is exclusively an Early Upper Palaeolithic industry. More dating research is needed to confirm the more controversial results of this research.     

DEPENDENCE OF SUPRALINEARITY ON PRE-DOSE: SOME OBSERVATIONS

Recent studies on pottery and related materials have shown there to be cases where the degree of supralinearity is dependent on the previous radiation history of the sample. Results are presented of two investigations of this variation with pre-dose: one using pottery, the other using fired feldspars. For these samples no simple form for the variation can be inferred.     

THE DATE AND SEQUENCE OF USE OF NEOLITHIC FUNERARY MONUMENTS: NEW AMS DATING EVIDENCE FROM THE COTSWOLD-SEVERN REGION

Summary.   In this paper we discuss 26 new Neolithic AMS dates obtained from human and animal bone from four previously undated funerary monuments in the Cotswold-Severn region. By strategically targeting particular portions of these skeletal assemblages, a number of valuable inferences are made concerning the extent of variation in apparently co-existing burial practices both within and between monuments. Of particular interest is the observation that variations in the extent to which interments have become disarticulated cannot necessarily be equated with chronological relationships regarding their deposition. This project has also obtained dates from cremated bone, which establish that the range of funerary treatments in practice during the earlier Neolithic also included cremation. Additionally it is observed that whilst some, apparently primary, deposits may in fact be later insertions, other material in apparently secondary contexts may actually return earlier Neolithic dates.     

A NEW DATING METHOD FOR HIGH‐CALCIUM ARCHAEOLOGICAL GLASSES BASED UPON SURFACE‐WATER DIFFUSION: PRELIMINARY CALIBRATIONS AND PROCEDURES*

The first European settlers came to North America in the early 17th century using glass in the form of containers and decorative objects. Thus, glass is a horizon marker for all historic period settlements and a potential source of chronometric dates at archaeological sites belonging to the historic period in the Americas. We have developed a new absolute dating method based upon water diffusion into the surface of manufactured glasses that predicts diffusion coefficients based upon variation in glass chemical constituents. Low‐temperature (< 190°C) hydration experiments have been performed on a set of five high‐calcium (21.7–28.3%) glasses that were used to manufacture wine bottles from the 17th?19th centuries. Infrared spectroscopy and secondary ion mass spectrometry was used to model the water diffusion/alkali exchange process. The ability of the model to accurately predict archaeological ages was evaluated with artefacts recovered from ceramic‐dated contexts at Thomas Jefferson's plantation known as Monticello.     

A NEW METHOD TO DATE PETROGLYPHS

A new calibrated method based on erosion phenomena is presented for the dating of petroglyphs (rock carvings and engravings) and geomorphic surfaces. In contrast to previous methods of petroglyph dating, which sought to determine the age of various mineral and organic deposits coating the art, microerosion analysis attempts to ascertain the time of mark production itself, by creating a geomorphologically based time frame. The method involves the establishment of calibration curves for the crucial variables to be considered. These are the rock type and climate of a particular region, microerosional indices and age. The theory, practical application, and prerequisites of the method are considered, and the paper concludes by defining the disadvantages and advantages of the method.     

THE DATING OF RELIEF-PATTERNED FLUE-TILES

The use of relief-patterned flue-tiles in Roman Britain falls into three main periods: c. 75–90, c. 120–25, and c. 155–75. The assignment of particular dies to each of these periods is examined. The nature of the industry and the specialised functions of particular types of tiles are discussed within the chronological framework. An appendix deals with the sequence of tiletypes used at Fishbourne and a chronological difficulty involving Fishbourne and the Chichester thermae.     

TOWARDS A NEW APPROACH TO ARCHAEOMAGNETIC DATING IN EUROPE USING GEOMAGNETIC FIELD MODELLING*

We introduce a new approach to producing secular variation curves for archaeomagnetic dating, using global geomagnetic field modelling techniques. Using published palaeosecular variation curves for five European locations as input, and a previous global model for regularization, we produce a model for the period ad 0–1900, which reproduces the input curves within their 95% confidence intervals, and successfully fits data from other regions in Europe. Our global model performs as well as a previous regional model, but additionally ensures consistency with physical constraints. We show that the curves currently used for dating are not mutually consistent, and therefore that in the future this new approach will provide more reliable curves for archaeomagnetic dating.