Coupling lead isotope analysis and petrography to characterize fabrics of storage and trade containers from Hala Sultan Tekke (Cyprus)*

Lead isotopes, thin‐ and sherd‐section analyses are coupled on pottery‐vessel fragments excavated from the Late Bronze Age site of Hala Sultan Tekke (south‐east Cyprus) and representing fabrics used for the production of storage and trade containers. The fabrics of the sherds are first described according to general macroscopic observations. Based on the different fabrics identified, a petrographic analysis is carried out on thin sections and compared to lead isotope results on the same samples. This study shows that a specific fabric corresponds to a specific lead isotopic composition and proposes different sources for the various groups of associated sherds/fabrics. It also demonstrates the compatibility and complementarity of petrography and lead isotopes within pottery provenance study.     

A Late Bronze Age Ship from Liman Tepe with Reference to the Late Bronze Age Ships from İZMIR / Bademgediği Tepesi and Kos / Seraglio

In this article, a Mycenaean pottery sherd from Liman Tepe is discussed. The piece, which was locally produced, probably belongs to a ring‐based crater (FS 281). Comparisons with other, similar sherds suggest that warriors aboard a ship are depicted. As one of the few examples of its period decorated in this way, the sherd has been dated to the early or middle phase of LH III C, belonging to the period after the collapse of the Hittite Empire in Anatolia and the Mycenaean kingdoms in mainland Greece. The depictions on this sherd are highly significant, as they contribute to the corpus of evidence for migrations from the western to the eastern Mediterranean and the unrest which characterized the period.     

Directional analysis of surface artefact distributions: a case study from the Murghab Delta, Turkmenistan

This paper investigates directional influences in the distribution of Bronze Age surface pottery in the northern Murghab Delta, Turkmenistan. Drawing upon a continuous dataset of pottery sherd counts obtained by intensive field survey, it examines the degree to which we can make sense of the archaeological processes at work in a heavily obstructed and dynamic landscape. In so doing, it makes use of two analytical methods that have rarely been used in archaeology: a) geostatistical analysis using variograms to investigate directional spatial autocorrelation in recorded sherd counts; and b) angular wavelet analysis in evaluating directional influences in the sherd distributions for particular chronological periods. While some kinds of directional influence can be identified visually, a quantitative approach is particularly useful in deconstructing such patterns. In this particular dataset, distinct but related directional processes can be identified and measured: a) the impact of the complex system of watercourses in the delta on both settlement and post-depositional processes; and b) recovery bias in the observations made during survey.     

NON-DESTRUCTIVE SURFACE ANALYSIS OF ROMAN TERRA SIGILLATA: A POSSIBLE TOOL IN PROVENANCE STUDIES?

In the past, studies on the average chemical composition of a sherd vs its origin have successfully been carried out, but attempts failed to reach the same goal with spot analysis (electron microprobe) on the high gloss surface of terra sigillata. When chemical data on the average composition of the surface is used for provenance determinations, significant results are obtainable on the basis of non-destructive energy dispersive X-ray fluorescence analysis (EDS-XFA). Terra sigillata from Arezzo, Lezoux, La Graufesenque and Lyon (± 20 B.C. to ± 150 A.D.) were analysed in order to determine the statistically distinctive chemical elements. It is clearly possible under favourable conditions to allocate archaeologically unknown sherds to specific pottery centres.     

The forest or the trees? Behavioral and methodological considerations for geochemical characterization of heavily-tempered ceramic pastes using NAA and LA-ICP-MS

In this paper, the utility of LA-ICP-MS for instrumentally separating clay and temper within pottery samples is examined through a well-known case study that has been previously characterized through NAA and petrography. Coarse Orange pottery is composed of kaolinitic clays heavily tempered within volcanic ash from the basalt-rich Tuxtla Mountains of southern Veracruz, Mexico. We attempt to address the following topics with analyses on this pottery: 1) can LA-ICP-MS replicate the same groups previously identified by NAA and petrography; 2) can instrumental isolation of the clay fraction within the pottery replicate known patterns in raw clay source geochemistry in the Tuxtla Mountains; 3) can data for both the clay and volcanic ash fractions of each pottery sherd be combined to simulate the bulk INAA data? The results demonstrate that the clay fraction of the pottery sherds can be isolated. Furthermore, the LA-ICP-MS data for the clay fractions display nearly identical chemistry to available NAA data for raw clay samples collected from geological contexts in the region. Instrumentally isolating the clay fraction in this case eliminates the homogenizing effects of adding a common temper and increases the chemical separation among groups making it easier to identify clay procurement strategies for each specimen. However, focusing only on the clay fraction ignores significant tempering variation. Attempts to simulate the bulk NAA by combining LA-ICP-MS data for clays and temper was reasonably successful in reestablishing the tempering variation lost by exclusive focus on clays, but such an approach could not replace the more precise data generated from NAA and petrography.     

Post‐Depositional Elemental Alterations in Pottery: Neutron Activation Analyses of Surface and Core Samples*

From 38 sherds with ‘corroded’ surfaces, two samples per sherd were examined using Neutron Activation Analysis, one from the surface and one from the core of each sherd, in order to analyse post‐depositional alterations of minor and trace elements. The most striking effect was that a leaching of Ca could be found at the surface. Another group of elements that is severely affected are the alkali metals, with Cs and Rb showing the strongest changes. A third conspicuous group of elements are the Rare Earth Elements. Finally, the effect of such alterations on a statistical data evaluation to classify pottery according to provenance is investigated.     

Teotihuacan pottery as evidence for subsistence practices involving maguey sap

As in most other pre-industrial cities, urban life at Teotihuacan was closely intertwined with ceramic technology, perhaps nowhere more so than in the realm of foodways. Here, we use two kinds of information derived from ancient pottery—ceramic residues and intra-site sherd distribution patterns—to shed new light on the city’s subsistence economy. We concentrate in particular on the amphora, a type of vessel that may have been used to contain aguamiel and pulque, liquid foodstuffs made of maguey sap. Distributional data distilled from surface collections of the Teotihuacan Mapping Project are informative about patterned variation in the use of these pots at the scale of the entire city. More focused analyses are aimed at chemical characterization of organic residues preserved in ceramic sherds recovered from recent excavations. Part of a broader project aimed at identifying both animal and plant remains, the results of the residue analysis provide the first direct identification of pulque remains in Teotihuacan pottery.     

CORRESPONDENCE AND DISCRIMINANT ANALYSES OF SAND AND SAND TEMPER COMPOSITIONS,TONTO BASIN,ARIZONA*

Geologists use petrographic modal analysis to relate fluvial sand composition to source rock composition, thus establishing provenance. Archaeologists seeking to establish provenance of sand temper in pottery can use similar petrographic methods, but their finer scale of investigation requires more precise statistical tools than those employed by geologists. A quantitative method for performing that task is presented. It utilizes correspondence analysis and discriminant analysis of logratio transformed point‐count data to define petrofacies, or sand temper resource procurement zones. The procedure is illustrated with sand and sand‐tempered sherd samples collected from the Tonto Basin, central Arizona; temporal trends in utilitarian ceramic production c. AD 100–1350 are reviewed.     

A comparison of chemical and petrographic analyses of Neolithic pottery from South-eastern Europe

This paper deals with the importance of chemical analyses in characterising prehistoric pottery fabrics. Two three-year projects focussed on the minero-petrographic and SEM/EDS analyses of the oldest pottery from south-east Europe (ca. 6000 cal BC). Whereas in the Impressed Ware culture of the Adriatic region, optical microscopy was sufficient to identify provenance, the more uniform geological background of the central Balkans required chemical analyses to be able to differentiate between different raw materials. Multiple bulk analyses of each sherd were obtained to gauge the variability in composition within each vessel. The limiting factor in determining provenance in this area appears to be the similarity of clay sources, not the inhomogeneity of the coarse pottery. This is shown here using results from four of the sites, including three where petrographic analyses could not establish provenance.     

甘肃新石器时代与青铜代陶器研究的内容和科学意义

综述了现代分析测试方法和数学方法在古代陶器成分分析、年代测定、制作工艺、产地判断、形态分析方面的应用以及甘肃新石器与青铜时代陶器研究的意义。     

THERMOLUMINESCENCE DATING OF POTTERY: AN ASSESSMENT OF THE DOSE-RATE FROM RUBIDIUM

The naturally occurring radioisotope ⁸⁷Rb makes a small contribution to the total dose-rate. Assuming an average potassium:rubidium ratio of 200:1 the contribution is estimated at 2.9% of the B dose-rate From potassium. The effect will be negligible in quartz inclusion dating because of the strong attenuation of the B- emission from ⁸⁷Rb. In fine-grain dating the omission of the ⁸⁷Rb contribution will overestimate the age of a pottery sherd by not more than 2% and this is regarded as of minor importance when the total error in the technique is at least 15%.     

Implications of Petrographic Temper Analysis for Oceanian Prehistory

Petrographic examination of prehistoric Pacific potsherds in thin section allows robust distinctions to be drawn between indigenous temper sands derived from islands where sherds were collected and exotic temper sands derived from other islands, except that calcareous temper sands of reef detritus are undiagnostic of origin. Ceramic transfer or movement of ceramic raw materials from island to island can be detected because small islands serve as virtual point sources of noncalcareous terrigenous sands, and local island geology is controlled by systematic and well-known geotectonic patterns. Prehistoric Oceanian pottery was made locally on multiple islands, rather than being dispersed from a discrete number of ceramic centers, but limited ceramic transfer was widespread within nearly all island groups. As temper analysis is independent of ceramic typology, sherd tempers in common with obsidian artifacts and other manuports provide unambiguous physical evidence for migration, trade, or exchange within and between island groups.     

Of Ships and Deer: early Western Mediterranean ship graffiti reappraised

Re‐analysis of the Hal Tarxien prehistoric ship graffiti, the incised figure on a pottery sherd, from the Neolithic site of Grapceva cave on a Croatian island, known as the ‘Hvar boat’, and the Villanovian‐Etruscan bronze razor from Bologna allow the last two to be reinterpreted as animals rather than ships, and the first to be dated to the Bronze Age Cemetery phase of the site. These findings require the earliest ship graffiti in the western Mediterranean to be reconsidered.     

Discrimination of Ceramic Surface Finishing by Vertical Scanning Interferometry

Finishing techniques are significant markers of the technological ‘know‐how’ involved in the production of the traditional, clay‐based ceramic ware. In order to provide a reliable tool to discriminate among two main surface processing techniques—that is, smoothing and burnishing—vertical scanning interferometry (VSI), a recently developed non‐destructive technique for analysing the surface roughness and topography, is applied. The smoothed areas have an obvious roughness expressed by linear structures. The latter are made of parallel ridges and trenches with an average depth of 15–20 μm. Burnishing leads to a lower topography and a lower roughness compared to the smoothed surface section. VSI quantifies the spatial distribution of the surface building blocks, which consist of phyllosilicate aggregates of variable size. The statistical treatment of the roughness data obtained by VSI shows that the surface topography provides significant information on the pottery processing and a clear qualitative and quantitative discrimination between different surfaces. VSI supports the reconstitution of the chaîne opératoire for traditional ceramic pottery and the recognition of the surface finishing techniques.     

仙人好楼居:襄阳新出相轮陶楼与中国浮图祠类证

湖北襄阳东汉—三国蔡越墓出土的相轮陶楼,在建筑形制上为汉式陶楼和印度式相轮塔刹的结合,在装饰母题上同时兼有汉地神仙瑞兽与印度—犍陀罗式有翼天人的图像,明显带有佛教初传时期汉、印文化杂糅的特点。本文在讨论陶楼形制的过程中,分别联系同期北方墓葬中出土的陶楼明器和汉晋之际江南地区的佛饰堆塑重楼魂瓶进行类比分析,证明这两类墓葬明器都与文献记载的"浮图祠"相关联。在佛教初传汉地时,由"仙人好楼居"的汉式重楼过渡到高层佛塔,浮图祠是初期的标志,襄阳蔡越墓陶楼或可看作是浮图祠的标准器。浮图祠用作明器进入墓葬,反映了汉地民间埋葬方式因佛教传入而起的新变化,并在随后长江中游六朝砖墓的建造中留下了印记。     

THE UTILIZATION OF TRACE CHEMICAL COMPOSITION TO CORRELATE BRITISH POST-MEDIEVAL POTTERY WITH EUROPEAN KILN SITE MATERIALS

This study uses X-ray fluorescent analysis to compare the trace chemical composition of seventeen pottery sherds excavated from sites in Britain with the trace analyses of twenty four sherds from continental sources. Results indicate that certain elements, notably zirconium, titanium, rubidium, and strontium show little variation within a particular sherd and are consistent among samples from the same source. Certain other elements appear to show wide variation which is possibly attributable to firing conditions, burial or is connected with the glaze. The comparisons of analyses indicate that nine of the seventeen British sherds can be closely correlated with particular continental sources. Tentative correlation is suggested for five sherds. The remaining three sherds clearly do not come from any of the sources investigated.     

Ancient Egyptian Pottery from the Subsurface Floodplain of the Saqqara–Memphis Area: Its Mineralogical and Geochemical Implications*

Potsherds recovered from the Saqqara–Memphis floodplain in Egypt, dated according to their typology and radiocarbon dating of the included sediments, are analysed geochemically and mineralogically to identify source materials and fabrication characteristics. Pottery layers were identified and potsherds were recovered from several settlement levels. Sherd typology was used to identify sherds from four periods (the Old and New Kingdoms, and from the Late Period to the Ptolemaic). The Pharaonic pieces were found at depths of between 8 and 12 m and the later material was between 6 and 3 m. Chemical analyses of the potsherds revealed three main source materials: local Nile silt, marl clay and mixed Nile silt–marl. Two marl clay types were recognized: marl clay from Upper Cretaceous marine sediment and another one from Late Pliocene deltaic sediments. The mineralogical composition of the pottery samples shows that the estimated firing temperature was about 850–900°C. No consistent differences in sherd mineralogy and geochemistry were found according to pottery types, so that the ancient Egyptian potters used essentially the same materials throughout the Pharaonic period. However, this initial study has revealed the existence of extensive pottery‐rich occupation sites buried within the Nile floodplain deposits between Memphis and Saqqara.     

Pottery Styles during the Early Jomon Period: Geochemical Perspectives on the Moroiso and Ukishima Pottery Styles

Energy‐dispersive X‐ray fluorescence (EDXRF) was used to determine the minor and trace element chemistry of 92 Early Jomon pottery sherds. The sherds came from four contemporary sites in the Kanto region and belong to either the Moroiso or Ukishima style of pottery. Principal components analysis (PCA) and discriminant analysis indicate that there are four major groups in the data set, which correspond to site location. Furthermore, for sites having both Moroiso and Ukishima pottery, the statistical tests indicate that both styles of pottery were made from the same or geochemically similar raw materials. This suggests that both styles were probably made at the same site, and indicates that if the different pottery styles are reflecting ethnic identity, then intermarriage between ethnic groups is occurring. Alternatively, the pottery styles could be reflecting some sort of social interaction between groups.     

CORRECTIONS FOR DRILL-BIT CONTAMINATION IN SAMPLING ANCIENT POTTERY FOR NEUTRON ACTIVATION ANALYSIS

The routine measurement of tungsten concentrations in pottery sampled with tungsten-carbide drill bits has enabled the measured concentrations of cobalt, tantalum, and lutetium to be corrected for drill-bit contamination. The corrected data, for cobalt at least, are sufficiently accurate that they regain their value as chemical indicators of pottery provenance.     

Geochemical provenience of 16th–19th century C.E. Asian ceramics from Torres Strait,northeast Australia

Existing insights into the history of southeast Asian contacts with northern Australia prior to British colonization in 1788 are limited to Macassan visitors and the trepang industry beginning in the early 18th century and perhaps 16th century. Neither historical nor archaeological evidence indicate extension of such contacts to Torres Strait of northeast Australia. To shed further light on this issue, a collection of 16 Asian ceramic sherds surface collected and excavated recently from the islands of Pulu and Mabuyag in Torres Strait were compared to a large database of Southeast and East Asian stoneware jars that are well characterised, elementally, typologically and chronologically. This comparison matched a number of sherds with two jar types with likely production origins in Thailand and southern China. While the surface collected sherds from Pulu sourced to Thailand date probably to the 19th century, the small glazed sherd from Mabuyag island is typical of a southern Chinese decorated jar type dating to c. 1500–1600 C.E. This Chinese sherd is the earliest known Asian artefact in Australia and parallels recent archaeological evidence on the antiquity of contacts between Macassan trepangers and Aboriginal Australians. It is unknown if the Chinese sherd came ashore to Mabuyag through direct contact with Asian traders or from a nearby shipwreck through salvage.