The Carving Technology of the Handle‐Shaped Artefacts from Yinxu (c.1300–1046 bc) in China

The handle‐shaped artefact is a special jade object of the Three Dynasties (c.2000–200 bc ) period. The manufacturing technology and function of the handle‐shaped artefacts are widely questioned. In this paper, two handle‐shaped artefacts from Yinxu (c.1300–1046 bc ) are tested by digital microscope, Raman spectrometer and scanning electron microscope. The results indicate that the handle‐shaped artefacts might be made in four steps, namely rough shape cutting, edge reforming, handle making and single‐side polishing. It also suggests that the handle‐shaped artefacts might be used as sacrificial offerings, but not as hairpins or handles.     

Middle Stone Age pièces esquillées from Sibudu Cave,South Africa: an initial micro-residue study

In this paper I present the results of a micro-residue study conducted on ten pièces esquillées (scaled pieces) from Sibudu Cave, South Africa. These artefacts are associated with the Howiesons Poort Industry (∼61.7 and ∼64.7 ka years ago at Sibudu), representing part of the later phase of the Middle Stone Age. Until now, it was unclear on what these pieces were used, and whether they were functional. Previous experimental use-wear work tentatively pointed towards bone processing. However, replication work on stone tool production technology suggests that pièces esquillées are merely the by/end-product of bipolar knapping. I used residue analysis on the Sibudu artefacts because this alternative method has the potential to identify if they were used, and if so, illuminate the specific materials the pieces were used on. Although the sample is small, all the pièces esquillées reveal a clear animal processing signal. There are some bone deposits on the utilised edges that may substantiate bone processing, or perhaps a bone hammer was used with them, but additional study, including Later Stone Age artefacts, is needed to assess the feasibility of these observations. It remains possible that the artefacts are core reduced pieces that were subsequently used as tools or simply knapped with a bone hammer.     

Middle Bronze Age Arsenical Copper Alloys in Southern Portugal

In the Iberian Peninsula, the copper metallurgy from the Chalcolithic to the Middle Bronze Age (MBA) was mostly characterized by low arsenic contents. A collection of 53 MBA artefacts from southern Portugal was analysed by micro‐EDXRF, optical microscopy, SEM–EDS and Vickers to investigate the metal composition and manufacture. No technological distinction was found between artefacts from domestic and funerary contexts, which were radiocarbon‐dated to 2000–1500 cal bc . The arsenic contents of almost 100 MBA artefacts from this region, including the above‐mentioned set, have a Gaussian distribution with a high average (3.9 wt% As). Possible explanations are discussed for this distinctive metallurgy at the south‐western end of the Iberian Peninsula.     

Assessing the macrofracture method for identifying Stone Age hunting weaponry

Macrofracture analysis is an experimentally derived method used as an initial step in investigating the hunting function of stone artefacts. Diagnostic impact fractures, which can only develop as a result of longitudinal impact, underpin this method. Macrofracture analysis recently gained favour in Middle Stone Age studies, supporting hypotheses for effective hunting during the late Pleistocene in southern Africa. However, the factors affecting diagnostic impact fracture formation and the interpretation of these fracture frequencies are not yet fully understood. This paper outlines a set of experiments designed to test macrofracture formation under human and cattle trampling and knapping conditions. The results show that: (a) macrofractures occur frequently when stone artefacts are trampled by cattle and humans and in knapping debris; (b) diagnostic impact fractures occur on some of the trampled flakes and knapping debris (≤3%), but significantly less often than in previous hunting experiments; (c) when they do occur, they are likely produced by longitudinal forces similar to those experienced during hunting; (d) considering artefact morphology is important during macrofracture analysis; and (e) macrofracture analysis is not a standalone method, but is most useful as part of a multi-analytical approach to functional analysis. These experiments help to establish a significant baseline diagnostic impact fracture frequency for the interpretation of archaeological macrofracture frequencies.     

Advancing the Analysis of Past Human/Plant Relationships: Methodological Improvements of Artefact Pollen Washes

The ‘pollen washes’ technique, based on the analysis of the pollen embedded in the porous surface of archaeological artefacts, is developed for investigating past plant usage and consumption and to characterize the functionality of artefacts related to plant processing, gathering and storage. The research presented results in relevant methodological improvements of this technique, which has never previously been applied on materials from European contexts. The improvements allow: (1) faster analysis of a broad series of artefacts or those with large use‐surface areas likely to retain more pollen; and (2) a more thorough, deeper and precise cleaning method, allowing the study of smoother artefacts. Finally, the recovery of Trifolium‐group pollen from a macro‐lithic tool from Xicotó rock shelter (Montsec ranges, Spain) demonstrates that the pollen washes technique can reveal new insights into both the use and consumption of wild and domestic plants by prehistoric societies, and the functionality of archaeological objects whose interpretation is still problematic.     

MULTIVARIATE MIXTURE OF NORMALS WITH UNKNOWN NUMBER OF COMPONENTS: AN APPLICATION TO CLUSTER NEOLITHIC CERAMICS FROM AEGEAN AND ASIA MINOR USING PORTABLE XRF*

Multivariate techniques and especially cluster analysis have been commonly used in archaeometry. Exploratory and model‐based techniques of clustering have been applied to geochemical (continuous) data of archaeological artefacts for provenance studies. Model‐based clustering techniques such as classification maximum likelihood and mixture maximum likelihood have been used to a lesser extent in this context and, although they seem to be suitable for such data, they either present practical difficulties—such as high dimensionality of the data—or their performance gives no evidence that they are superior to standard methods. In this paper standard statistical methods (hierarchical clustering, principal components analysis) and the recently developed model‐based multivariate mixture of normals with an unknown number of components, are applied and compared. The data set provides chemical compositions of 188 ceramic samples derived from the Aegean islands and surrounding areas.     

Clues to Stone Tool Function Re-examined: Comparing Starch Grain Frequencies on Used and Unused Obsidian Artefacts

The identification of plant residues observed on prehistoric stone artefacts has often been used to inform on tool function without adequate consideration of potential contamination due to post-depositional processes. The paper redresses this balance by proposing a methodology which combines use-wear and residue analyses with systematic testing of depositional context to distinguish residues formed during tool use from accidental contamination. A case study involving obsidian artefacts from an open site in Papua New Guinea is used to illustrate the new approach. Starch grains, a class of residue which has had little attention outside Australia, were chosen as the focus of study because of their abundance at this site. The frequency of starch grains extracted from residues on stone artefacts was compared with those in sediments adhering to and adjacent to the artefact. A use-wear study conducted as a blind test provided an independent measure of whether the artefacts had been used. The frequency of starch grains was shown to be significantly correlated with used artefacts and not correlated with unused artefacts or the sediments. The case study demonstrates the importance of testing for contamination and also illustrates the benefit of studying starch grains as a class of plant residue.     

Obsidian provenance analyses at Göytepe,Azerbaijan: Implications for understanding Neolithic socioeconomies in the southern Caucasus

This study presents a provenance analysis of the Neolithic obsidian assemblages from the early to mid‐sixth millennium bc settlement at Göytepe, Azerbaijan. The study is unique in that (1) it involves a complete, non‐selected obsidian assemblage (901 artefacts) from one particular area of the site; (2) the material is derived from a well‐stratified sequence of 10 securely radiocarbon‐dated architectural levels; and (3) the use of an extraordinarily wide range of sources (more than 20) was identified by provenance analysis using energy‐dispersive X‐ray fluorescence. The results reveal a previously unknown diachronic change in obsidian use in the region, suggesting the occurrence of significant socioeconomic changes during the Late Neolithic of the southern Caucasus.     

AN INTERIM REPORT OF THE STAR CARR MICROWEAR STUDY

Summary. This paper presents some preliminary observations based on the microwear analysis of 173 artefacts from the mesolithic site of Star Carr, near Scarborough, Yorkshire. One hundred discrete and utilized edges were identified by the presence of various microwear traces on 79 of the artefacts belonging to the following general types: scrapers, edge-damaged or marginally retouched blades and flakes, bilaterally backed blades (awls), burins, backed blades, axe resharpening flakes, denticulated or truncated blades and flakes, microliths, and cores. The microwear traces identified on the tools indicates that they were used in a variety of ways in the processing of hide, bone, wood, antler and meat. A comparison of wear-traces and tool shape has shown that there are morphological differences between scrapers used on hide and those used on bone, and also, that edge-damaged or marginally retouched blades were selected for use on the basis of their cross-sectional configuration.     

Exponential Decline in the Dispersal of Stone Artefacts in Roman Britain: Further Expressions of Trade

Several industries that exploited stone are known to have sprung up in Iron Age–Roman and Roman Britain. They include the fashioning of rotary querns from the Upper Old Red Sandstone of the Forest of Dean and the Lower Cretaceous Hythe Beds (Lodsworth rock) of West Sussex, the production of whetstones from sandstones in the Weald Clay Formation of the north‐west Weald, and the manufacture of a wide range of products from the Upper Jurassic Purbeck Marble of south‐east Dorset. The dispersal of goods from these sources is found to exhibit a similar exponential decline with distance to that previously demonstrated for prehistoric stone artefacts and Romano‐British ceramics. Evidently, interactions at settlements led to the retention of a roughly constant proportion of the goods brought there.     

Ochre fingerprints: Distinguishing among Malawian mineral pigment sources with Homogenized Ochre Chip LA–ICPMS

In this study, we compared the effectiveness of instrumental neutron activation analysis (INAA) of bulk ochre to laser ablation‐inductively coupled plasma mass spectrometry of homogenized ochre chips (HOC LA–ICPMS) at distinguishing among three ochre sources in northern Malawi. Both techniques upheld the Provenance Postulate; however, HOC LA–ICPMS required less sample material than INAA and facilitated fast, inexpensive replicate observations that allowed for more robust statistical analysis. Our results indicated that HOC LA–ICPMS is a maturing technique that will be a valuable option for analysing artefacts that require minimally destructive sampling but are too large to fit into the laser cell for direct ablation. With regard to the statistical procedures used, stepwise canonical discriminant analysis was demonstrated to be a highly effective method for distinguishing among ochre sources, even in the presence of significant intra‐source and intra‐sample heterogeneity. Continued development of the HOC sample preparation technique will expand the range of archaeological ochre artefacts that can be included in provenance studies and prevent bias towards artefacts of convenient‐to‐analyse dimensions.     

The World's Oldest Stone Artefacts from Gona, Ethiopia: Their Implications for Understanding Stone Technology and Patterns of Human Evolution Between 2·6–1·5 Million Years Ago

The systematic archaeological and geological survey and excavations at Gona between 1992–1994 led to the discovery of well-flaked stone artefacts which are currently the oldest known from anywhere in the world. More than 3000 surface and excavated artefacts were recovered at 15 localities documented east and west of the Kada Gona river. Based on radioisotopic dating (⁴⁰Ar/³⁹Ar) and magnetostratigraphy, the artefacts are dated between 2·6–2·5 million years ago (Ma). EG10 and EG12 from East Gona are the most informative with the highest density, providing the best opportunity for characterizing the oldest assemblages and for understanding the stone working capability of the earliest tool makers. Slightly younger artefact occurrences dated to 2·4–2·3 Ma are known from Hadar and Omo in Ethiopia, and from Lokalalei in Kenya. Cut-marked bones dated to 2·5 Ma from Bouri in Ethiopia are now providing important clues on the function of these artefacts. In addition, Australopithecus garhi known from contemporary deposits at Bouri may be the best candidate responsible for the oldest artefacts. Surprisingly, the makers of the Gona artefacts had a sophisticated understanding of stone fracture mechanics and control similar to what is observed for Oldowan assemblages dated between 2·0–1·5 Ma. This observation was corroborated by the recent archaeological discoveries made at Lokalalei. Because of the similarities seen in the techniques of artefact manufacture during the Late Pliocene–Early Pleistocene, it is argued here that the stone assemblages dated between 2·6–1·5 Ma group into the Oldowan Industry. The similarity and simplicity of the artefacts from this time interval suggests a technological stasis in the Oldowan.     

THE TECHNOLOGICAL AND TYPOLOGICAL BEHAVIOUR OF A NEANDERTHAL GROUP FROM EL SIDRÓN CAVE (ASTURIAS,SPAIN)

This paper presents the first detailed analysis of the lithic industry from El Sidrón Cave. Previously we have published other works concerning Anthropology and Palaeogenetics. The lithic assemblage contains 415 artefacts coming from both unofficial and official excavations and is largely flake‐based. The raw material derives from the immediate cave environment, and is mostly chert, with quartzite in a lesser proportion. To date, 67 artefacts have been refitted, including some tools and cores. The spatial distribution of the refitted lithic artefacts confirms, on the one hand, the unity of the assemblage and, on the other, its secondary context.     

Prehistoric Whale Bone Technology in Southern New Zealand

Whale bone was used by Māori throughout New Zealand prehistory as an industrial resource for the manufacture of a range of artefacts. However, the selection of bone and the methods used to process it are poorly understood. This paper details the analysis of a southern right whale (Eubalaena australis) bone working floor that was excavated from a fifteenth‐century coastal fishing camp at Kahukura, on the southeast coast of New Zealand. The whale bone working floor assemblage, comprising a large quantity of debitage fragments, was used to reconstruct reduction methods and to determine the products being made at the site. Rib bones were the main element being worked, and were reduced longitudinally using a chipping technique. The intensive bone working assemblage at Kahukura represents the by‐products from primary processing. This stage focused on reducing the bones into workable portions so that they could be easily transported to another location, where they were likely further reduced into artefacts. Copyright © 2015 John Wiley & Sons, Ltd.     

First Insights into the Technique Used for Heat Treatment of Chert at the Solutrean Site of Laugerie‐Haute,France

The earliest evidence of flint and chert heat treatment was found in the ~21.5–17 ka old European Solutrean culture. The appearance of pyrotechnology as part of the production of stone tools has important implications for our understanding of Upper Palaeolithic technological evolution and the specific adaptations during the last glacial maximum in Europe. However, the techniques and procedures used to heat‐treat rocks during the Solutrean remain poorly understood. No direct archaeological evidence has so far been found and the most promising approach is to understand these techniques by determining the parameters with which flint and chert were heated at that time. In this study, we investigate the heating temperature of 44 heat‐treated laurel‐leaf points from Laugerie‐Haute, using a non‐destructive technique based on infrared spectroscopy. Our results document that most of the artefacts were heated to a narrow interval of temperatures between 250 °C and 300 °C. This indicates a standardized technique that allowed to created similar conditions during successive heating cycles. The implications of these results for our understanding of the technical complexity during the Solutrean must be discussed in the light of different heating techniques used at different places and periods.     

The Use of Mineralogy to Identify Sources of Soapstone Artefacts: an Example from Soapstone Ridge,Georgia (USA)

The late Archaic Soapstone Ridge quarries, near Atlanta, Georgia, are the largest sources of archaeological soapstone in the south‐eastern USA. Ten soapstone artefacts from the coastal plain, over 200 km south of Soapstone Ridge (SSR), were used in an attempt to relate their mineralogy to that of the Soapstone Ridge quarries and to investigate the utility of mineralogy in the sourcing of soapstone. There is an overall similarity in the abundance of the major soapstone minerals, talc, chlorite and amphiboles in the artefacts and the SSR soapstone. Differences in the variety of amphibole (tremolite/actinolite, magnesiohornblende and magnesiocumingtonite/anthophyllite) and FeTi oxides (magnetite and ilmenite) eliminate SSR as a source for some of the artefacts. The compositions of chlorite (Cr), magnesiohornblende (Si, Al) and Fe oxides (Cr, Mn) in other artefacts are not consistent with a Soapstone Ridge source. The talc compositions are identical in the artefacts and the SSR soapstone. The mineral assemblage and compositions of two artefacts are consistent with a Soapstone Ridge source. Despite an overall similarity in the modal mineralogy of the artefacts and Soapstone Ridge quarries, there is enough diversity to distinguish between artefacts from Soapstone Ridge or some other source. Mineralogy is a useful tool for the evaluation of soapstone sources.     

DETECTING AND QUANTIFYING HEAT TREATMENT OF FLINT AND OTHER SILICA ROCKS: A NEW NON‐DESTRUCTIVE METHOD APPLIED TO HEAT‐TREATED FLINT FROM THE NEOLITHIC CHASSEY CULTURE,SOUTHERN FRANCE

Heat treatment of lithic raw material is known from the Middle Stone Age to the Neolithic. These findings require archaeometric techniques and methods for detecting the heat‐induced effects within lithic artefacts. However, the existing methods are often cost‐intensive and time‐consuming, and most of them are destructive. Here, we present a new method using the infrared spectroscopic measurement of the strength of H‐bonds formed between surface silanole groups (SiOH) and H₂O molecules held in open pores of the samples. The reduction of H‐bond strength in chalcedony is shown to be strongly correlated with the loss of open pores induced by heat treatment. Hence, the method is based on measuring one of the transformations aimed for by the instigators of the heat treatment: the reduction of porosity that modifies the rock's mechanical properties. A first application to heat‐treated material from the Neolithic Chassey culture (southern France) shows that flint was heated to temperatures between 200°C and 250°C in this period. This has important implications for the study of the procedures used and the heating environments. Our new method is non‐destructive, rapid, cost‐effective and allows for detection of the used annealing temperatures.     

CONSTRUCTING CARIBBEAN CHRONOLOGIES: COMPARATIVE RADIOCARBON DATING OF SHELL AND WOOD ARTEFACTS FROM PRE‐COLUMBIAN SITES IN CUBA

The lack of robust chronological frameworks for pre‐Columbian archaeology in the Caribbean limits the interpretive potential of ongoing studies of inter‐site and inter‐island interaction. This paper reviews the dating of 28 wood and shell artefacts from sites in northern Cuba in an attempt to date pre‐Columbian activity in the region and develop dating methodologies for the study of pre‐Columbian interaction in the Caribbean. This research compares dates from wood and shell artefacts from the waterlogged site of Los Buchillones in north‐central Cuba with dates from shell artefacts from sites on eight islands in the Sabana–Camaguey archipelago in the Bahama Channel. In addition to providing a chronological framework based on absolute dates for pre‐Columbian activity in northern Cuba, this paper also considers the methodological issues of using shell for dating pre‐Columbian activity in the Caribbean.     

DETECTION OF ANCIENT MARBLE FORGERY: TECHNIQUES AND LIMITATIONS*

Since 1960, scientific results have replaced aesthetic judgements in marble authentication studies and the technology to perform analytical tests on micro‐samples has developed rapidly. However, no single method can be used to determine the authenticity of a piece of marble. A ‘detective‐like’ investigation is usually adopted by using optical microscopy, ultraviolet‐induced fluorescence, provenance determination techniques and mineralogical, chemical and morphological analyses of the patina. A newly proposed thermoluminescence methodology calculates the ‘burial age’ of recently excavated objects or distinguishes artefacts exposed to sunlight since antiquity from those exposed recently. The technique shows a lot of potential; however, much work remains to be done.     

Complex raw materials and the supply system: Mineralogical and geochemical study of the jade artefacts of the Longshan Culture (2400–2000 bce) from Sujiacun site in coastal Shandong,China

X‐ray fluorescence (XRF), X‐ray diffraction (XRD) and Raman spectroscopy were employed to analyse the chemical compositions and phase structures of nine pieces of jade artefacts unearthed from Sujiacun, a Longshan Culture (2400–2000 bce ) site in coastal Shandong, eastern China. The results of the analyses indicated these samples were primarily made from multiple raw mineral materials, including antigorite, actinolite, clinochlore, turquoise and muscovite. No nephrite was recovered from the Sujiacun site. This is strikingly different from other top‐ranking settlements of Longshan Culture, such as Dantu, Liangchengzhen and Xizhufeng, in which nephrite was the main material of jade artefacts. This may reflect the distinctions in the supply system of jade raw materials among different rankings of Longshan period sites. In addition, laser ablation inductively coupled plasma mass spectrometry (LA‐ICP‐MS) was used to analyse the composition of the rare earth elements of serpentine jade. These preliminary results were compared with published data on the composition of serpentine jade and it was found that the Sujiacun serpentine jade artefacts were likely sourced from the Taishan jade deposit.