METHODS OF ENGRAVING MESOPOTAMIAN CYLINDER SEALS: EXPERIMENTAL CONFIRMATION*

Previous observations of the intaglios on quartz cylinder seals from Western Asia suggested that they had been engraved by one or more of four basic techniques, that is, micro-chipping, filing, drilling and wheel-cutting. In this paper we test our earlier observations and interpretations experimentally. Examination and comparison of experimentally engraved features with the seal intaglios was made directly with a binocular microscope and also by examination of impressions with a scanning electron microscope. Successful replication was achieved using tools of flint, chalcedony, copper, bronze and iron together with quartz and emery abrasives.     

Some Evidence for Seasonality amongst Later Stone Age Hunter-gatherers in Southern Africa

Abstract

The Later Stone Age (LSA) period in Southern Africa is characterised by a succession of cultural traditions. The LSA hunter-gatherer populations were ancestral to the present-day San. They moved around in small bands, within a semi-fixed territory visiting open air and shelter sites to coincide with available resources.

The hunter-gatherers filled every niche in the environment, including the high mountains, deserts and semi-deserts, bush savanna and grass lands. They were well aware of the food sources available in their territories during the course of a year and utilized these opportunities. As winters in southern Africa are relatively mild, and most regions have foods available throughout the year, seasonality is difficult to demonstrate.

In only a few instances there is some evidence for seasonal use or seasonality. Age profiles of seals at Elands Bay Cave suggest short occupation periods during late winter and early spring. In the high mountains of South Africa and Lesotho, where winters are cold and frost and snow common, the faunal and floral remains suggest occupation during late spring, summer and early autumn. Abbot's Cave in the semi-arid central Karoo was used as a hunting lodge during September, relating to the lambing season and migratory behaviour of springbok (Antidorcas marsupialis).     

Advances in Polychrome Ceramics in the Islamic World of the 12th Century AD

As part of a multidisciplinary programme of research on Islamic glazed pottery, the development of polychrome decoration during the 12th century AD has been investigated by examining polished sections through glazed pottery in an analytical scanning electron microscope. The two main decorative techniques used were underglaze and overglaze painting. The results suggest that true underglaze decoration, involving the application of pigment without any associated slip, was first developed in Syria, from where it spread to Iran, on to China and ultimately across wide areas of the world. In contrast, the overglaze technique used on mina'i ware was both very short‐lived and confined to Iran. The analytical results suggest that the probable explanation for this was the technical problems associated with maturing the overglaze paint and the consequent risk of unsatisfactory products.     

LUMINESCENCE DATING OF POTTERY FROM LATER PREHISTORIC BRITAIN*

Dating of later prehistoric settlements relies heavily on potter; typologies in England and yet there has been little scientific dating in order to verify these typologies. In this work, luminescence dating techniques were applied directly to the pottery which forms the typological framework. Excellent agreement was obtained between the luminescence ages, and archaeological age ranges for known‐age pottery sherds with diagnostic form and surface decoration. A lower correlation, however, was found in several regions between the luminescence ages for undecorated body sherds and the archaeological assessment which was necessarily based solely on fabric, suggesting the need for reassessment of these fabric chronologies.     

MICROSCOPIC IDENTIFICATION AND SOURCING OF ANCIENT EGYPTIAN PLANT FIBRES USING LONGITUDINAL THIN SECTIONING*

Plant fibres and the artefacts constructed from them often remain overlooked in the archaeological record because of their poor survival and the problems related to the precise identification of the species to which the fibres belong. The goal of this study was to design a simple and accurate method of identifying archaeological plant fibre sources. Twenty‐two fibre samples from two sets of ancient Egyptian botanical artefacts were examined under both a stereomicroscope and a compound microscope, and compared to a large reference collection and to previously published research. By examining longitudinal thin sections of the ancient plant specimens, we identified plant fibres from the following species: Hyphaene thebeica, Cyperus papyrus, Desmostachya bipinnata, Imperata cylindrica, Phragmites australis and Linum usitatissimum. Our identification of these plant fibres reveals essential information about the materials used for producing ropes, baskets, sandals, mats and fabric. The results of this study demonstrate the value of longitudinal thin sectioning and light microscopy as a major means of identifying the source material of botanical artefacts, and advance our knowledge of ancient Egyptian plant exploitation as well as the associated technologies involved in constructing these types of artefacts.     

LEAD ISOTOPIC ANALYSIS FOR THE IDENTIFICATION OF LATE BRONZE AGE POTTERY FROM HALA SULTAN TEKKE (CYPRUS)

Lead isotopic compositions were measured for 65 sherds from five pottery wares (Plain White, Coarse, Canaanite, White Slip and Base‐ring) excavated from the Late Bronze Age site of Hala Sultan Tekke (Cyprus). The elemental composition and isotopic signature of the sherds were compared with those of 65 clay samples collected in south‐east Cyprus, mainly in the surroundings (<20 km) of Hala Sultan Tekke. This work shows the effectiveness of using lead isotopic analysis in provenance studies, along with other analytical techniques, such as X‐ray diffraction (XRD) and a scanning electron microscope (SEM) equipped with an energy dispersive X‐ray detection (EDX) facility, to identify the composition of pottery wares and the clay sources used for pottery ware production.     

Unusual Use of Freshwater Mussel (Unio sp.) Shells during the Early Bronze Age at Tell es-Sa'idiyeh,Jordan

Abstract

Amongst the marine, land and freshwater molluscs from the Early Bronze Age at Tell es-Sa'idiyeh, Jordan, is a group of freshwater mussels which shows evidence of distinctive working. These Unio bivalves have been examined using the scanning electron microscope in order to characterise the patterns of modification. Despite the fact that their precise function remains enigmatic, the range of possibilities has been better understood as a result.     

Damage caused by insects during the mummification process: an experimental study

The process of mummification had been known since the Fourth Dynasty of the Old Kingdom (ca. 2600 bc) and continued to develop throughout ancient Egyptian history. Although mummification protected the body from decay, especially by microbes, some mummification techniques left the body susceptible to insect attack. Certain types of insects have been detected in the mummies. In scholarly publications, most authors have dealt with microorganisms, while few have concerned themselves in depth with the effect of insects on the mummies. This study aims to discuss the significance of insects and the changes they affected to the mummies during embalming. To achieve this goal, experiments were carried out replicating various mummification techniques using albino Wistar rats. Analysis and investigative techniques used included visual observation, Fourier transform infrared spectroscopy, investigation of the surface morphology by a scanning electron microscope, and color change by a spectrophotometer. The following insects could be identified as being present during the second and third processes of mummification: Dermestes maculatus, Necrobia rufipes, Saprinus gilvicornis, Chrysomya albiceps, Wohlfahrtia magnifica, and Attagenus fasciatus. In addition, the majority of our findings confirmed that the degradation by insects increased with the second and third methods of mummification. Finally, the experimental study conducted using the mummification techniques of the New Kingdom (ca. 1570–1070 bc) indicated that they were more resistant to insect attack than the other types.     

INSIGHTS INTO NORTH MESOPOTAMIAN ‘METALLIC WARE’*

With the aim of shedding new light on the still poorly understood North Mesopotamian metallic ware, ceramic and soil samples from Tell Beydar (northeastern Syria, third millennium bc ) were investigated using a range of analytical techniques, including optical microscopy, SR–XRD and SEM–EDX. The objective of this work was to differentiate calcareous metallic ware from non‐calcareous ware without the aid of chemical analyses and to find further validation of the existing hypothesis that the former group is an imitation of the latter. A third group of metallic wares from Tell Beydar is believed to be of non‐local, still regional origin.     

LUMINESCENCE DATING OF SEDIMENTS—THE DETECTION OF HIGH EQUIVALENT DOSE GRAINS USING AN IMAGING PHOTON DETECTOR*

In this paper we describe quantitative measurements on the thermoluminescence of many single grains, made with an imaging photon detector. In several of the sediments examined a few bright grains were found which had a high equivalent dose (ED). Physical measurements made on these grains using binocular microscopy and analytical scanning microscopy enabled several possible explanations for the causes of the high ED grains to be rejected. Insufficient bleaching at deposition or the intrusion of grains from an older sediment were identified as the most probable explanation for these grains.     

GLASS CORROSION ACROSS THE ALPS: A SURFACE STUDY OF CHEMICAL CORROSION OF GLASSES FOUND IN MARINE AND GROUND ENVIRONMENTS*

Ancient glasses deriving from differing environments (marine and ground) and areas (Mediterranean and Continental) have been investigated to understand their weathering processes. Although the glass technologies, developed in various ways, and the differing compositions of the glasses from the two areas, have generated differing durabilities, the weathering features of both typologies of glass are identical. Therefore, the corrosion phenomena are due to the action of water, and they are not related to the sample microclimate. Data have been collected using optical microscopy, RGA and surface analysis techniques: XPS, ESEM and SIMS.     

How the Romans got themselves into hot water: temperatures and fuel types used in firing a hypocaust

Abstract

The remains of hypocausts are noted as being widespread throughout the Roman Empire but, whereas the structure of hypocaust systems has been widely documented, primary knowledge of operating temperatures is limited. The petrographic technique of reflectance microscopy is used here to quantify cell wall reflectance values for charcoals from the hypocaust furnace of a bath suite forming part of small Romano-British villa complex at Groundwell Ridge near Swindon (Wiltshire, UK). The technique utilises material of archaeological origin to infer operating temperatures of the hypocaust furnace using established calibrations. The charcoals recovered from the furnace were identified as being predominantly Quercus (Oak) with some Populus/Salix (poplar/willow). Mean random reflectance of the samples indicated furnace-operating temperatures of 330–410°C. These temperatures fall below that of charcoal fuel production and hence suggest that it was wood that was used to fuel the hypocaust at Groundwell Ridge and not charcoal. Knowledge of the operating temperature of the furnace is a starting point in further calculations to understand, using primary evidence, the operating temperatures throughout the hypocaust system.     

BYZANTINE OPAQUE RED GLASS TESSERAE FROM BEIT SHEAN,ISRAEL*

This paper presents the results of analysis of Byzantine opaque red glass tesserae derived from three separate locations in the ancient city of Beit Shean, Israel. Investigation proceeded using reflective light microscopy, energy dispersive X‐ray fluorescence and energy dispersive scanning electron microscopy. The glass matrix of the tesserae was found to be heterogeneous, with many inclusions. Similarities and differences between tesserae from the two mosaics are examined and discussed. Implications for locale of manufacture and production techniques are considered. Comparisons between the three locations led to conclusions about the use of the tunnel as a storage site and the implications of this for future research on mosaics.     

Probable Fibres from Hemp (Cannabis sativa L.) in Bronze Age Scotland

Abstract

Diameter measurements of bast fibres from cloth and string with a hoard of bronze age metalwork found in St Andrews, were different from those of flax (Linum usitatissimum L.) but comparable with those of hemp (Cannabis sativa L.) leading to the suggestion that hemp was used as a textile fibre in Britain much earlier than has been thought.     

FTIR AND SOLID‐STATE 13C CP/MAS NMR SPECTROSCOPY OF CHARRED AND NON‐CHARRED SOLID ORGANIC RESIDUES PRESERVED IN ROMAN IRON AGE VESSELS FROM THE NETHERLANDS*

In this study, solid‐state ¹³C magnetic resonance spectroscopy using cross‐polarization combined with high‐powered proton decoupling and magic‐angle sample spinning and Fourier transform infrared spectroscopy using a diamond anvil cell, are employed to give information about the organic functional groups present in charred and non‐charred solid organic residues and to give an insight into the degree of condensation of the chars. Residues were preserved in ceramic vessels recovered from the indigenous settlement of Uitgeest–Groot Dorregeest, dating back to the Roman period. In addition, the application of these solid‐state techniques is used for verification of earlier results obtained in analytical pyrolysis studies and to clarify the relationship between the already thermally degraded charred residues and the controlled heating fragmentation taking place during analytical pyrolysis and direct temperature‐resolved mass spectrometry.     

CONIFEROUS WOOD PULP IN TRADITIONAL KOREAN PAPER BETWEEN THE 15TH AND 18TH CENTURIES ad*

One hundred and sixty‐nine fibre samples from books in the Korean collection and 68 samples from books in the Japanese collection at the British Library were analysed. A further 15 samples of Korean paper from a private collection were also examined. The analysis confirmed that most of the papers contained mulberry species (Moraceae family) as the main papermaking material, and other materials, such as hemp, rice straw and reed, which have been commonly known as supplements to traditional Korean papermaking. However, 15 Korean papers and one Japanese paper dating between ad 1498 and 1798 appeared to include coniferous wood fibres. This substantial find supports a previous single find of a coniferous wood fibre in Korean paper. The dates of most of these papers containing wood fibres precede the use of wood pulps in European paper.     

CHEMICAL AND MINERALOGICAL ANALYSES OF GALLO-ROMAN WALL PAINTING FROM DIETIKON,SWITZERLAND

Around 90 samples of Roman wall painting dating from the first to the third century AD were analysed using different analytical techniques: X-ray diffraction, X-ray fluorescence, infrared spectrometry, scanning electron microscopy, energy dispersive spectrometry, optical microscopy and physico-chemical tests. The identified pigments are: ash, calcite, carbon black, celadonite, cinnabar, Egyptian Blue, glauconite, goethite, hematite and red lead. Pigment mixtures were used to get other colours such as brown, pink or purple. Three types of plaster were used: a first, and most dominant, with river sand, a second with crushed tile for damp places and a third, to which cinnabar was exclusively applied, was prepared with crushed calcite crystals.     

PALAEOCLIMATIC IDENTIFICATION BASED ON AN ISOTOPE STUDY OF TRAVERTINE FROM THE COPPER AGE SITE AT LOS MILLARES,SOUTH-EASTERN SPAIN*

Remains of an aqueduct from the Copper Age settlement of Los Millares have been studied. The isotope results (—7‰ < δ¹⁸O — 5.3‰) show that the aqueduct was used to transport fresh water at room temperature. The results are inconsistent with the aqueduct being used for hot water transport or as a container for water exposed to evaporation processes. Both isotopic and mineralogical results were useful in identifying the origin and use of building materials and also in determining climatic conditions during the time of the settlement occupation.