AN ARCHAEOMAGNETIC STUDY OF POTTERY KILNS FROM BRÜHL-PINGSDORF (GERMANY)*

Four pottery kilns from Brühl-Pingsdorf (Germany) were dated by comparing their characteristic remanent magnetization with a curve of the palaeo-secular variation of the geomagnetic field. Archaeomagnetic results suggest last heating events between AD 775 and 1020. The archaeological evidence generally supports the relative temporal succession and the duration of use, but indicates that the kilns are about 150 years younger on average. Hence, a systematic offset between these independently developed chronologies must be considered. Rock magnetic parameters display radial variations through the kiln walls. These variations are controlled by the maximum temperature the rock was exposed to. These parameters were used to identify specimen which acquired a thermoremanent magnetization.     

MAGNETIZATION DATING AT A MEDIEVAL MONASTERY (TUPHOLME,LINCOLNSHIRE)*

Tupholme Abbey, founded by c. 1166, was constructed of limestone masonry, some of which was reoriented at several times through its history. The limestone progressively acquired a ‘soft’, time-dependent magnetization in the earth's magnetic field—viscous remanent mag-netization (VRM)—that acts like a clock. Although VRM is normally disregarded by geologists because of its ephemeral nature, this remanence is acquired and persists over time-scales that are useful to archaeologists. Successive VRMs were initiated, at different ages of stabilization of the masonry, thus yielding a chronometric curve that allows us to determine, at least relatively, when masonry was installed.     

ARCHAEOMAGNETIC FIELD INTENSITY DURING THE ROMAN PERIOD AT SIWA AND BAHRYN OASIS,EGYPT: IMPLICATIONS FOR THE FIDELITY OF EGYPTIAN ARCHAEOMAGNETIC DATA

A preliminary survey was conducted in Siwa and Bahryn Oasis to test the possible influence of various rock magnetic and experimental constraints on the fidelity of the Egyptian archaeomagnetic field record. Five potsherds from the Roman era, which lasted from 1981 bp to 1555 bp , have been investigated. Archaeologists dated the localities to ～1620 bp . Ten ceramic specimens, two of each potsherd, were subjected to archaeointensity determination, including tests for domain state effects, magnetic anisotropy and magnetic cooling rate dependency. Six successful archaeointensity determinations are obtained from three individual cooling units, revealing an average field value of 37.7 μT for the late Roman period in Siwa and Bahryn oasis, which is comparable to the present‐day field strength. The error propagation of the individual uncertainties related to all applied experimental techniques results in a maximum uncertainty estimate of 4.4 μT. The obtained field value is significantly smaller than early results and slightly smaller than some more recent determinations of the field intensity in Egypt. The difference is attributed to a combined effect of alteration, magnetic anisotropy and magnetic cooling rate dependencies. Along with other high‐quality data from the south‐east Mediterranean, our data suggest a field intensity minimum during the Egyptian Roman era.     

POST‐MEDIEVAL CRUCIBLE PRODUCTION AND DISTRIBUTION: A STUDY OF MATERIALS AND MATERIALITIES*

This paper is concerned with the manufacture and trade of post‐medieval crucibles (14th–19th centuries). The analytical study of crucibles from different contexts in Europe and America employed optical microscopy and SEM–EDS, coupled with archaeological and historical data. We identified two major producers of crucibles, both of them in Central Europe, whose products appear widely distributed internationally. The analytical data allow an explanation of the technical reasons behind their superior reputation, as both crucible types shared comparable material properties, such as thermal, chemical and mechanical stability. Conversely, the two crucible types were radically different in their manufacture and appearance. We argue that, besides technical considerations, sensorial aspects such as texture and colour may have played an important role in the perception and choice of materials.     

ON THE AGE AND CONTENT OF JAR‐35—A SEALED AND INTACT STORAGE JAR FOUND ON THE SOUTHERN PLATEAU OF QUMRAN*

An intact and sealed storage jar known as Jar‐35 was found in 2004, south of the Qumran settlement. A previous study identified tartrate in the deposit of the jar, indicating the possible past presence of wine ( Buti et al. 2006 ). However, we cannot confirm this finding. Using liquid and gas chromatography with mass spectrometric detection, no trace of tartaric acid or salts thereof could be detected in our samples. We show that the major component of the deposit is gypsum. No other organic compounds were identified with the methods that we have applied. Both radiocarbon dating of charcoal in the deposit and thermoluminescence dating of the ceramic jar show that it dates to the main period of habitation at Qumran (c. 100 bc to ad 70).     

THE CHEMICAL COMPOSITION OF BLUE PIGMENT ON CHINESE BLUE‐AND‐WHITE PORCELAIN OF THE YUAN AND MING DYNASTIES (ad 1271–1644)*

The chemical compositions of the glazes and pigments of 39 blue‐and‐white porcelains of Ming Dynasty date and three of Yuan date were examined by SR‐XRF. Both the analysis of the Fe/Mn ratio in the light blue areas of the glaze and a comparison of the Fe/Mn values between light blue, dark blue and clear glaze areas reveals that the samples can be divided into three groups. The results indicate that there are two significant changes of provenance of blue pigment during the Ming Dynasty and that some kinds of pigment were most probably imported from the Middle East. Considering literature records and other scholars’ studies, an outline picture of the pigment used on Chinese blue‐and‐white porcelain produced in Jingdezhen in the Yuan and Ming Dynasties is presented.     

GLAZED CERAMIC MANUFACTURING IN SOUTHERN TUSCANY (ITALY): EVIDENCE OF TECHNOLOGICAL CONTINUITY THROUGHOUT THE MEDIEVAL PERIOD (10TH–14TH CENTURIES)*

Archaeometric investigation allowed the characterization of two important classes of ceramics: ‘vetrina sparsa’ and ‘invetriata grezza’. Their archaeological peculiarity makes them particularly suited for tracing the evolution of glaze manufacturing in southern Tuscany throughout the medieval period (10th–14th centuries). These ceramics were found in different sites of historical importance, and also from a mining perspective. Local copper, lead, zinc and iron mineralizations supported the growth of several settlements in the vicinity of the mines. The many castles and different archaeological finds (ceramics, glazed ceramic, slag etc.) attest to the intense mineral exploitation of the area from at least the first millennium bc up to the modern period. In light of these geological and archaeological characteristics, archaeometric investigation was intended to provide insight into ancient technical knowledge of ceramic glazing and to determine the source area for raw materials in the medieval period (10th–14th centuries). Ceramic bodies were analysed through OM, XRDp, SEM–EDS and XRF, while coatings were investigated through SEM–EDS. Mineralogical, petrographic and chemical analyses revealed slightly different preparation and firing processes for the two classes of ceramics. These data suggest the continuity through the centuries of the ‘vetrina sparsa’ and ‘invetriata grezza’ production technology. The mineralogical phases, such as monazite, xenotime, zircon, barite, Ti oxide, ilmenite, titanite, tourmaline and ilvaite, and the lithic (intrusive and volcanic) fragments detected within the ceramic bodies suggest a source area in the vicinity of the Campiglia mining district. Lastly, the presence of Cu–Zn–Pb (Ag) and Fe sulphide mineralizations (materials used to produce glaze) in the area supports the hypothesis of local manufacture.     

THE PETROGRAPHY AND CHEMISTRY OF THIN‐WALLED WARE FROM AN HELLENISTIC– ROMAN SITE AT SEGESTA (SICILY)*

Samples of Roman thin‐walled ware from Segesta (northwestern Sicily), dating back to the early Imperial period, were studied by optical microscopy (OM) and Neutron Activation Analysis (NAA). Up to now, this class of Roman fine tableware has only occasionally been evaluated archaeometrically. Nevertheless, numerous production centres are believed to have been simultaneously active in the western Mediterranean area. Petrographic and chemical data seem to be in agreement with the archaeological hypothesis of local manufacture in Segesta for most of the analysed samples, through a comparison with kiln wasters and local raw materials. The effectiveness of thin‐section petrography for determining the provenance of such a tiny tempered class of pottery and the integrated use of two different grouping procedures (petrography and chemistry) were also tested.     

ASSESSING WHAT LIES BENEATH THE SPATIAL DISTRIBUTION OF A ZOOARCHAEOLOGICAL RECORD: THE USE OF GIS AND SPATIAL CORRELATIONS AT EL MIRÓN CAVE (SPAIN)*

Geographical Information Systems (GIS) are being incorporated into archaeology as a technique to improve the understanding of spatial organization and the relationships among finds within specific areas. Although their use as a basic tool in predicting the location of archaeological sites or in assessing the extent of their catchment areas is relatively common, in general, they have less often been applied to the study of the spatial distribution of archaeological remains within individual deposits, and in particular to faunal assemblages. Despite this, they can prove essential to understanding dispersion and grouping patterns within deposits fully, and, together with various correlation analytical techniques, they provide valuable information about the economic organization of settlements and inhabitant lifeways. To demonstrate the potential of this methodology, a zooarchaeological GIS has been prepared for the Middle and Late Magdalenian and Azilian layers in El Mirón Cave (eastern Cantabria, Spain), and the spatial distribution patterns of various attributes of the archaeological record have been analysed. Significant conclusions in terms of type and duration of human occupation have been drawn.     

ARCHAEOLOGICAL RESEARCH AT THE INSTITUTE OF NUCLEAR TECHNIQUES,BUDAPEST UNIVERSITY OF TECHNOLOGY AND ECONOMICS: SCHOLARLY ACHIEVEMENTS OF A PROSPEROUS LONG‐TERM COLLABORATION

The laboratory is part of a university institute with a nuclear reactor on the premises. NAA of archaeological materials started in the early 1980s, and has found continuous interest since then. Site‐specific characteristics of the NAA procedure are the long irradiation and counting times, due to the relatively low neutron flux, the single comparator method of standardization and the use of reference materials for quality control. The main research interest focuses on provenance studies of potteries; 90% of the analysed samples are ceramic materials. Most of the projects concentrate on the investigation of pottery finds from Roman Pannonia, and from different archaeological sites in Israel. The Qumran pottery project is presented as a typical example.     

A MULTI‐ANALYTICAL APPROACH FOR THE CHARACTERIZATION OF COMMODITIES IN A CERAMIC JAR FROM ANTINOE (EGYPT)*

This paper describes a multi‐analytical chemical study performed on the original, almost totally conserved, content of a small ceramic jar from the Antinoe archaeological site (fifth to seventh centuries ad, Roman Egypt) and now belonging to the archaeological collection of the Istituto Papirologico ‘Girolamo Vitelli’ (Florence, Italy). Scanning electron microscopy with an energy‐dispersive X‐ray spectrometer (SEM–EDX), Fourier transformed infrared spectroscopy (FTIR) and X‐ray diffraction (XRD) were all used to characterize the inorganic components of the archaeological material. The organic substances were analysed using FTIR, direct exposure mass spectrometry (DE–MS) and gas chromatography – mass spectrometry (GC–MS). The inorganic component essentially consisted of halite (NaCl). Among the NaCl crystals, lamellar elements were identified. They were chemically characterized by carbonato‐apatite and showed a concentric morphology typical of the scales of small fish. The most prevalent organic constituents of the sample were monocarboxylic acids, α,ω‐dicarboxylic acids, and cholesterol and its oxidation products. The organic material composition was consistent with the occurrence of lipids of animal origin. In addition, diterpenes related to pine pitch were also identified. The overall results suggest that the material recovered in the small ceramic jar found in Antinoe is a residue of fish‐based pickles such as garum, muria, allex and liquamen, which were commonly used in Roman times.     

THE EMIGRATION OF PREALPINE LAKE MASTERS: A STUDY OF A 17TH‐CENTURY MANTELPIECE ATTRIBUTED TO THE CARLONE FAMILY OF ROVIO (TICINO,SWITZERLAND)*

This work illustrates the possible connections between the phenomenon of the seasonal emigration of lake masters and the production of artistic artefacts. Within the ambit of these dynamics, a stucco mantelpiece was taken into consideration. Nothing was known about the object: neither its origin, nor the artist who produced it, nor the period of execution. Historical, stylistic and formal analyses of the materials and of the technique with which the work was executed allow us to verify that the mantelpiece was produced using the stucco technique in the 17th century, in Rovio (southern Switzerland, Ticino), and that it comes from one of the exponents of the Carlone workshop, whose representatives were important in the tradition of itinerant artistic workers. Due to their good technical and professional specialization, the Carlone workshop served both public and private buyers. Tommaso Carlone is the principal representative artist of the Carlone workshop; it is certain that his workshop produced the stucco mantelpiece. The migrations of the artists were seasonal and they maintained a close bond with their country of origin. When they returned to the country of origin, they produced works of great artistic value, of which the mantelpiece represents a splendid example. Through the employment of conventional analytical techniques (optical and electron microscopy, infrared spectroscopy and porosity measurements), it has been possible to study the technique with which the work was executed, the materials used and the decay. The mantelpiece was produced using the stucco technique by means of a body layer (slaked lime and silicate and carbonate aggregates) and a marmorino finishing layer (slaked lime and pointed calcite crystals). Above this layer, whose thickness varies in relation to the executed result, there is a thin lime plaster whitewash, pigmented with the dispersion of yellow ochre particles; chromatic alterations are an oxalate patina caused by firm adhesion to the marmorino layer, due to the denaturation of the proteic substances employed. The final treatment was made with beeswax, which increased the marmoreal effect. Several additional layers of lime plaster whitewash have also been applied over the centuries. The figurative central square of the plastic decoration was made using red ochre.     

A NEW DATING METHOD FOR HIGH‐CALCIUM ARCHAEOLOGICAL GLASSES BASED UPON SURFACE‐WATER DIFFUSION: PRELIMINARY CALIBRATIONS AND PROCEDURES*

The first European settlers came to North America in the early 17th century using glass in the form of containers and decorative objects. Thus, glass is a horizon marker for all historic period settlements and a potential source of chronometric dates at archaeological sites belonging to the historic period in the Americas. We have developed a new absolute dating method based upon water diffusion into the surface of manufactured glasses that predicts diffusion coefficients based upon variation in glass chemical constituents. Low‐temperature (< 190°C) hydration experiments have been performed on a set of five high‐calcium (21.7–28.3%) glasses that were used to manufacture wine bottles from the 17th?19th centuries. Infrared spectroscopy and secondary ion mass spectrometry was used to model the water diffusion/alkali exchange process. The ability of the model to accurately predict archaeological ages was evaluated with artefacts recovered from ceramic‐dated contexts at Thomas Jefferson's plantation known as Monticello.     

REGIONAL VARIATIONS IN BLOOMERY SMELTING SLAG OF THE IRON AGE AND ROMANO‐BRITISH PERIODS*

This study highlights regional variation in the composition of iron‐smelting slag produced in England prior to the medieval period and attempts to link slag composition to the type of ore smelted. For many sites, the slag compositions were consistent with the use of limonite ore, but there is evidence that siderite ore was smelted at sites in Sussex in the late Iron Age/Romano‐British periods. A compositional comparison of smelting slags and slag inclusions in Iron Age currency bars, using data from Hedges and Salter (1979 ), illustrates the potential of smelting slag compositional data in provenance studies of early iron objects.     

CONSTRUCTING CARIBBEAN CHRONOLOGIES: COMPARATIVE RADIOCARBON DATING OF SHELL AND WOOD ARTEFACTS FROM PRE‐COLUMBIAN SITES IN CUBA

The lack of robust chronological frameworks for pre‐Columbian archaeology in the Caribbean limits the interpretive potential of ongoing studies of inter‐site and inter‐island interaction. This paper reviews the dating of 28 wood and shell artefacts from sites in northern Cuba in an attempt to date pre‐Columbian activity in the region and develop dating methodologies for the study of pre‐Columbian interaction in the Caribbean. This research compares dates from wood and shell artefacts from the waterlogged site of Los Buchillones in north‐central Cuba with dates from shell artefacts from sites on eight islands in the Sabana–Camaguey archipelago in the Bahama Channel. In addition to providing a chronological framework based on absolute dates for pre‐Columbian activity in northern Cuba, this paper also considers the methodological issues of using shell for dating pre‐Columbian activity in the Caribbean.     

FROM RAW IRON TO SEMI‐PRODUCT: QUALITY AND CIRCULATION OF MATERIALS DURING THE IRON AGE IN FRANCE*

Iron raw materials provide a privileged source of information for the reconstruction of metallurgical techniques and the circulation of iron products. An interdisciplinary approach, combining archaeological and archaeometrical studies of the exemplars known from the French Iron Age, has been undertaken. This enables a new typological classification to be produced that demonstrates a correlation between morphological and structural properties. Through comparison with chronological data, it is possible to propose a reconstruction of the organization of production according to three main periods, which are characterized by the circulation of different qualities of iron and by diverse levels of artisanal specialization.     

LEAD ISOTOPE ANALYSES OF BRONZE AGE COPPER‐BASE ARTEFACTS FROM AL‐MIDAMMAN,YEMEN: TOWARDS THE IDENTIFICATION OF AN INDIGENOUS METAL PRODUCTION AND EXCHANGE SYSTEM IN THE SOUTHERN RED SEA REGION*

The results of the lead isotope analysis (LIA) of 15 copper‐base artefacts from the Bronze Age site of al‐Midamman, Yemen, are reported. The LIA data suggest the existence of an indigenous Bronze Age metal production and exchange system centred on the southern Red Sea region, distinct from those in neighbouring regions of Arabia and the Levant. These preliminary results are highly significant for the archaeology of the region, suggesting that local prehistoric copper extraction sites have thus far gone unrecorded, and highlighting the need for systematic archaeometallurgical fieldwork programmes in the countries surrounding the southern Red Sea.     

BLACK AND RED GRANITES IN THE EGYPTIAN ANTIQUITY MUSEUM OF TURIN: A MINERO‐PETROGRAPHIC AND PROVENANCE STUDY

A recent project to investigate the stone artefacts preserved in the Egyptian Antiquity Museum of Turin has been undertaken, with the aim of supplying their systematic classification and suggesting the provenance site of the original raw materials. This paper focuses on seven sculptures dating back to the New Kingdom (18th–19th Dynasties): the statue of Ramses II, three of the 21 sculptures of the goddess Sekhmet, the statue of the goddess Hathor, the Ram‐headed Sphinx and the sarcophagus lid of Nefertari. Petrographic observations have shown that all the sculptures are made of granitoid rocks, with variable composition from granite to granodiorite and tonalite. The observation of strong macroscopic analogies with the so‐called black and red granites outcropping in the Aswan area has suggested a common origin of all the raw materials used for their manufacture. In order to verify this provenance hypothesis, several samples were collected in the Aswan quarry districts. According to results of a minero‐petrographic and geochemical comparison between the statues and the Aswan quarry samples, it was possible to identify the source area of the stone sculptures and finally to highlight the importance of an archaeometric approach to the solution of archaeological problems.     

THE USE OF TRACE ELEMENT ANALYSIS OF ENTRAPPED SLAG INCLUSIONS TO ESTABLISH ORE – BAR IRON LINKS: EXAMPLES FROM TWO GALLO‐ROMAN IRON‐MAKING SITES IN FRANCE (LES MARTYS,MONTAGNE NOIRE,AND LES FERRYS,LOIRET)*

Knowledge of the iron trade in ancient times rests on determining the source of the objects recovered during archaeological excavations. Unfortunately, attributing the origin is not always possible using archaeological tools alone. Trace element data of the ore and the archaeological material (reduction and reheating slags, entrapped slag inclusions from the bloom, bar iron and iron blades) from two Gallo‐Roman iron‐making centres, Les Martys (Montagne Noire) and Les Ferrys (Loiret), were determined using ICP–AES/MS and LA–ICP–MS. The results highlight a continuity of composition that makes it possible to establish a link between the initial ore and the semi‐finished iron products.     

ON THE ADVANTAGE AND DISADVANTAGE OF BLACK HISTORY MONTH FOR LIFE: THE CREATION OF THE POST‐RACIAL ERA

This article takes the Nietzschean dictum that history must “serve life” as a point of departure for an analysis of the American institution of Black History Month. Many continue to place great faith in the power of historical education to solve problems of race in America. Against this common‐sense view, this article argues that the excessive historicization of the problem of racism is at least as oppressive as forgetting. The black history propagated during this month has mostly been a celebration that it is history and thus a thing of the past. The article makes the claim that it is precisely a surfeit of black history that has encouraged the view that racism is vanishing in the river of time. The constant demand to view American racism through a historical frame has led to the perception that racism is a problem that must be historically transcended rather than solved. In other words, it is through the widespread dissemination of black history during Black History Month and elsewhere that the historical category of the post‐racial era has been constituted. The postracial era is not, as is so often claimed, a denial of historical context. On the contrary, it is an assertion that the horrors of racist discrimination were once real but are now over and done with.