PROVENANCE STUDIES OF CHALCOLITHIC OBSIDIAN ARTEFACTS FROM NEAR LAKE URMIA, NORTHWESTERN IRAN USING WDXRF ANALYSIS

In 2005–2006 we initiated a major archaeological survey and chemical characterization study to investigate the long-term use of obsidian along the eastern shores of Lake Urmia, northwestern Iran. Previous research in the area suggested that almost all archaeological obsidian found in this area originated from the Nemrut Daĝ source located in the Lake Van region of Anatolia (Turkey). More recent research on obsidian artefacts from the Lake Urmia region has identified a significant number of obsidian artefacts with compositions different from the sources near Lake Van. This suggests that the obsidian artefacts are from a yet to be identified geological source, but possibly one that was not too distant. In order to advance our knowledge of Iranian obsidians and eventually refine provenance criteria we analysed obsidian from 22 Chalcolithic sites and some source areas. The compositions of both obsidian source samples and artefacts were determined using wave length dispersive X-ray fluorescence spectrometry (WDXRF). This paper presents results from the trace elemental analysis of both geological and archaeological obsidians, providing important new data concerning the diachronic relationship between lithic technology and raw material in the north-west of Iran.     

The Use of Mineralogy to Identify Sources of Soapstone Artefacts: an Example from Soapstone Ridge,Georgia (USA)

The late Archaic Soapstone Ridge quarries, near Atlanta, Georgia, are the largest sources of archaeological soapstone in the south‐eastern USA. Ten soapstone artefacts from the coastal plain, over 200 km south of Soapstone Ridge (SSR), were used in an attempt to relate their mineralogy to that of the Soapstone Ridge quarries and to investigate the utility of mineralogy in the sourcing of soapstone. There is an overall similarity in the abundance of the major soapstone minerals, talc, chlorite and amphiboles in the artefacts and the SSR soapstone. Differences in the variety of amphibole (tremolite/actinolite, magnesiohornblende and magnesiocumingtonite/anthophyllite) and FeTi oxides (magnetite and ilmenite) eliminate SSR as a source for some of the artefacts. The compositions of chlorite (Cr), magnesiohornblende (Si, Al) and Fe oxides (Cr, Mn) in other artefacts are not consistent with a Soapstone Ridge source. The talc compositions are identical in the artefacts and the SSR soapstone. The mineral assemblage and compositions of two artefacts are consistent with a Soapstone Ridge source. Despite an overall similarity in the modal mineralogy of the artefacts and Soapstone Ridge quarries, there is enough diversity to distinguish between artefacts from Soapstone Ridge or some other source. Mineralogy is a useful tool for the evaluation of soapstone sources.     

Māori Textiles from Puketoi Station,Otago, New Zealand

Abstract

A group of Māori textile artefacts were discovered in a rock shelter in the southern South Island of New Zealand in 1895. The assemblage comprised a significant number of textile and textile-related artefacts including large and small bags, footwear and prepared leaf and fibre for textile production. The artefacts were privately owned until the 1920s when they were acquired by the Otago Museum, remaining there until new techniques made further investigation possible. This paper presents information from an interdisciplinary investigation of the Puketoi Station assemblage of textile artefacts, which examined artefact structure, form and function, and materials of construction. Interpretation of these artefacts using contemporary textile analysis methods, traditional weaving knowledge, and recent archaeological research, turns them from static objects into dynamic components of culture. The Puketoi Station artefacts embody and illustrate a unique material culture associated with the late prehistoric southern New Zealand Māori lifestyle.     

Bronze production in Southwestern Iberian Peninsula: the Late Bronze Age metallurgical workshop from Entre Águas 5 (Portugal)

Archaeological works at Entre Águas 5 (Portugal) uncovered a seasonal LBA settlement with significant metallurgical remains (crucibles, moulds, prills and a tuyere) related to bronze production. Radiocarbon dating ascribes an occupation period (10th–9th century BC) previous to Phoenician establishment in Southwestern Iberia. In spite of the proliferation of metal artefacts during LBA, the production of bronze alloys is still poorly understood. An integrated analytical approach (EDXRF, optical microscopy, SEM–EDS, micro-EDXRF and Vickers microhardness) was used to characterise this metallurgy. Crucibles show immature slags with copious copper nodules, displaying variable tin content (c. 0–26 wt.%), low iron amount (<0.05 wt.%) and different cooling rates. Certain evidences point to direct reduction of oxide copper ores with cassiterite. Scorched moulds with residues of copper and tin indicate local casting of artefacts. Finished artefacts also recovered at the site have an analogous composition (bronze with ∼10 wt.% Sn and low amounts of Pb, As and Fe) typical of coeval metallurgy in SW Iberia. Some artefacts reveal a relationship between typology and composition or manufacture: a higher tin content for a golden coloured ring or absence of the final hammering for a bracelet. An uncommon gilded nail (gold foil c. 140 μm thick; 11.6 wt.% Ag; ∼1 wt.% Cu) attests the existence of evolved prestige typologies. This LBA settlement discloses a domestic metallurgy whose main features are typical in Iberian Peninsula. Finally, it should be emphasized that a collection as comprehensive and representative of a single workshop has rarely been studied, enabling a deeper understanding of the various operations involving the bronze production and manufacture of artefacts.     

BLACKSMITHING TECHNOLOGY IN IRON AGE WESSEX

Summary. The sophistication of Iron Age blacksmithing technology in Wessex was determined by the metallurgical examination of 503 iron artefacts using Optical Metallography, Electron Microprobe Analysis and Vickers Hardness Testing. Iron artefacts from the different regions and site types of Southern Britain were examined to determine both the capabilities of Iron Age blacksmiths to alter the properties of iron artefacts through cold-working, carburization, heat-treatment and alloy selection, and the distribution of these possible techniques. The reasons for the selection of the areas, the sites, and the actual artefacts chosen for examination are discussed.     

Clues to Stone Tool Function Re-examined: Comparing Starch Grain Frequencies on Used and Unused Obsidian Artefacts

The identification of plant residues observed on prehistoric stone artefacts has often been used to inform on tool function without adequate consideration of potential contamination due to post-depositional processes. The paper redresses this balance by proposing a methodology which combines use-wear and residue analyses with systematic testing of depositional context to distinguish residues formed during tool use from accidental contamination. A case study involving obsidian artefacts from an open site in Papua New Guinea is used to illustrate the new approach. Starch grains, a class of residue which has had little attention outside Australia, were chosen as the focus of study because of their abundance at this site. The frequency of starch grains extracted from residues on stone artefacts was compared with those in sediments adhering to and adjacent to the artefact. A use-wear study conducted as a blind test provided an independent measure of whether the artefacts had been used. The frequency of starch grains was shown to be significantly correlated with used artefacts and not correlated with unused artefacts or the sediments. The case study demonstrates the importance of testing for contamination and also illustrates the benefit of studying starch grains as a class of plant residue.     

APPLICATIONS OF PETROGRAPHY AND ELECTRON MICROPROBE ANALYSIS TO THE STUDY OF INDIAN STONE SCULPTURE*

Examples of research on ancient Indian stone artefacts utilizing petrographic examination coupled with qualitative and quantitative electron beam microprobe analysis of specific minerals are described. Types of artefacts discussed include Gandharan schist sculptures. Pala dynasty phyllite and schist objects from eastern India, Hoysala sculptures from Karnataka state (southern India), and sandstone objects from northern India. In spite of the rich history of stone sculpture in the Indian subcontinent, characterization studies to date have been limited in scope, typically involving unprovenanced artefacts. The examples described point to areas in which more extensive research could produce useful information for the provenancing of artefacts.     

The Carving Technology of the Handle‐Shaped Artefacts from Yinxu (c.1300–1046 bc) in China

The handle‐shaped artefact is a special jade object of the Three Dynasties (c.2000–200 bc ) period. The manufacturing technology and function of the handle‐shaped artefacts are widely questioned. In this paper, two handle‐shaped artefacts from Yinxu (c.1300–1046 bc ) are tested by digital microscope, Raman spectrometer and scanning electron microscope. The results indicate that the handle‐shaped artefacts might be made in four steps, namely rough shape cutting, edge reforming, handle making and single‐side polishing. It also suggests that the handle‐shaped artefacts might be used as sacrificial offerings, but not as hairpins or handles.     

A Provenance Study of Early Bronze Age Artefacts Found in Asturias (Spain) by Means of Metal Impurities and Lead,Copper and Antimony Isotopic Compositions

We describe here the first combined isotopic and impurities study on 27 copper artefacts found in the north‐west of Spain. This study follows previous studies on the lead isotopic composition of copper ores in three local mines that were exploited during the Bronze Age. The levels of impurities found were clearly different from ingots and axes, with ingots having much higher levels of impurities. It was not possible to differentiate the origin of the artefacts only by the impurities present. On the other hand, the lead isotopic composition indicated that all artefacts were prepared from local ores, the ‘La Profunda’ mine being the most probable source for most artefacts that carried out a clear radiogenic lead signature. The copper isotopic composition seemed to be able to differentiate artefacts from the ‘El Aramo’ mine from those from the ‘El Milagro’ and ‘La Profunda’ mines. On the other hand, the antimony isotopic signature was not useful for source allocation.     

A Case of Identity: The Artefacts of the 1770 Kamay (Botany Bay) Encounter*

Collections of Indigenous artefacts made during the voyages of Captain James Cook have been extensively researched, but significant issues around the provenance and identification of artefacts remain complex and unresolved. This article considers the case of a shield in the British Museum, said for fifty years to have been appropriated by Cook at the time of first contacts with Gweagal in April 1770, and other artefacts associated with the same encounters.     

NEW RADIOCARBON ACCELERATOR DATES ON ARTEFACTS FROM THE EARLY MESOLITHIC SITE OF STAR CARR,NORTH YORKSHIRE*

For the well‐known early Mesolithic site of Star Carr, dating of organic artefacts by accelerator mass spectrometry (AMS) has been hampered by treatment of bone and antler recovered during the original excavations with preservatives. Some, untreated, artefacts were, however, collected after Clark's excavation in 1950. Four of these artefacts were AMS dated in 1995, but two of the dates were significantly younger than the others, and were questionable due to their low collagen yields. These suspect samples have now been re‐analysed, demonstrating that all four artefacts are of similar date. The significance of these dates for the chronology of Star Carr is discussed.     

Exploring preferences and non-use values for hidden archaeological artefacts: a case from Denmark

This paper presents a choice experiment study of a proposed wetland restoration project which aims to preserve archaeological artefacts from Stone Age villages which are presently buried within the topsoil. Wetland restoration can avoid destruction of the artefacts due to agricultural cultivation and drainage, and in addition improve biological diversity and recreational opportunities. The results indicate that even though the artefacts are not visible or usable for the population of today, but may contain information and potential value for future generations, the strongest preferences displayed is for ensuring permanent protection of archaeological artefacts, rather than biological diversity and recreational opportunities. The results are discussed in relation to the Prospect Theory: people value a loss of cultural heritage higher than a gain of new cultural goods or services. This insight is of general interest to cultural economics and cultural policy, especially with respect to heritage protection.     

Jetty-site artefacts from Holdfast Bay, South Australia: tracing the State's historical development from its early years, based on a functional analysis of submerged material culture

The results of an analysis conducted on an assemblage of artefacts recovered from an old jetty site in Holdfast bay, South Australia are presented. More than 5,000 artefacts were recovered during excavations in the 1970s at the site where the State's first settlers landed. Various objects were raised from the seabed, representing aspects of social, religious, economic, military, commercial, and maritime activities. The artefacts were recently recorded, catalogued, and analysed in an attempt to trace the history and development of the township from its early years as well as to assess the significance of the site.     

Archaeology and the Irish rediscovery of the Celtic past

This article examines the place of archaeology in the second wave of Irish cultural nationalism, and how archaeological findings were appropriated by rival ethno‐religious communities in Ireland. In particular, it focuses on George Petrie, who was the founder of ‘scientific’ archaeology and was also one of the leading figures in the nineteenth‐century Celtic revival that sought a moral regeneration of the Irish nation In Ireland, as elsewhere, archaeology was important in reconstructing an early history of the nation where few written records existed and in making this visible through material artefacts. However, archaeology was only significant as part of a wider cultural revival that presented artefacts and sites as national symbols to an island undergoing rapid social change. This article will explore the relationship between archaeology and this national revival, and how the material objects recovered by archaeologists extended and transformed the existing repertoires of how the nation was imagined and felt. It will assess the different reception of these images in the rival Catholic and Protestant communities. Finally, it will comment on the capacity of a medieval ‘Celtic’ repertoire to provide the basis of a dynamic modern Irish national culture.     

The role of arsenic in Chalcolithic copper artefacts – insights from Vila Nova de São Pedro (Portugal)

The Castro of Vila Nova de São Pedro (VNSP) is an emblematic settlement located at Azambuja, Portuguese Estremadura. It was occupied during the third and second millennia BC, predominantly during the Chalcolithic period. A diversified collection of 53 copper-based artefacts (most part in a fragmentary condition), belonging to an extensive metallic collection recovered during excavations carried out in VNSP, was studied using micro-EDXRF spectrometry, optical microscopy and SEM-EDS. Additionally, Vickers microhardness measurements were performed to establish the effectiveness of the thermomechanical treatment in the hardness of the artefacts. Results show that the Largo do Carmo, artefact collection is mainly composed of copper or arsenical copper, being 37% of the artefacts made of copper alloyed with arsenic (As > 2%). A statistically significant association was found between copper alloyed with arsenic and artefacts classified as tools/weapons (arrowheads, daggers and knives). In several cases, the presence of arsenic rich phases in the microstructure, resulting from an inverse segregation phenomenon, shows no evidence of chemical homogeneity control during the artefact manufacture. Microstructural analyses also show that the majority of this group (73%) was shaped with forging plus annealing operation cycles and 23% of the artefacts received a final cold hammering after the forging and annealing. An association between the presence of a final forging treatment and artefacts presenting higher arsenic contents was also identified. Nevertheless, no direct correlation was found between the arsenic content of the alloy and its hardness. Also no direct correlation was found between the hardness and a final forging operation. However, it was observed that a harder forging was applied to the cutting edge of the artefacts and consequently a high hardness in this area was obtained despite the arsenic content of the alloy. Concerning arsenical copper alloys, all evidences point out that the potential for obtaining a harder material was not recognized by the ancient metallurgists and the selection of the alloy was possibly made based on colour.     

Non-destructive pXRF of mafic stone tools

Archaeological use of non-destructive pXRF has been most systematically applied to the classification and provenancing of volcanic glass (obsidian) artefacts. Comparable work has yet to be developed for non-vitreous artefacts. We report results of pXRF analysis for a sample of grey to black (mafic) aboriginal hatchets from Sydney and adjacent coastal regions to the north and south. The study shows both broad and detailed classification is achievable depending on rock type and degree of elemental depletion or enrichment of the samples. PXRF analysis reveals not only distinct patterns of resource use between the three regions of this study but also enables a high degree of geographic resolution in the case of the basalt artefacts of our sample. We conclude that non-destructive pXRF is effective for reliable characterisation of non-vitreous stone artefacts that have a sufficiently complex and enriched compositional signature (i.e., unaltered basalts); with ∼50% of the basalt hatchets in our sample matched with spatially and geologically specific sources.     

Bladelet cores as weapon tips? Hafting residue identification and micro-wear analysis of three carinated burins from the late Aurignacian of Les Vachons,France

The interpretation of Upper Palaeolithic carinated lithic forms as discarded cores from the production of bladelets is now well established and the weight of evidence to support this indisputable. However, it is also clear that the relationships between lithic typology, technology and function are complex. Presented here are micro-wear analyses of three carinated burins from the late Aurignacian level of Les Vachons, France. The remains of birch pitch adhering to the artefacts are clear evidence that they were hafted; the first time this material has been identified on Aurignacian artefacts. Thus, while the techno-morphology of the artefacts is consistent with their role as bladelet cores our results indicate that they functioned as hafted tools. Unlike other Middle and Upper Palaeolithic industries the Aurignacian is not thought to include (non-bladelet) lithic weapon tips. However, due to patterns of use-wear present on two of the artefacts we suggest that this was their most plausible hafted function.     

First results of metallographic analysis and absolute dating of iron finds from Nowe Brzesko,site 26, Proszowice District

This paper presents the results of analyses of metal artefacts discovered at a multiphase site in Nowe Brzesko, Małopolskie Voivodeship, Poland. Fieldwalking prospection led to the discovery of steely iron objects, ploughed out on the site among other numerous archeological finds. A prospecting sondage yielded more corroded metal artefacts, identified mainly as agricultural tools (e.g. sickles, scythes). These chronologically nondistinctive artefacts could be assigned to the third to fourth century AD using radiocarbon dating, complemented by metallurgical analysis. The results open up new research perspectives on the economy and society of the Przeworsk culture in the Late Roman period.     

THE TECHNOLOGICAL AND TYPOLOGICAL BEHAVIOUR OF A NEANDERTHAL GROUP FROM EL SIDRÓN CAVE (ASTURIAS,SPAIN)

This paper presents the first detailed analysis of the lithic industry from El Sidrón Cave. Previously we have published other works concerning Anthropology and Palaeogenetics. The lithic assemblage contains 415 artefacts coming from both unofficial and official excavations and is largely flake‐based. The raw material derives from the immediate cave environment, and is mostly chert, with quartzite in a lesser proportion. To date, 67 artefacts have been refitted, including some tools and cores. The spatial distribution of the refitted lithic artefacts confirms, on the one hand, the unity of the assemblage and, on the other, its secondary context.