Small things in perspective: the contribution of our blind tests to micro-residue studies on archaeological stone tools

Our blind tests are distinctive for they were conducted on replicated stone tools used for a variety of tasks that included the processing of animal remains and plants. The analyst was required to differentiate an array of residues from microscopic morphological characteristics, using light microscopy. The original aim of our first tests was to assess the analyst's ability to identify a variety of plant and animal residues, but issues and problems that arose during the testing process made it clear that greater value might be gained from the lessons that we learnt about methodology and the direction for future micro-residue research. We show that problems identified during our first tests stimulated research. Amongst other things, we learnt to distinguish plant and animal remains more confidently than previously. Our residue analyses are firmly embedded in wider archaeological research and our tests help to explain why there are sometimes contradictions between the evidence from archaeologically recovered remains and residues on stone tools. A further outcome of the tests is that we have adopted a multi-stranded approach that provides a cautious, but secure strategy for identifying and interpreting use-residues. Our studies of contaminants through replications have also been invaluable for distinguishing incidental residues from use-related residues.     

Starch residues on museum artefacts: implications for determining tool use

A sample of 11 museum artefacts was examined to assess the preservation of any adhering organic residues, particularly starch granules, and to assess the potential for the identification of cooked starchy foods. The primary aim was to examine starchy deposits, extract starch granules and examine their physical condition to increase our understanding of the taphonomy of starch granules and associated organic residues in archived material and archaeological deposits. The study shows that organic plant residues could be recovered from archived artefacts and makes a significant contribution to understanding the function of this material. Recovered starch granules showed an interesting pattern of varying organic preservation on the surface of stone and wooden artefacts. Some starch granules were found to be well preserved while others in the same sample appeared to have been affected by enzyme degrading micro-organisms. Recovered residues included fully gelatinised starch.     

Experiments with Lithic Tools: Understanding Starch Residues from Crop Harvesting

Stone knives were used widely in Neolithic East Asia, presumably in the harvesting of grain crops, but their function has not been clearly understood due to the lack of study of residues from these tools. To address this issue, starch grain analysis was employed to study the residues on the surface of ancient stone knives and large amounts of starches were recovered. The sources of these starches, however, were not well understood, because harvesting of crops involves the cutting of stems rather than direct contact with starchy seeds. To determine whether harvesting could deposit these types of residues, we designed a simulation experiment using stone flakes to harvest ears of wheat, rice and foxtail millet, then analysed the residues on both the flakes and in the plant tissues. A large number of starch grains were found in the stems, including both typical morphotypes from seeds and newly described types that occur only in stems, which can be used as indicators of harvesting. Our study demonstrates that starch grains from residues on the surfaces of archaeological stone knives can indicate not only that the tools were used to harvest ears, but also the type of crops harvested.     

关于石片台面研究的一些问题-兼与卫奇先生商榷

本讨论了石片台面的分类、石片台面的类型等问题。台面可能按其保留情况、性质、加工情况和形态等不同层次进行分类,本主张应着重前3个层次进行分类。在某些特殊技术形成的石片中,台面的形态因为与该打片技术密切相关故也具有一定的分类意义。     

Clues to Stone Tool Function Re-examined: Comparing Starch Grain Frequencies on Used and Unused Obsidian Artefacts

The identification of plant residues observed on prehistoric stone artefacts has often been used to inform on tool function without adequate consideration of potential contamination due to post-depositional processes. The paper redresses this balance by proposing a methodology which combines use-wear and residue analyses with systematic testing of depositional context to distinguish residues formed during tool use from accidental contamination. A case study involving obsidian artefacts from an open site in Papua New Guinea is used to illustrate the new approach. Starch grains, a class of residue which has had little attention outside Australia, were chosen as the focus of study because of their abundance at this site. The frequency of starch grains extracted from residues on stone artefacts was compared with those in sediments adhering to and adjacent to the artefact. A use-wear study conducted as a blind test provided an independent measure of whether the artefacts had been used. The frequency of starch grains was shown to be significantly correlated with used artefacts and not correlated with unused artefacts or the sediments. The case study demonstrates the importance of testing for contamination and also illustrates the benefit of studying starch grains as a class of plant residue.     

UNDER THE HAMMER: RESIDUES RESULTING FROM PRODUCTION AND MICROWEAR ON EXPERIMENTAL STONE TOOLS*

This paper presents the results of an experimental programme investigating the effects of production processes on stone tools and their interference with use‐related features. In the first part of the experimental programme, a series of flint flakes was retouched with different kinds of hammers in order to assess the extent and nature of percussion residues. After careful environmental scanning electron microscope (ESEM) observation and energy‐dispersive X‐ray (EDX) analysis, the retouched flakes were thoroughly cleaned and the underlying flint deformation was recorded. The second part of the experimental programme involved selecting several uncleaned retouched pieces for use in short woodworking, hide‐processing and butchery experiments. These pieces were observed and analysed before, during and after use. Some of the percussion features proved to be surprisingly resistant to use, and in some cases turned out to be strikingly similar in appearance to use‐generated features.     

DNA AND PROTEIN RECOVERY FROM WASHED EXPERIMENTAL STONE TOOLS*

Traces of protein and DNA are preserved on stone tools used to process animals. Previous research documents the identification of protein residues from tools sonicated in 5% ammonium hydroxide, but it remains untested whether the same treatment yields useable DNA. In this study we report both DNA and protein recovery using 5% ammonium hydroxide from residues on stone tools. We extracted 13‐year‐old residues from experimentally manufactured stone tools used to butcher a single animal. We also show that surface washing procedures typically used to curate stone tools remove only a small fraction of the DNA and protein deposited during animal butchery.     

The oldowan reassessed: A close look at early stone artifacts

Early Stone Age assemblages called “Oldowan” and early “Developed Oldowan” are discussed, based on the results of a long-term study of Plio-Pleistocene sites at Koobi Fora, Kenya and an extensive experimental research program of replicating and using early stone artifact forms. Five major conclusions are drawn from this investigation: (1) many Oldowan core forms (“core-tools”) are probably simple by-products of flake manufacture rather than representations of stylistic norms; (2) flakes and retouched flakes - were essential tools in Oldowan technology, particularly for activities involving cutting; (3) this simple technology does not necessarily reflect the cognitive abilities of the early hominids that manufactured the stone artifacts; (4) there is evidence to show that Oldowan technology can be viewed as a simple curated one, in which raw material was intentionally carried from place to place for future use; (5) early hominid populations that made and used stone implements were not necessarily dependent upon them for their survival.     

Factors affecting Early Stone Age cut mark cross-sectional size: implications from actualistic butchery trials

Early Stone Age cut marks are byproducts of hominins' tool-assisted animal carcass consumption and provide a potential avenue of inference into the paleoecology of hominin carnivory. If diagnostic cut mark characteristics can be linked to flake and core tool use or the completion of distinct butchery actions, it may be possible to infer ancient tool preferences, reconstruct the consumption of specific muscular tissues, and illuminate landscape-scale stone resource use. Recently, diagnostic morphological criteria including cut mark width and depth have been used to identify marks made by different classes of experimental and archaeological stone tools (Bello, S.M., Parfitt, S.A., Stringer, C., 2009. Quantitative micromorphological analyses of cut marks produced by ancient and modern handaxes. Journal of Archaeological Science 36: 1869–1880; de Juana, S., Galan, A.B., Dominguez-Rodrigo, M., 2010. Taphonomic identification of cut marks made with lithic handaxes: an experimental study. Journal of Archaeological Science 37: 1841–1850; Dominguez-Rodrigo, M., de Juana, S., Galan, A. B., Rodriguez, M., 2009. A new protocol to differentiate trampling marks from butchery cut marks. Journal of Archaeological Science 36: 2643–2654). The work presented here adds to this experimental butchery database by using measurements of cut mark cross-section taken from bone surface molds to investigate how stone tool characteristics including flake versus core tool type, edge angle, and tool weight, influence cut mark width and depth, ultimately testing whether cut mark size is a useful indicator of tool identity. Additionally, these experiments investigate the influence of contextual factors, including butchery action, carcass size, and bone density on cut mark size. An experienced butcher used replicated Oldowan flakes and bifacial core tools in experimental trials that isolated skinning, bulk and scrap muscle defleshing, and element disarticulation cut marks on goat and cow skeletons. This sample explores cut mark traces generated under realistic butchery scenarios and suggests the following results: 1) Core and flake tools were equally efficient at completing all butchery tasks in size 1 and 3 bovid carcasses. 2) Samples of cut mark width and depth produced by core and flake tools were similar and cut marks could not be accurately classified to a known tool type. 3) Skinning and disarticulation activities produced significantly wider and deeper marks than defleshing activities. 4) Cut marks on cows tended to be wider and deeper than those on goats. 5) Cut mark width is negatively correlated with bone density when carcass size and bone portion are taken into consideration. These results suggest that a general quantitative model for inferring tool type or edge characteristics from archaeological cut mark size is not warranted.     

Levallois economics: an examination of ‘waste’ production in experimentally produced Levallois reduction sequences

Mathematical modelling has suggested that Levallois core morphology represents a reduction strategy driven by economic considerations; particularly the minimization of ‘waste’ while aiming to maximize cutting edge length of flakes obtained from cores of a given size. Such models are elegant in that they facilitate formal modelling of economic considerations that potentially motivate patterns seen in prehistoric data. However, the abstract nature of such models means that they do not take full account of all the practical difficulties and material challenges involved in reproducing Levallois-style reductions in stone. In particular, such models have only examined nodule morphology in two-dimensions, and did not take account of the fact that in the case of classic (lineal) Levallois reduction, core surfaces must be re-prepared between successive stages of flake removal. Hence, the potential economic implications of these factors are currently unknown, potentially undermining the significance of models that assume specific economic conditions. Here, we undertook to examine these factors using a series of experimentally produced Levallois reduction sequences. A total of 3957 flaking events were considered in our analyses, and we used six specific measures of economy to examine Levallois reduction across successive phases. Our analyses found that key assumptions of mathematical models suggesting that Levallois core morphology was driven by economic considerations (i.e. conservation of raw material when attempting to remove flakes with long cutting edges) can be upheld under the practical challenges of replicating Levallois-style reduction in stone. In supporting the notion that Levallois reduction has advantageous economic properties, our results emphasize the importance of considering why Levallois reduction did not emerge earlier in the archaeological record, and indeed, why even during the later Pleistocene the temporal and geographic distribution of Levallois technology varies. Our results also re-emphasize the value of formally modelling lithic reduction strategies in specific economic terms.     

Slicing Cut Marks on Animal Bones: Diagnostics for Identifying Stone Tool Type and Raw Material

Abstract

Butchering implements leave identifying signatures on bones. From these signatures, it is possible to distinguish the different raw materials and types of chipped stone butchering tools. The results of recent experiments enable us to distinguish the different types of raw materials and tools used in the butchering process, in particular those implements that produce slicing cut marks. Three types of chipped stone tools (blades,flakes, and side scrapers) and raw materials (flint, obsidian, and quartzite), as well as issues relevant to lithic production and use were examined and tested. Silicone molds of cut marks produced by each of the instruments were made and subjected to analysis in light optical and scanning electron microscopes under various levels of magnification. The criteria used for distinguishing tool type, raw material, type of production and use characteristics of the respective cutting instruments are presented, as well as a discussion of the application of the experimental results to the Early Bronze Age I site of Afridar, Israel. The data from Afridar indicate that almost all of the butchering marks on animal bones from the site were made by stone tools, in particular haphazardly-made flakes.     

河北昌黎渟泗涧细石器地点

<正> 淳泗涧细石器地点发现于1990年,91年10月,河北省文物研究所会同秦皇岛市文物管理处,昌黎县文物保管所对该地点进行了为期一个月的试掘。试掘面积25平方米,共发现400多件石制品,没有发现动物化石。 一、地理位置与地层 该地点位于昌黎县城东北2公里处,距其东南的淳泗涧村约0.5公里,地理坐标;E119°10′N39°44′,海拔65米。该地点背靠燕山余脉亮甲山,南为平原,京山铁路在地点南部穿过。其东南约14公里处即为渤海(图一)。 淳泗涧南为饮马河,东北为东沙河,两河向东注入渤海。地点附近的山前地带为饮马河的支流,支流两岸有两级阶地发育。二级阶地紧靠山脚,由于洪水冲刷以及山脚下基岩中泉水     

Swept under the rug: the problem of unacknowledged ambiguity in lithic residue identification

Microscopic analysis of organic residues on stone tools is used to interpret prehistoric stone tool functions. The morphology of some residues can be difficult to interpret, yet this ambiguity is rarely acknowledged in the literature. Our research seeks to understand the nature of this ambiguity by objectively identifying ambiguous residues in our reference collection. We trained four archaeologists in residue analysis using one part of our reference collection, then tested their ability to identify sixty-eight residues in another part of the same collection. Forty-eight of the residues in the test (70%) were correctly identified by three or all four subjects. We considered the remaining twenty residues, which were correctly identified by two or fewer of the subjects, to be ambiguous. These are most often in the hide-scraping, bone-scraping, and hardwood-scraping (macerated) categories, and tend to have an atypical morphology which falls in the range of variability of another residue category. Some of these residues also have optical properties which make them more difficult to image than others. We explore the potential for scanning electron microscopy (SEM) to improve residue identification in a second test. This test shows a modest improvement in identification success rates of ambiguous residues when SEM images are included. We conclude that while images from different types of microscopes can improve reliability of identification, some residues will always be ambiguous. Rather than being ignored, these ambiguities should be brought to light, closely examined, and published as such.     

An experimental ethnoarchaeological approach to understanding the development of use wear associated with the processing of river cane for split-cane technology

Southeastern Indians have been using cane (Arundinaria spp.) for basketry and matting for thousands of years. Unfortunately, it is only under extraordinary preservation conditions that such items survive archaeologically. Inferring the production of split-cane technology requires an understanding of prehistoric manufacturing and processing techniques. It is hypothesized that stone tools were once used to process cane for use in split-cane technologies. In the Southeast, it is not uncommon to find stone tools with traces of plant use; however attributing wear to specific plants has been problematic. Pilot experiments, grounded on ethnoarchaeological observations, were conducted with river cane (Arundinaria gigantea) in collaboration with expert basket weavers in the Cherokee Nation. The experimental ethnoarchaeological program was designed to test the efficiency of stone tools in cane processing and document use wear through microscopic observations. The results found that non-retouched flakes were efficient for processing river cane and that the different stages of splint preparation resulted in the differential development of use-related wear. Additional experimentation with river cane is necessary to better define use wear and establish criteria for identification in archaeological contexts. Nonetheless, the collaborative and experimental approach undertaken demonstrated the utility of combining traditional archaeological methods with experimentation, ethnoarchaeology, and tribal knowledge.     

The Mousterian bone retouchers of Noisetier Cave: experimentation and identification of marks

Retouchers are fragments of bone used during the Paleolithic to strike stone flakes in order to transform them into retouched tools. Our experiments show that the mark produced on retouchers differs depending on whether they were used to strike flint or quartzite. Our results suggest that numerous pits, most often with an ovoid form, characterize the retouching of quartzite flakes. Most of the scores produced with this material have a sinuous morphology with rough interior faces. The areas with superposed traces have a pitted appearance. On the other hand, the retouching of flint flakes, produces pits that are most often triangular in form. Most of the scores have a rectilinear morphology with smooth interior faces and their superposition results in the formation of hatch marks. There is also a relationship between the characteristics of the mark and the relative state of freshness of the retouchers. The validity of the criteria identified was confirmed by a blind test. These diagnostic criteria were applied to archaeological retouchers from the Mousterian site of Noisetier Cave. The results obtained improve our knowledge of the technical behaviors of Neanderthals and allow us to address questions concerning their techno-economic implications.     

Chemical Alteration of Lithic Artefacts: an Experimental Case Study on the effect of Guano on Stone Flakes and Its Contextualization in the Archaeological Assemblage of Azokh Cave (Southern Caucasus)

Chemical weathering of archaeological material is well known; however, while there have been a number of experimental studies demonstrating different types and degrees of chemical alteration on faunal remains, little attention has been paid to stone tools, and the few studies that exist relate mainly to siliceous materials and water‐induced chemical alteration. Azokh Cave, located in the South Caucasus, contains a Middle Pleistocene to Holocene infill, and detailed macro‐ and microscopic examination of the lithic assemblages recovered there indicates potential chemical weathering of the stone artefacts. The cave is also currently home to one of the largest bat colonies in the region, and their guano forms a significant component of the infill of the inner galleries. Based on these two factors, an experimental pilot study was set up to artificially chemically alter a range of stone flakes produced specifically for the task, in order to determine the nature and likely cause of weathering. The experimental flakes, produced from different raw materials, were buried in fresh bat guano for up to two years. The results reported herein demonstrate that in a relatively short time, the highly acidic composition of bat guano strongly affects calcium‐bearing rocks (e.g., limestone, basalt) altering their entire surface. Similar comparisons may be made with chemical alteration evident on archaeological lithics from Azokh Cave, suggesting that bat guano has played a significant role in diagenetic alteration.     

Toolstone constraints on knapping skill: Levallois reduction with two different raw materials

Lithic raw material constraints are widely assumed to be a determining factor of flaked stone tool morphology, but this assumption remains largely untested. We conducted a controlled experiment to determine whether a knapper’s growing replication skills would be hindered if the toolstone used was switched from large flakes of an easily worked chert to nodules of less tractable one. Two batches of Preferential Levallois cores were knapped, an earlier series made from standardised large flakes of sediments dominated by chalcedonic quartz followed by a more challenging one using variably-shaped, cortical nodules of microcrystaline quartz that varies in the completeness of quartz replacement of calcite and dolomite. Skill level markers were designed to measure the knapper’s ability to achieve a series of set goals. These were quantified and subjected to statistical testing. In all but one test, significant increases in skill could be detected from the earlier to the later batch of reductions, despite the drop in toolstone quality. Significant improvements in the consistency of the knapper’s output could also be detected. However, the switch to a more challenging, nodular chert did require extra shaping, which resulted in more waste. This masked visible progress towards producing a less costly core. Overall, our results do not support the assumed primacy of toolstone constraints over other factors in influencing the morphology of flaked stone tools.     

Experimental assessment of maize phytolith and starch taphonomy in carbonized cooking residues

Many taphonomic studies of plant microfossils, specifically phytoliths and starch, are concerned with post-depositional movement, contamination, and morphological changes due to environmental fluctuations or plant processing. Additionally, the identification of phytoliths and starches archaeologically are based on their presence or absence. This paper examines whether it is possible to identify maize (Zea mays ssp. mays) phytolith and starch abundance associated with different processing behaviors as replicated through experimentally produced cooking residues. If successful, identification of likely associated processing and taphonomy of these microfossils will allow for a more refined interpretation of plant use as it relates to timing and plant form and processing.     

Stone Tool-Making and Brain Activation: Position Emission Tomography (PET) Studies

This study introduces to archaeology a new experimental technique for examining the relationship between stone tool-making and brain function. The principal focus of this exploratory study was the development of effective methods for the identification and examination of the regions of the modern human brain recruited during the manufacture of simple (Oldowan or Mode I) stone tools. The functional brain imaging technique employed, Positron Emission Tomography (PET), examines task-related brain activity by assessing changes in regional cerebral blood flow during specific tasks. The single-subject study reported here represents a heuristic, initial exploration of this subject. Results indicate that during stone tool-making there was heavy activation of cortical and subcortical regions of the brain associated with motor and somatosensory processing. Especially interesting was the high degree of activation in areas known to be involved with complex spatial cognition requiring integration of diverse sensory inputs (e.g. vision, touch, and proprioception, or sense of body position and motion). Expansion of such higher-order association areas has been particularly important during the course of human evolution. This single-subject pilot study demonstrates the application of the PET brain imaging technique to the study of early stone technologies and suggests hypotheses to be tested in more comprehensive studies in the future.     

Developing FTIR Microspectroscopy for the Analysis of Animal-Tissue Residues on Stone Tools

The analysis of microscopic residues on stone tools provides one of the most direct ways to reconstruct the functions of such artifacts. However, new methods are needed to strengthen residue identifications based upon visible-light microscopy. In this work, we establish that reflectance Fourier-transform infrared microspectroscopy (FTIRM) can be used to document IR spectra of animal-tissue residues on experimental stone tools. First, we present a set of reflectance FTIRM standards for the most commonly identified animal-tissue residues on stone tools: skin, meat, fat, hair, blood, feather barbules, fish scales, and bone. We provide spectral peak assignments for each residue and demonstrate that high-quality reflectance FTIRM spectra can be generated under ideal circumstances. Second, we document the spectra for these residues when they are located on a stone substrate such as flint or obsidian. We discuss procedures for correcting spectra that are affected by specular reflection and explain the effects of spectral interference from the stone. Our results show that reflectance FTIRM is sensitive to small intra-sample differences in composition. This means that it will record the effects of decomposition in ancient residues. The methodological developments we present here will help lithic residue analysts incorporate in situ reflectance FTIRM into their analysis protocols to strengthen identifications.