On-line computing and radiocarbon dating at the British Museum

This paper describes the way in which the Hewlett Packard 2100A computer installed at the British Museum Research Laboratory is used by the Radiocarbon Dating Unit. A system of programmes and files has been developed to register sample count rates, calculate age estimates and monitor the performance of the counting equipment. The system was designed to be simple and convenient to use and has fulfilled our expectations.     

AMS C dating of early human occupation of southern South America

The time of appearance of a persistent and demographically-viable hunter-gatherer population in late Pleistocene southern South America must be determined by evaluating evidence from as large as possible a sample of candidate archaeological sites in the region. We co-ordinated the AMS dating of multiple bone and charcoal samples from previously-excavated strata at the following sites: Arroyo Seco 2, Paso Otero 5, Piedra Museo, and Cueva Tres Tetas (all in Argentina), and Cueva del Lago Sofia 1 and Tres Arroyos (both in Chile). With one possible exception, we did not obtain new results to confirm earlier observations of pre-Clovis-age cultural activity at any of the sites considered in this study. The possible exception, Arroyo Seco 2, is considered in detail elsewhere [Politis G., Gutierrez M.A., Scabuzzo, C. (Eds), in press. Estado actual de las Investigaciones en el sitio 2 de Arroyo Seco (región pampeana, Argentina). Serie Monográfica INCUAPA 5. Olavarría]. However, our results for the samples which were the most preferred indicators of cultural events (hearth charcoal and cut-marked bone) confirm that people were in the southern cone of South America at or soon after 11,000 BP (13,000 cal BP). Considered alongside recent age estimates for the Clovis culture in North America, these results imply the contemporaneous emergence of a consistent and archaeologically-robust human occupation signal at widely-separated locations across the Western Hemisphere. Such findings suggest that Palaeoindian demic expansion may have involved more than one terminal Pleistocene dispersal episode.     

Characterisation and blind testing of radiocarbon dating of cremated bone

The success of radiocarbon dating of burned or cremated bones depends on the exposed temperature during burning and the degree of re-crystallisation of the inorganic bone matrix. We present a method for characterisation of likely cremated bones by employing visual inspection, infrared spectrometry and carbon stable isotope analysis on the bio-apatite fraction. The method of radiocarbon dating of cremated bones was tested by dating paired samples of bone and associated context materials such as pitch, charcoal and a dendrochronologically dated oak coffin. The dating of these paired test samples were largely performed as blind tests and showed excellent agreement between pitch and bone. The weighted mean age difference of all test samples is observed to −9 ± 60 ¹⁴C yr. To test the indicators and the effects of the degree of burning, a Late-Neolithic human individual has been studied, as this individual exhibits the full spectrum from low temperature burning (charred) to high temperature (“cremated”) from one end of a single bone to the other. This is reflected as a marked step in numerous parameters as well as in a significant difference in ¹⁴C age between the charred and the cremated bone samples.     

Contemplating the history and future of radiocarbon dating in the American Southeast

We consider the history, present, and future of radiocarbon dating in the American Southeast. We point out some of the past and present flaws related to archaeological research and dating. Our approach to this review is rooted in the perspective that each radiocarbon date collectively adds to our knowledge of the region and not just a particular site. Based on our observations, we suggest some “good” practices with respect to certain aspects of radiocarbon dating. Our concluding discussion considers Bayesian chronological analysis and the growing contribution of chronological modeling to the Southeast.     

Luminescence and radiocarbon dating as tools for the recognition of extraterrestrial impacts

Extraterrestrial events and the extraterrestrial origin of both material and impact forms were recognized in the Morasko, Kaali and Przełazy shallow geological profiles by means of luminescence and radiocarbon dating as well as the frequency of magnetic spherules. The obtained results provide a promising tool for proving theat extraterrestrial events affected characteristic lithological and morphological environmental features.     

A comparison of the treatment of errors in radiocarbon dating calibration methods

The application of radiocarbon dating to archaeological samples generally requires calibration of ¹⁴C dates to calendar ages and interpretation of dating errors. In this paper, four recent methods of age calibration are assessed, particularly with regard to their quality of error treatment. Recent experimental research has suggested that commonly quoted errors on “raw” ¹⁴C dates may require enlargement to more realistic levels, which, when incorporated in the calibration schemes, produce a considerable increase in the size of the typical calibrated interval. A general decrease in the sensitivity of ¹⁴C dating using single, “normal precision” dates is implied. Thus typical calibrated age intervals range from 300 to 1300 years (approximate 95% confidence level), with little improvement resulting if “high precision” calibration systems are used to correct “normal precision” dates. Of the four methods considered here, that proposed by Neftel is found to provide the most objective, flexible, comprehensive and “easy to use” scheme. This method is particularly recommended for its treatment of errors both on the dates to be calibrated and on the calibration curve itself.     

Dendrochronological and radiocarbon dating of subfossil wood from the Morava River basin

The paper deals with dendrochronological and radiocarbon dating of subfossil trunks found in the basin of the Morava River. The research into subfossil trunks had been conducted in the Czech Republic in the past but the research stopped in 2001. 160 records of measurements of subfossil, predominantly oak trunk samples, are preserved from that time. Three years ago the research was reopened and again the most trunks were found in the basin of the Morava River. 92 samples of oak trunks and 7 samples of other tree species (poplar, elm, maple, beech) were taken from selected sites. The samples were processed in compliance with the standard dendrochronological methodology. To date the samples, Czech, Austrian, Polish and German standard chronologies were used. In cases when the dendrochronological dating was unsuccessful, the samples were sent for radiocarbon dating. In total, 35 samples were dated, mainly by the radiocarbon method. Subfossil trunks from gravel pit Tovačov were dated and classified into 4 different periods, the oldest being from 2780–2190 BC. In Osek nad Bečvou, the samples were taken from two sites. Whereas from the 4 trunks taken in the river channel each was from a different period, the trunks from the gravel pit come from 981–1015 AD. The trunks found in the Morava River basin near Strážnice were dated to the 10^th–15^th century. In the future, we expect to extend the amount of the acquired samples with the aim to create a link to the existing standard chronology or to create a long floating average treering curve.     

Testing the human factor: radiocarbon dating the first peoples of the South Pacific

Archaeologists have long debated the origins and mode of dispersal of the immediate predecessors of all Polynesians and many populations in Island Melanesia. Such debates are inextricably linked to a chronological framework provided, in part, by radiocarbon dates. Human remains have the greatest potential for providing answers to many questions pertinent to these debates. Unfortunately, bone is one of the most complicated materials to date reliably because of bone degradation, sample pre-treatment and diet. This is of particular concern in the Pacific where humidity contributes to the rapid decay of bone protein, and a combination of marine, reef, C₄, C₃ and freshwater foods complicate the interpretation of ¹⁴C determinations. Independent advances in bone pre-treatment, isotope multivariate modelling and radiocarbon calibration techniques provide us, for the first time, with the tools to obtain reliable calibrated ages for Pacific burials. Here we present research that combines these techniques, enabling us to re-evaluate the age of burials from key archaeological sites in the Pacific.     

Ancient long-distance trade in Western North America: new AMS radiocarbon dates from Southern California

Eleven Olivella biplicata spire-lopped shell beads from six sites located 250–365 km inland from the Pacific coast of southern California produced AMS dates between 11,200 and 7860 CAL BP. Olivella shell beads were well-documented items of prestige and media of exchange in Native California, and recovery of these examples from inland contexts indicates low-level exchange between resident populations of the coast and the southwestern Great Basin by at least 10,300–10,000 CAL years BP. These findings represent some of the earliest unequivocal evidence for long-distance trade in western North America and push the antiquity of this important form of inter-group interaction back several thousand years earlier than previously thought.     

The formation process of a paleoindian open-air site in Central Brazil: integrating lithic analysis,radiocarbon and luminescence dating

Lithic analysis, radiocarbon dating and luminescence dating are applied to a stratified open-air Paleoindian site in Central Brazil, lending some balance to a published record dominated by rock shelter sites. Most lithics are found in two discrete occupation layers. Lithics found outside these layers are attributed to post-depositional movement of small flakes mainly upwards. Single-grain luminescence dating on quartz grains also suggest post-depositional movement. Both wind and bioturbation are suspected mechanisms. The luminescence analysis does not provide precise depositional dates in this situation but does support such dates suggested by radiocarbon.     

Combining an archaeomagnetic and radiocarbon study: dating of medieval fireplaces at the Mühlegasse,Zürich

During the restoration of the Radium cinema located in the old Town of Zürich, a stratigraphic sequence of medieval fireplaces came to light. Based on ceramic finds, a preliminary age of about 1000 AD was assigned. In this paper we show the results from archaeomagnetic and radiocarbon dating, which combined with the stratigraphic information yield a better constrain of the period of use of these fireplaces. Whilst the radiocarbon technique continues to be the most widespread methodology for dating young archeological artifacts, archaeomagnetic dating is becoming increasingly more established in Europe thanks to the increased number of available measurements. A Bayesian model on the period of use of these fireplaces was produced with OxCal, by a combination of magnetic and radiocarbon ages, together with the stratigraphic information. The results show that the fireplaces were probably used during 1 to 2 generations (e.g. 20–40 years each), and are in good agreement with the archaeological context of this site. To make use of the magnetic measurements for future reconstructions of the field, we carried out an additional age model using only the radiocarbon and the stratigraphic information. Although some of the structures show large directional scatter due to poor baking in antiquity, the results confirm the trend of the geomagnetic field around 1000 AD.     

Comparison of fluoride and direct AMS radiocarbon dating of black bear bone from Lawson Cave,Missouri

Abstract

After a 20-year hiatus (1955–1975) during which few archaeologists discussed fluoride dating, the method again received attention in the 1980s and 1990s when some argued for its validity. As a dating method, fluoride dating depends on the rate at which fluorine ions replace hydroxyl ions in osseous tissue. The rate of replacement is influenced by the properties of the skeletal part (SP), sediment chemistry (K), and sediment hydrology (H), and the replacement rate influences estimates of time. Calibrated AMS radiocarbon assays of 10 black bear (Ursus americanus) femora from a natural-trap cave in central Missouri are weakly correlated with fluorine concentrations, determined by neutron activation analysis in the 10 femora. Despite minimal variation in SP, K, and H, results indicate fluoride dating can be considered a valid dating method only in cases when the chronological validity of its results are confirmed with independent chronometric data. As similarities in fluorine amounts across specimens increase, provenience information and bone orientation data as well as fine resolution data on K and H become critical to the application of fluoride dating.     

Funerary practices and kinship in an Early Bronze Age society: a Bayesian approach applied to the radiocarbon dating of Argaric double tombs

The main aim of this paper is to test the hypothesis on kinship relations (affinity/marriage vs descent/consanguinity, and matrilocality) expressed in the funerary record of the El Argar Bronze Age society (South-east Iberia, 2200–1550 cal BCE), taking into account the absolute chronological dimension of double adult tombs. A set of 23 double tombs having radiocarbon dates for both skeletons were selected, and radiocarbon calibration and Bayesian probability analysis was conducted. The results support the ‘descent’ hypothesis, since for most of the cases the chronological distance between individuals buried together was larger than two decades. Finally, several guidelines for future research are suggested in order to overcome shortages in current chronological and archaeological data.     

High-resolution radiocarbon dating of marine materials in archaeological contexts: radiocarbon marine reservoir variability between Anadara, Gafrarium, Batissa, Polymesoda spp. and Echinoidea at Caution Bay, Southern Coastal Papua New Guinea

The remains of shellfish dominate many coastal archaeological sites in the Pacific and provide a wealth of information about economy, culture, environment and climate. Shells are therefore the logical sample type to develop local and regional radiocarbon chronologies. The calibration of radiocarbon (¹⁴C) dates on marine animals is not straightforward, however, requiring an understanding of habitat and dietary preferences as well as detailed knowledge of local ocean conditions. The most complex situations occur where terrestrial influences impinge on the marine environment resulting in both the enrichment and depletion of ¹⁴C (Ulm Geoarchaeology 17(4):319–348, 2002; Petchey and Clark Quat Geochronol 6:539–549, 2011). A sampling protocol that combines a high-resolution excavation methodology, selection of short-lived samples identified to species level, and a tri-isotope approach using ¹⁴C, δ¹³C and δ¹⁸O, has given us the ability to identify ¹⁴C source variation that would otherwise have been obscured. Here, we present new research that details high-resolution mapping of marine ¹⁴C reservoir variation between Gafrarium tumidum, Gafrarium pectinatum, Anadara granosa, Anadara antiquata, Batissa violacea, Polymesoda erosa and Echinoidea from the Bogi 1 archaeological site, Caution Bay, southern coastal Papua New Guinea. These isotopes highlight specific dietary, habitat and behavioural variations that are key to obtaining chronological information from shell radiocarbon determinations.     

New radiocarbon dating of the transition from the Middle to the Upper Paleolithic in Kebara Cave,Israel

The Middle to Upper Paleolithic transition (MP-UP transition) is considered a major technological and cultural threshold, at the time when modern humans spread “out of Africa”, expanded from the Levant into Europe and possibly into central and northern Asia. The dating of this techno-cultural transition has proved to be extremely difficult because it occurred sometime before 40,000 radiocarbon years before present (¹⁴C years BP), which is close to the end of the effective dating range of radiocarbon. Other dating methods such as Thermoluminescence (TL) or Electron Spin Resonance (ESR) are not sufficiently precise to date the recorded archaeological MP-UP transition in the Levant. Here we report a consistent set of stratified radiocarbon ages on freshly excavated charcoal from Kebara Cave, Mt. Carmel (Israel), that span the late Middle Paleolithic (MP) and Early Upper Paleolithic (EUP) This study applied novel strategies to improve sample preparation techniques and data analysis to obtain high-resolution radiocarbon models. From this study it is proposed that the MP-UP transition for this site can be placed immediately after 45,200 ± 700 ¹⁴C years BP and before 43,600 ± 600 ¹⁴C years BP or from 49/48 to 47/46 radiocarbon calibrated years before present (years Cal BP).     

Relation between radiocarbon,archaeological dating and sediment properties on the example of colluvial deposits (NE Poland)

This study focuses on the analysis of the structural and textural features of the colluvial (deluvial) deposits in the Suwałki Lake District (NE Poland) and their absolute age. The colluvium has a thickness of up to 150 cm. The dates of the peat under colluvium or lowermost fossil humus-rich horizons point to the ages from 5405±80 BP to 480 BP. Deposition of material at the footslope is a result of a denudation triggered by human action (surface water erosion and tillage erosion) and usually corresponds with the settlement stages. The ¹⁴C dating of deposited sediment sometimes indicated to older dates of colluvium then the archaeological evidence available for examined sites. Locally, the overlying fossil humic horizon was older then the lowermost one. The textural features of the colluvial deposits such as: the content of fine fraction, weak sorting and relationship between the mean grain-size (Mz) and the sorting index (σ₁) were used to recognize sediment redeposited from the upper part of the slope. Basing on the mineral composition and electrical conductivity of fossil humus horizon it is possible to say whether the soil was degraded or aggraded. These features of the humus-rich horizons occurring between colluvial sediments can be used to explain discrepancy between the radiocarbon dating and archaeological evidence.