Optically stimulated luminescence (OSL) dating investigations of rock and underlying soil from three case studies

Three rock samples and associated underlying surface (floor) soils of geoarchaeological significance from Greece, Sweden and a modern surface stone-sample from a Danish site were investigated using OSL dating. Thin slice, sub-samples, from drilled core surfaces were prepared. A single-aliquot regenerative-dose (SAR) protocol was used on whole rock slices to estimate the laboratory equivalent dose. Laboratory tests showed that the SAR protocol successfully corrected for sensitivity changes and that a known laboratory dose could be measured accurately.     

沙特阿拉伯宪政历程的源头--自由亲王运动

"自由亲王"是沙特阿拉伯现代化发展初期的第三种政治力量,是沙特阿拉伯经历从传统君主制到"发展的独裁模式"之历史性变革的重要推手。自由亲王运动根源于石油时代沙特阿拉伯经济社会秩序的变动,在沙特阿拉伯首次提出宪政民主等现代政治理念并尝试付诸实践,由此成为沙特阿拉伯宪政历程的源头,对沙特阿拉伯政治现代化的发展具有启蒙意义,预示着沙特阿拉伯政治现代化进程的发展方向。     

Palaeochannels of the Balkh river (northern Afghanistan) and human occupation since the Bronze Age period

In 2002, the unexpected discovery of Hellenistic architectural blocks, buried in 8 m of alluvium, found displaced in a former bed of the river of Balkh, brought about a programme of surveys and excavations under the aegis of the French Archaeological Mission in Bactria. The geoarchaeological side of the programme focused on the drawing of a regional geomorphological map then on the identification, mapping and dating of the palaeochannels of the river of Balkh. We established the chronology of several fluvial channel generations by association with archaeological settlements of different eras (Bronze Age, Bactro-Achaemenid period, Kushan period, Islamic period) and with optically stimulated luminescence dating carried out on alluvium deposits. The present riverbed leading up to Aqcha was formed during the Islamic period. We suspect the primary agent of this change in the river channel to, be tectonic activity and the activation of a blind fault crossing the floodplain. We identified a northern Bactro-Achaemenid aqueduct, currently located in the desert area separating the plain of Balkh from the Amu Darya.     

Google earth and the archaeology of Saudi Arabia. A case study from the Jeddah area

Archaeologically, Saudi Arabia is one of the least explored parts of the Middle East. Now, thanks to Google Earth satellite imagery, a number of high-resolution ‘windows’ have been opened onto the landscape. Initial investigations already suggest large parts of the country are immensely rich in archaeological remains and most of those identified are certainly pre-Islamic and probably several thousand years old. Detailed interpretation of one ‘window’ east of Jeddah forms the basis for illustrating the richness of the heritage and how the satellite imagery can be exploited to shed important light on the character and development of the human landscape. Through this ‘window’ we set out a proposed methodology for future work and where it may lead.     

A note on the dating of the clay smoking pipes collected in the course of two archaeological surveys conducted in Saudi Arabia: the Comprehensive Survey of Saudi Arabia (1976–1981) and Michael Gilmore’s survey of the Darb al‐Hajj

Several clay smoking pipes (chibouks) were recovered during the course of two archaeological surveys conducted during the late 1970s and early 1980s in Saudi Arabia. At the time these projects took place, no published clay tobacco pipe typologies existed, forcing the participants to assign a cursory date of ‘Ottoman period’ to the pipes. Since then, considerable archaeological research has been done on the Ottoman clay pipe. The following concerns the refining of the dates of these tobacco pipes in light of new studies.     

On the intrinsic accuracy and precision of luminescence dating techniques for fired ceramics

Luminescence dating techniques have been used extensively for archaeological and geological samples. Such techniques are based on thermally or optically stimulated signals. This paper presents simulations of several luminescence techniques for equivalent dose (ED) estimation for ceramic materials containing quartz. The simulations are carried out using a recently published comprehensive kinetic model for quartz, consisting of 11 electron and hole traps and centers. The complete sequence of the experimental protocols for several thermoluminescence (TL) and optically stimulated luminescence (OSL) techniques are simulated using the same set of kinetic parameters. The specific simulated protocols are: additive dose TL protocol, predose technique (both additive and multiple activation versions), phototransfer protocol, single aliquot regenerative optically stimulated luminescence (SAR-OSL) protocol, and SAR thermoluminescence protocol (SAR-TL). One hundred random variants of the natural samples were generated by keeping the transition probabilities between energy levels fixed, while allowing simultaneous random variations of the concentrations of the 11 energy levels. The relative intrinsic accuracy and precision of the protocols are simulated by calculating the equivalent dose (ED) within the model, for a given natural burial dose of the sample. The intrinsic accuracy of these techniques is estimated by simulating natural irradiation of the samples with a known burial dose, followed by simulation of the luminescence method used to recover the estimated dose ED. The percent difference between the burial dose and the ED value represents the simulated accuracy of the luminescence technique. The relative intrinsic precision of these techniques is estimated by fitting Gaussian probability functions to the ED values obtained with the 100 model variants. It is found that the various techniques can reproduce natural paleodoses in the range 10 mGy–10 Gy with a typical intrinsic accuracy of +1 to 10%. Techniques based on single aliquot protocols were found in general to be more precise than techniques requiring the use of multiple aliquots. In addition, techniques based on interpolation of experimental data were found to be consistently both more precise and accurate than those based on extrapolation of experimental data.     

Strofilas (Andros Island,Greece): new evidence for the cycladic final neolithic period through novel dating methods using luminescence and obsidian hydration

The recently excavated coastal prehistoric settlement of Strofilas on Andros Island (Cyclades, Greece) in the Aegean sheds new light on the transitional phase from the Final Neolithic to Early Cycladic period regarding masonry, fortification, and richly engraved rock art. The fortification possesses early evidence of preserved defensive architecture, as evidenced from the plethora of scattered finds from within and around the settlement. Important features are carvings on rock walls which mainly depict ships, animals, and fish. Initial archaeometric dating via the application of luminescence dating of two samples from the fortified wall bearing engraved ships, and by obsidian hydration of two blades employing the new SIMS-SS method (secondary ion mass spectrometry via surface saturation), has been undertaken to determine the site's chronology. The former yields an average date of 3520 (±540) BC and the latter an average date of 3400 (±200) years BC, both of which, within overlapping errors, suggest the main settlement occurred during the Final Neolithic.     

An improved OSL chronology for the Still Bay layers at Blombos Cave,South Africa: further tests of single-grain dating procedures and a re-evaluation of the timing of the Still Bay industry across southern Africa

This paper presents a series of new single-grain optically stimulated luminescence (OSL) ages for the Still Bay at Blombos Cave, South Africa, and compares them to previously published OSL, thermoluminescence (TL) and electron-spin resonance (ESR) ages for this site. Details are provided about the measurement and analytical procedures, including a discussion of the characteristics of the OSL signals of individual quartz grains. This forms the basis for further investigations into the sensitivity of the equivalent dose (D_e) estimates to a range of different analytical approaches, including changes in the size of the test dose, the choice of signal integration interval, the subtraction of an appropriate background, and isolation of the most light-sensitive (‘fast’) component of quartz OSL. We also report the results of an inter-operator test of D_e determination using seven new samples from Blombos Cave, and demonstrate the reproducibility of results obtained for two samples that had been dated previously at another laboratory and were measured and analysed again in this study. Together, these tests validate the robustness of the Blombos Cave single-grain OSL age estimates to a variety of alternative OSL dating procedures. We have incorporated, for the first time, these ages for Blombos Cave into a data set of all single-grain OSL ages for Still Bay and Howieson's Poort sites across southern Africa, and have used a statistical model to re-evaluate the timing and duration of the Still Bay industry. We calculate the most plausible start and end dates of the Still Bay as 72.2 ka and 71.3 ka, respectively – amounting to a duration of 0.9 ka – and estimate (with conventional 95% confidence) that this industry began no earlier than 75.5 ka, ended no later than 67.8 ka and lasted no longer than 6.6 ka.     

OSL and TL dating of the Middle Stone Age sequence at Diepkloof Rock Shelter (South Africa): a clarification

Diepkloof Rock Shelter offers an exceptional opportunity to study the onset and evolution of both Still Bay (SB) and Howiesons Poort (HP) techno-complexes. However, previous age estimates based on luminescence dating of burnt quartzites (Tribolo et al., 2009) and of sediments (Jacobs et al., 2008) were not in agreement. Here, we present new luminescence ages for 17 rock samples (equivalent dose estimated with a SAR-ITL protocol instead of classical MAAD-TL) as well as for 5 sediment samples (equivalent dose estimated with SAR-single grain OSL protocol) and an update of the 22 previous age estimates for burnt lithics (modified calibration and beta dose estimates). While a good agreement between the rock and sediment ages is obtained, these estimates are still significantly older than those reported by Jacobs et al. (2008). After our own analyses of the sediment from Diepkloof, it is suspected that these authors did not correctly chose the parameters for the equivalent dose determination, leading to an underestimate of the equivalent doses, and thus of the ages.     

江苏泰州宋代涵洞发掘简报

江苏泰州城历史悠久,有"汉唐古郡,淮海名区"之称,但是唐宋时期的城市布局不明。2006年8月,泰州市博物馆对泰州城宋代涵洞进行了考古发掘,发现不同时期灰坑、墓葬,出土了一批汉、五代、宋、明时期的陶瓷器、擂球。此次发掘不仅解决了不同时期涵洞和城墙的建筑年代问题,而且为研究宋代泰州的城市规模和布局、研究古代城墙配套设施提供了新的资料。     

How Oil Twists the Hegemon's Arm: The Case of the United States and Saudi Arabia and Their Ambivalent Partnership

The U.S.–Saudi relationship is often seen as an oxymoron. These allies have differed in their foreign policy interests — varied in the need, one for the other — but never severed ties. When the 9/11 attacks are added to the mix, questions are raised about why these ambivalent allies continue to tolerate each other. This study argues that although the United States is the preponderant power, Saudi Arabia has primacy in the energy market. This has caused both countries to remain allies through the different oil crises, the 9/11 attacks, and in spite of the Arab‐Israeli conflict. This contravenes the hegemonic stability theory about alliance formation and duration. Saudi Arabia's roles in the 1973, 1979, 2008, and 2012–2015 oil crises all demonstrate its ability and willingness to act independently of the United States. The fact that it can do this and still maintain its strategic partnership with the United States is incredulous. This invites a revision of the hegemonic stability theory since strong and persistent defection from the hegemon's wishes should catalyze some comparable form of punishment or a severance of the relationship.     

Life at the end of the Holocene moist phase in south‐east Arabia — the Late Neolithic site of Jebel Thanais 1 (JTH1)

The surface site of Jebel Thanais 1 is located in the Emirate of Sharjah (U.A.E.) at the western flank of the Jebel Faya/Jebel Buhais anticline structure. A dense scatter of lithic artefacts and fireplaces indicates Stone Age settlement activities in this area. Radiocarbon dates obtained from fireplaces date the occupation of the site to both the beginning and the very end of the fifth millennium cal. BC. During the second half of the fifth millennium the deterioration of climatic conditions in south‐east Arabia had a noticeable impact on settlement patterns and subsistence strategies. While coastal habitation sites from this time are well known along the shores of the Oman peninsula, only a few poorly dated sites allow insights into habitation and raw material procurement strategies and lithic technology in the interior. Investigations into the spatial structure of the site and an analysis of lithic finds will contribute to a better understanding of this period.     

On the provenance and manufacture of red-slipped fine ware from ancient Cassope (NW Greece): evidence by X-ray analytical methods

Energy-dispersive X-ray fluorescence spectroscopy was used to characterize red-slipped pottery (2nd–1st century BC) from ancient Cassope, north-western Greece. The compositional data were statistically treated by principal component analysis and chemical groups were established, representing locally produced and imported items. Mineralogical investigation by X-ray diffraction indicated firing temperatures in the range from 850 to 1000 °C for most of the sherds, while one group consisted of over-fired items, possibly in excess of 1050 °C. The morphology and elemental composition of the ceramic bodies and surface slips were examined through scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy. The analyses revealed that different pottery groups exhibit surface slips of different nature, in terms of thickness, degree of vitrification and elemental composition. Overall, the diversity in technological characteristics of the examined sherds is indicative of the socio-economic conditions prevailing in Cassopaea during the late Hellenistic period.     

Characterization of prehispanic cosmetics found in a burial of the ancient city of Teotihuacan (Mexico)

The present paper reports the chemical data obtained on samples of pigmenting materials contained in 31 miniature vessels found in a burial found in Teopancazco, a multiethnic neighborhood center located in the southeastern sector of the archaeological site of Teotihuacan (Central Mexico) and the analytical protocol established for the complete characterization of these archaeological materials. For this purpose a multi-technique approach based on the combination of several non destructive and micro-destructive instrumental techniques, namely, light microscopy (LM), scanning electron microscopy-X-ray microanalysis (SEM-EDX), transmission electron microscopy (TEM), voltammetry of microparticles (VMP), X-ray microdiffraction (μXRD), X-ray diffraction (XRD), UV-Vis spectrophotometry, FTIR spectroscopy and gas chromatography-mass spectrometry (GC-MS) has been developed in an attempt to completely characterize these materials. These instrumental techniques provide reliable and complementary data including elemental and mineralogical composition, identification of functional groups as well as speciation studies of electroactive species. Among the most relevant findings, volcanic pyroclastic rocks and clayey soils, most probably, from the Teotihuacan valley as well as galena, jarosite and mica from other provenances in Mesoamerica, have been identified. Charcoal and Ocote resin have also been identified. The chemical composition of the samples is discussed with a view to the possible function as cosmetic materials and their use in funerary rites. The results have been critically compared with those others obtained in other ancient civilizations. The study carried out on the materials found in the burial 105 is especially relevant insofar it represents the first evidence, scientifically characterized, of the use of cosmetics in Mesoamerica at this early period (AD 200-550).     

Radiocarbon and U-series dating of the endemic deer Praemegaceros cazioti (Depéret) from “Grotta Juntu”, Sardinia

Radiocarbon and U-series methods (²³⁰Th/U and ²³¹Pa/²³⁵U) for absolute age determination have been applied to some fossil samples from Grotta Juntu, in North Eastern Sardinia (Italy). The remains belong to the endemic deer species Praemegaceros cazioti, which is here represented by an almost complete skeleton. The three dating methods lead to concordant ages of about 7500 years BP, indicating that the skeleton was maintained as closed system after burial. Taking into consideration these results, Praemegaceros cazioti from Grotta Juntu is now the youngest representative of this species in Sardinia.     

The cultural landscape near the ancient city of Tharros (central West Sardinia): vegetation changes and human impact

The evolution of the cultural landscape in coastal western Sardinia is investigated by means of pollen analysis in the Mistras Lagoon sediments, near the ancient city of Tharros, with particular attention to changes in evergreen vegetation and the impact of human activity. The pollen diagram, spanning the time interval from 5300 to 1600 cal BP, documents the influence of man, climate, and geomorphic dynamics on the evolution of a semi-open evergreen vegetation landscape and variations in extent of a salt-marsh environment. Anthropogenic indicators and microcharcoals concur in depicting increased land use coinciding with the Nuragic, Phoenician, Punic and Roman dominations. Pollen data, along with archaeobotanical evidence, suggest a prevailing arable farming economy, vocated to Vitis and cereals exploitation, during the Nuragic phase until 2400 cal BP, replaced since then by a prevailing stock rearing economy. Between 2050 and 1600 cal BP, a less intensive human impact on the landscape is profiled, consistently with the archaeologically documented abandonment of the rural villages in favour of a slow urbanization, experienced by the Sinis territory in Imperial times. The pollen record provides new insights into the history of important economic plants in the Mediterranean, such as Vitis, Olea and Quercus suber. The results of the pollen analysis reveal how the records of these taxa are primarily influenced by the cultural development of the Sinis region and secondarily by dynamics involving the natural companion vegetation.     

Direct radiocarbon (AMS) dating of split-based points from the (Proto)Aurignacian of Trou de la Mère Clochette,Northeastern France. Implications for the characterization of the Aurignacian and the timing of technical innovations in Europe

Radiocarbon (AMS) dates on two split-based point wings and a hominin molar from the site of Trou de la Mère Clochette in the French Jura are presented in this paper. Dating split-based points has very rarely been undertaken. This is unfortunate given that these artefacts are critical to our definition and characterization of Early Upper Palaeolithic technocomplexes, as they are considered to be the type fossil of the Classic Aurignacian.     

Calcium oxalate AMS C dating and chronology of post-Palaeolithic rock paintings in the Iberian Peninsula. Two dates from Abrigo de los Oculados (Henarejos,Cuenca, Spain)

Since 2005 we have been utilizing accelerator mass spectrometry (AMS) ¹⁴C dating in research on calcium oxalate crusts associated with open air rock art of the Iberian Peninsula. In this paper we present two dates linked with three eye-idol pictographs at Abrigo de los Oculados (Henarejos, Cuenca, Spain). Radiocarbon ages for these motifs agree with the expected iconography-based archaeological chronology. Such oxalate dates could provide an independent basis for evaluating chronological theories for post-Palaeolithic sites, designated in the UNESCO World Heritage List as Rock Art of the Mediterranean Basin on the Iberian Peninsula.