Radiocarbon Dates on Textile and Bark Samples from the Central Grave of the Adena Mound (33RO1), Chillicothe,Ohio

The Adena Mound (33RO1) is the type site of the Adena culture, yet there have been no radiocarbon dates to place it reliably within a temporal framework. Fortunately, the artifact collection, curated by the Ohio Historical Society, includes objects that are highly suitable for radiocarbon dating, including fragments of textiles and tree bark associated with the central burial. We selected a textile fragment and two bark fragments for radiocarbon dating. The textile exhibits alternate pair twine with very fine yarns probably composed of cellulose bast fibers. The bark is from a black locust (Robinia pseudoacacia) tree. The results of the radiocarbon dating indicate that the Adena Mound was constructed between the end of the second century B.C. and the beginning of the first century A.D., placing it near the midpoint in the sequence of radiocarbon-dated Adena culture sites. This study demonstrates the value of museum collections for gleaning new data from curated materials.     

BAYESIAN ANALYSIS OF PLEISTOCENE CHRONOMETRIC METHODS*

Bayesian analysis of radiocarbon dates on Holocene archaeological sites has become well established. Application to Pleistocene sites dated by multiple techniques would be advantageous. This paper develops the necessary mathematical apparatus in the form of likelihoods for luminescence dating, and uranium‐series dating, and considers the possibility for amino‐acid racemization dating. Application of the new methods is illustrated using the stratigraphic sequences of dates from the sites of Saint‐Césaire and La Chaise‐de‐Vouthon. For application to amino‐acid racemization dating, fuller publication of data is found to be required.     

Radiocarbon dating of marine shell samples. The marine radiocarbon reservoir effect of coastal waters off Atlantic Iberia during Late Neolithic and Chalcolithic Periods

Radiocarbon dates on marine shells have not been used as extensively as charcoal or bone dates for the setting up of absolute chronologies because interpreting these dates is complicated by the marine radiocarbon reservoir effect. Nevertheless marine shellfish were used widely at least during the Holocene and their shells are abundant and usually well preserved in archaeological deposits located near shorelines. Consequently prior research concerning the oceanographic conditions and the marine radiocarbon reservoir effect of a particular coastal area is needed in order to set up reliable chronologies for that region. Values of regional marine radiocarbon reservoir effect – ΔR – of coastal waters off Atlantic Iberia, some of its variability along the Holocene and its correlation with the upwelling phenomenon were determined during previous research. More data related to the ΔR values for western Portuguese coastal waters during the Late Neolithic and the Chalcolithic, a time interval badly sampled in previous research, were recently obtained. These values can be compared with ΔR values already determined for the Gulf of Cadiz. Besides the importance of these values for a better knowledge of the palaeoceanography and palaeoclimatology of Atlantic Iberia, from now on archaeologists can set up reliable chronologies for Late Neolithic and Chalcolithic contexts using marine shell samples of that origin for radiocarbon dating.     

New radiocarbon dating of the transition from the Middle to the Upper Paleolithic in Kebara Cave,Israel

The Middle to Upper Paleolithic transition (MP-UP transition) is considered a major technological and cultural threshold, at the time when modern humans spread “out of Africa”, expanded from the Levant into Europe and possibly into central and northern Asia. The dating of this techno-cultural transition has proved to be extremely difficult because it occurred sometime before 40,000 radiocarbon years before present (¹⁴C years BP), which is close to the end of the effective dating range of radiocarbon. Other dating methods such as Thermoluminescence (TL) or Electron Spin Resonance (ESR) are not sufficiently precise to date the recorded archaeological MP-UP transition in the Levant. Here we report a consistent set of stratified radiocarbon ages on freshly excavated charcoal from Kebara Cave, Mt. Carmel (Israel), that span the late Middle Paleolithic (MP) and Early Upper Paleolithic (EUP) This study applied novel strategies to improve sample preparation techniques and data analysis to obtain high-resolution radiocarbon models. From this study it is proposed that the MP-UP transition for this site can be placed immediately after 45,200 ± 700 ¹⁴C years BP and before 43,600 ± 600 ¹⁴C years BP or from 49/48 to 47/46 radiocarbon calibrated years before present (years Cal BP).     

Debates over Palaeolithic chronology – the reliability of C is confirmed

The debate about the complex issues of human development during the Middle to Upper Palaeolithic transition period (45–35 ka BP) has been hampered by concerns about the reliability of the radiocarbon dating method. Large ¹⁴C anomalies were postulated and radiocarbon dating was considered flawed. We show here that these issues are no longer relevant, because the large anomalies are artefacts beyond plausible physical limits for their magnitude. Previous inconsistencies between ¹⁴C radiocarbon datasets have been resolved, and a new radiocarbon calibration curve, IntCal09 (Reimer et al., 2009), was created. Improved procedures for bone collagen extraction and charcoal pre-treatment generally result in older ages, consistent with independently dated time markers.     

RADIOCARBON DATING OF MORTARS FROM ANCIENT GREEK PALACES

This study deals with radiocarbon dating of lime mortars which were used as supports for Mycenaean and Minoan paintings. The ¹⁴C dates are. on the whole, compatible with the historical data. and thus show that a large proportion of the Mycenaean surficial coatings can be dated by the radiocarbon method. However. in order to determine the age of the mortars accurately. it is necessary to evaluate the amount of sedimentary carbonate which may have been added to them. It is shown here that the oxygen and carbon isotope compositions of lime mortars are significant indicators that such a mixing actually took place.     

Radiocarbon Wiggle-Match Dating in the Intertidal Zone

Radiocarbon wiggle-match dating is a technique that can combine the versatility of radiocarbon dating with chronological information from tree-rings. This makes it useful in contexts where timbers are preserved, but dendrochronological dating is impossible. As intertidal and marine timbers are waterlogged, this can favor their preservation and hence allow wiggle-match ¹⁴C dating, which can be of significant help in deriving relatively precise chronologies for a range of coastal structures. As the technique depends on making multiple radiocarbon measurements towards a single date, efficiency in application is the key and hence a number of practical considerations need to be taken into account in advance of conducting a dating program. This paper discusses some of these practical concerns and reviews them in the context of the intertidal crannogs in the Firth of Clyde on the west coast of Scotland.     

TREGIFFIAN: THE CHRONOLOGY OF AN ENTRANCE GRAVE

The Tregiffian project involved the analysis and dating of the archive from unpublished excavations in the 1960s and 1970s at an entrance grave in Penwith, Cornwall. A major aim of the project was to establish a robust chronological basis for the use of the entrance grave for burial: 10 samples of cremated human bone were submitted for radiocarbon dating and Bayesian modelling undertaken. The modelling indicates that the use of the chamber for burial between began in 1780–1510 BC and ended in 1595–1425 BC. The results are hugely significant as they provide the first modelled dating from a Penwith entrance grave. This paper discusses the results from the radiocarbon dating project and reconsiders entrance graves in the wider context of the Early Bronze Age megalithic tombs which are found around the Irish Sea.     

Radiocarbon dating: Some practical considerations for the archaeologist

The article is divided into four main sections in each of which a key aspect of radio-carbon dating is discussed with emphasis on the practical implications for users of dates. The four topics which the article attempts to deal with are, in turn, (i) the effect on the radiocarbon timescale of the variations in atmospheric ¹⁴C now known to have occurred in the past and the role of other absorlute dating methods in investigating these, (ii) laboratory measurement of ¹⁴C, (iii) selection of optimum samples for dating and (iv) some of the limitations of the final dates. The theme is essentially that the technical difficulties of radiocarbon measurement in the laboratory have been overcome to the extent that the physical measurements can now be made with high precision, that is to within ±1% or better, as a routine. Thus, it is more important than ever (a) that only reliable samples having very firm associations should be dated and (b) that pretreatment of such samples by the dating laboratory to remove any age contaminants should be completely effective. However, in addition to the recognized statistical limitations, the absolute accuracy of radio-carbon dating is limited by the past ¹⁴C variations. Coupled with the requirements of proper association and pretreatment of samples is the long-term need to establish an overall correlation between radiocarbon and calendar years. At present this is still a matter for final agreement by the laboratories concerned. Meanwhile, when all possible steps have been taken to ensure the reliability of the date messurements, these can strictly only be compared with one another in terms of radiocarbon years bp. In practice this is often too restrictive but any attempts at calibration must be regarded as approximations for the time being. In this article the lower and upper case notation advocated in Antiquity46, 265, for radiocarbon and calendar years respectively has been followed.     

X-RAY FLUORESCENCE CHARACTERIZATION OF THE CORONA FERREA*

X-ray fluorescence (XRF) analyses of metals, glasses and enamels from the Corona Ferrea, or Iron Crown, of Monza are reported. The method followed to obtain quantitative analysis of metal alloys was based on comparison with standards and it is framed on the more general problem of XRF quantitative analysis of irregularly shaped objects with a portable instrument. Preliminary radiocarbon dating results are also reported.     

Comparison of fluoride and direct AMS radiocarbon dating of black bear bone from Lawson Cave,Missouri

Abstract

After a 20-year hiatus (1955–1975) during which few archaeologists discussed fluoride dating, the method again received attention in the 1980s and 1990s when some argued for its validity. As a dating method, fluoride dating depends on the rate at which fluorine ions replace hydroxyl ions in osseous tissue. The rate of replacement is influenced by the properties of the skeletal part (SP), sediment chemistry (K), and sediment hydrology (H), and the replacement rate influences estimates of time. Calibrated AMS radiocarbon assays of 10 black bear (Ursus americanus) femora from a natural-trap cave in central Missouri are weakly correlated with fluorine concentrations, determined by neutron activation analysis in the 10 femora. Despite minimal variation in SP, K, and H, results indicate fluoride dating can be considered a valid dating method only in cases when the chronological validity of its results are confirmed with independent chronometric data. As similarities in fluorine amounts across specimens increase, provenience information and bone orientation data as well as fine resolution data on K and H become critical to the application of fluoride dating.     

ON THE AGE AND CONTENT OF JAR‐35—A SEALED AND INTACT STORAGE JAR FOUND ON THE SOUTHERN PLATEAU OF QUMRAN*

An intact and sealed storage jar known as Jar‐35 was found in 2004, south of the Qumran settlement. A previous study identified tartrate in the deposit of the jar, indicating the possible past presence of wine ( Buti et al. 2006 ). However, we cannot confirm this finding. Using liquid and gas chromatography with mass spectrometric detection, no trace of tartaric acid or salts thereof could be detected in our samples. We show that the major component of the deposit is gypsum. No other organic compounds were identified with the methods that we have applied. Both radiocarbon dating of charcoal in the deposit and thermoluminescence dating of the ceramic jar show that it dates to the main period of habitation at Qumran (c. 100 bc to ad 70).     

‘Old wood’ effect in radiocarbon dating of prehistoric cremated bones?

Numerous reports of successful radiocarbon dating of cremated bones have emerged during the last decade. The success of radiocarbon dating cremated bones depends on the temperature during burning and the degree of recrystallisation of the inorganic bone matrix. During cremation bones undergo major morphological and mineralogical changes which have raised some interesting questions and discussion on the origin of the carbon source in archaeologically cremated bones. Recent laboratory experiments reveal that the properties of the combustion atmosphere play a significant role regarding the source carbon in cremated bones. Thus radiocarbon dating cremated bones is potentially dating the wood used for the cremation fire. Here we compare a high precision radiocarbon dated human bone with an associated dendrochronological age from an oak coffin. We find that the age discrepancy between the dendrochronological age and the cremated bone of 73 ± 26 ¹⁴C yr is best accounted for by the so called ‘old wood’ effect.     

Radiocarbon dating of prehistoric hearths in alpine northern Sweden: problems and possibilities

The chronology of prehistoric Sami settlement sites has previously been established by conventional radiocarbon dating of bulk charcoal samples associated with hearths from sunken hut floors (stállo-foundations). Here we present results of a comprehensive dating exercise of stállo-foundations in the alpine area of northern Scandinavia using Accelerator Mass Spectrometry (AMS) radiocarbon dating of charcoal. Over a 3 km² study area, AMS calibrated ages of hearth charcoal from 22 stállo-foundations across 12 sites securely date these features to between cal. AD 640 and AD 1180. Only small variations in age were found between charcoal samples from different areas of a given hearth. Statistical analysis of all the charcoal AMS radiocarbon dates obtained reveals that 12 stállo-foundations across nine sites are contemporaneous and date to the Viking Period (AD 800–AD 1050). The tightly constrained AMS-based chronology of stállo-foundations contrasts with the existing chronology based on conventional radiocarbon analysis, which places these features within a significantly greater time-frame of between AD 600 and AD 1900, with most dates ranging between AD 800 and AD 1350.This discrepancy is likely to result from the necessity of collecting composite hearth charcoal particles, which may originate from different phases of occupation, in order to achieve the required final carbon content for conventional radiocarbon analysis. We argue that the new AMS-based radiocarbon chronology of stállo-foundations presented here supersedes the existing chronology based on conventional (Gas Proportional counting) radiocarbon analysis and we advocate the use of AMS radiocarbon dating in future hearth investigations.     

THERMOLUMINESCENT DATING OF COLOMBIAN POTTERY IN THE YOTOCO STYLE

Two contexts from the Colombian sites, Yotoco Ferry and Moralba, had been linked by archaeological similarities in pottery style, and dated by association with ware from other sites at circaa.d. 1000. However, radiocarbon dating of those contexts set Moralba at circa 800 b.c. , some 2000 yr older than Yotoco Ferry. Thermoluminescent dating of pottery from Yotoco Ferry dated it at circaa.d. 900, and pottery from Moralba was dated at circaa.d. 870. In addition a metal-smelting pottery crucible, thought to be prehispanic, was studied by thermoluminescence and dated, on the contrary, at less than 120 yr old.     

Human bioarchaeology: Group identity and individual life histories – Introduction

The approach of individual life histories has been facilitated by a rapid growth in the area of bio- and archaeological sciences, and in human osteology. Concurrent improvements to radiocarbon dating and focus on high resolution paleoenvironmental reconstructions have moved the new research to the annual or decadal scale of analysis. Together, this new approach allows us: (1) to reconstruct long segments of individual life histories from birth to death; (2) to assess variation in prehistoric human behaviour; and (3) to place this behaviour in the context of dynamic interactions with the natural environment. The emphasis on individuals rather than groups or cultures feeds naturally into the modern scientific-evolutionary archaeology, a school of thought which focuses on mechanisms generating human cultural diversity. While it is the populations that evolve, it is the variation generated at the individual level that is necessary to set this process in motion. To an evolutionary archaeologist and anthropologist it is the behavioural variability that is of primary research interest. Hence the paramount importance of documenting and understanding what people do on a daily basis and how they differ from each other in their needs, preferences, choices, decisions, and strategies developed and employed to satisfy them.     

Chronostratigraphy of an Eroding Complex Atlantic Round House,Baile Sear,Scotland

A high-resolution chronostratigraphy has been established for an eroding Atlantic round house at Sloc Sàbhaidh (North Uist, Scotland), combining detailed OSL profiling and dating of sediments encompassing the main bracketing events associated with the monument, radiocarbon AMS dates on bone recovered from excavated features and fills within it, and TL dates on pottery and burnt clay. Concordant OSL and radiocarbon evidence place construction of the wheelhouse in the first to second centuries AD, contemporary with dates from the primary occupation. Beneath the wheelhouse, clay deposits containing burnt material, attest to cultural activity in vicinity to the monument in the preceding second to first centuries BC. At a later date, the southern wall collapsed, was rebuilt, and the interior spaces to the monument re-structured. The chronology for the later horizons identified from the sediment luminescence dates extends to the second half of the first millennium AD, which goes beyond the range of the radiocarbon dates obtained. The data from ceramics encompass both periods. The juxtaposition of the dating evidence is discussed relative to short and longer chronologies for this Iron Age monument. Corollaries of this research are the implications that based on the long chronology, some of the ecofacts (bone) appear to be residual, and that the temporal duration of Hebridean Coarse Ware may extend into the second half of the first millennium AD.     

四川广汉三星堆遗址四号祭祀坑的碳十四年代研究

2020年,广汉三星堆遗址新发现祭祀坑的田野考古发掘工作正式启动,为解决祭祀坑的年代问题,四川省文物考古研究院委托国家文物局考古研究中心与北京大学考古文博学院考古年代学联合实验室对四号祭祀坑开展了碳十四年代研究,得到6个碳十四年代数据,经过贝叶斯统计树轮校正计算得到其埋藏年代有95.4%的概率落在距今3148—2966年的时间范围之内,属商代晚期。     

Radiocarbon Dating and the Historical Archaeology of Korea: An Alternative Interpretation of Hongryeonbong Fortress II in the Three Kingdoms Period,Central Korea

Relying heavily upon historical records to build archaeological chronologies, many Korean historical archaeologists question the utility of radiocarbon dating. To challenge this tendency, we test a model based on historical records by analyzing radiocarbon dates. We dated two bulk samples from Hongryeonbong Fortress II, Seoul, South Korea, which is known historically to have been occupied between a.d. 500 and 551. By dividing bulk samples into smaller aliquots, we dated 40 subsamples and statistically estimated consensus dates. The consensus dates do not support expectations of the historical model, as they do not lie within the temporal range provided by historical records. We propose an alternative model that explains both the radiocarbon dates and the historical records. It is suggested that radiocarbon dating can be successfully applied to the reconstruction of historical periods and is a way of mitigating possible biases of models based solely on historical records.